ES479718A1 - Procedimiento para la recuperacion de ciclohexanona-oxina a partir de una solucion de la oxima en tolueno. - Google Patents

Procedimiento para la recuperacion de ciclohexanona-oxina a partir de una solucion de la oxima en tolueno.

Info

Publication number
ES479718A1
ES479718A1 ES479718A ES479718A ES479718A1 ES 479718 A1 ES479718 A1 ES 479718A1 ES 479718 A ES479718 A ES 479718A ES 479718 A ES479718 A ES 479718A ES 479718 A1 ES479718 A1 ES 479718A1
Authority
ES
Spain
Prior art keywords
oxime
toluene
solution
cyclohexanone
recovery
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES479718A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stamicarbon BV
Original Assignee
Stamicarbon BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stamicarbon BV filed Critical Stamicarbon BV
Publication of ES479718A1 publication Critical patent/ES479718A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/14—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Procedimiento para la recuperación de ciclohexanona-oxima a partir de una solución de la oxima en tolueno obtenida en la preparación de ciclohexanona-oxima a partir de ciclohexanona separando el tolueno y la oxima por destilación y recuperando la oxima sustancialmente pura, caracterizado porque la separación por destilación se comienza a partir de una solución de la oxima en tolueno obtenido por conversión incompleta de la ciclohexanona y que tienen un contenido de cilohexanona de más de 0,5 gramos por 100 gramos de oxima y se recupera la ciclohexanona-oxima con menos 0,1 gramos de cliclohexanona por 100 gramos de oxima.
ES479718A 1978-04-20 1979-04-19 Procedimiento para la recuperacion de ciclohexanona-oxina a partir de una solucion de la oxima en tolueno. Expired ES479718A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL7804195A NL7804195A (nl) 1978-04-20 1978-04-20 Werkwijze voor het winnen van cyclohexanonoxime.

Publications (1)

Publication Number Publication Date
ES479718A1 true ES479718A1 (es) 1980-02-01

Family

ID=19830686

Family Applications (1)

Application Number Title Priority Date Filing Date
ES479718A Expired ES479718A1 (es) 1978-04-20 1979-04-19 Procedimiento para la recuperacion de ciclohexanona-oxina a partir de una solucion de la oxima en tolueno.

Country Status (10)

Country Link
EP (1) EP0005291B1 (es)
JP (1) JPS54148751A (es)
KR (1) KR850000718B1 (es)
BR (1) BR7902418A (es)
DE (1) DE2961592D1 (es)
ES (1) ES479718A1 (es)
IN (1) IN150575B (es)
NL (1) NL7804195A (es)
PT (1) PT69505A (es)
YU (1) YU89879A (es)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110423206A (zh) * 2019-07-17 2019-11-08 天津大学 从氨肟化反应产物中分离环己酮肟、环己酮与甲苯的方法

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1318141A1 (en) 2001-12-04 2003-06-11 Dsm Nv Process for treating an aqueous medium containing phosphate, cyclohexanone and cyclohexanone oxime
ITMI20011361A1 (it) * 2001-06-28 2002-12-28 Enichem Spa Metodo di purificazione della cicloesanossima
WO2003048110A1 (en) 2001-12-04 2003-06-12 Dsm Ip Assets B.V. Process for treating an aqueous medium containing cyclohexanone oxime and cyclohexanone
EP1663956A1 (en) * 2003-01-30 2006-06-07 DSM IP Assets B.V. Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent
SG123716A1 (en) * 2004-12-22 2006-07-26 Sumitomo Chemical Co Process for producing cyclohexanone oxime
CN103382164B (zh) * 2012-05-04 2017-08-11 Cap Iii 有限公司 一种纯化从环己酮肟合成区获得的有机物溶液的方法
CN103193672B (zh) * 2013-03-11 2014-09-17 浙江圣安化工有限公司 一种肟的蒸馏方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1303739A (es) * 1970-06-15 1973-01-17
JPS4936656A (es) * 1972-08-04 1974-04-05

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110423206A (zh) * 2019-07-17 2019-11-08 天津大学 从氨肟化反应产物中分离环己酮肟、环己酮与甲苯的方法
CN110423206B (zh) * 2019-07-17 2022-07-08 天津大学 从氨肟化反应产物中分离环己酮肟、环己酮与甲苯的方法

Also Published As

Publication number Publication date
DE2961592D1 (en) 1982-02-11
JPS54148751A (en) 1979-11-21
IN150575B (es) 1982-11-13
YU89879A (en) 1982-08-31
BR7902418A (pt) 1979-10-23
EP0005291B1 (en) 1981-12-23
KR850000718B1 (ko) 1985-05-23
PT69505A (en) 1979-05-01
EP0005291A1 (en) 1979-11-14
KR830001880A (ko) 1983-05-19
NL7804195A (nl) 1979-10-23

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 19970401