ES484556A1 - Un procedimiento para la preparacion de cloro-bis(alquilami-no)-s-triacina - Google Patents
Un procedimiento para la preparacion de cloro-bis(alquilami-no)-s-triacinaInfo
- Publication number
- ES484556A1 ES484556A1 ES484556A ES484556A ES484556A1 ES 484556 A1 ES484556 A1 ES 484556A1 ES 484556 A ES484556 A ES 484556A ES 484556 A ES484556 A ES 484556A ES 484556 A1 ES484556 A1 ES 484556A1
- Authority
- ES
- Spain
- Prior art keywords
- alkylamino
- chloro
- bis
- water
- triazines
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 125000003282 alkyl amino group Chemical group 0.000 title abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- 239000008346 aqueous phase Substances 0.000 abstract 2
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 abstract 2
- 150000002894 organic compounds Chemical class 0.000 abstract 2
- JYEUMXHLPRZUAT-UHFFFAOYSA-N 1,2,3-triazine Chemical compound C1=CN=NN=C1 JYEUMXHLPRZUAT-UHFFFAOYSA-N 0.000 abstract 1
- 150000003973 alkyl amines Chemical class 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/48—Two nitrogen atoms
- C07D251/50—Two nitrogen atoms with a halogen atom attached to the third ring carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/42—One nitrogen atom
- C07D251/44—One nitrogen atom with halogen atoms attached to the two other ring carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Un procedimiento para la preparación de cloro-bis (alquilamino)-s- triacina mediante reacción de sustitución por etapas de dos átomos de cloro de cloruro cianúrico por grupos alquilamino en un medio alcalino que comprende agua y un compuesto orgánico líquido, disolvente para el cloruro cianúrico y que forma un sistema de dos fases con agua, en donde la reacción se lleva a cabo con un exceso molar de alquilamina en la segunda etapa de sustitución y en donde dicho compuesto orgánico se separa por destilación de la mezcla reaccional resultante de la segunda etapa de sustitución, caracterizado porque una vez completada la citada segunda etapa de sustitución por reacción con el exceso de alquilamina, se libera dicha mezcla reaccional de su fase acuosa y se mezcla la suspensión o solución residual de cloro-bis (alquilamino)-s-triacina en el compuesto orgánico así obtenido, antes o durante la destilación del compuesto orgánico, con agua adicionada en una cantidad volumétrica de 30 a 150% con respecto a la de dicha fase acuosa.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT28220/78A IT1099671B (it) | 1978-09-29 | 1978-09-29 | Perfezionamenti nel procedimento per la produzione di cloro-bis (alchilammino)-s-triazine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES484556A1 true ES484556A1 (es) | 1980-05-16 |
Family
ID=11223170
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES484556A Expired ES484556A1 (es) | 1978-09-29 | 1979-09-28 | Un procedimiento para la preparacion de cloro-bis(alquilami-no)-s-triacina |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5817750B2 (es) |
| CH (1) | CH640841A5 (es) |
| DE (1) | DE2939552A1 (es) |
| ES (1) | ES484556A1 (es) |
| FR (1) | FR2437407A1 (es) |
| GB (1) | GB2032426B (es) |
| IL (1) | IL58212A0 (es) |
| IT (1) | IT1099671B (es) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60133697U (ja) * | 1984-02-16 | 1985-09-06 | 日鉱メタルプレ−テイング株式会社 | 電磁波シ−ルド材 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS52131592A (en) * | 1976-04-27 | 1977-11-04 | Daicel Chem Ind Ltd | Synthesis of triazines |
-
1978
- 1978-09-29 IT IT28220/78A patent/IT1099671B/it active
-
1979
- 1979-09-05 GB GB7930772A patent/GB2032426B/en not_active Expired
- 1979-09-10 IL IL58212A patent/IL58212A0/xx unknown
- 1979-09-24 FR FR7923675A patent/FR2437407A1/fr active Granted
- 1979-09-25 JP JP54123050A patent/JPS5817750B2/ja not_active Expired
- 1979-09-27 CH CH868979A patent/CH640841A5/it not_active IP Right Cessation
- 1979-09-28 DE DE19792939552 patent/DE2939552A1/de not_active Withdrawn
- 1979-09-28 ES ES484556A patent/ES484556A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CH640841A5 (it) | 1984-01-31 |
| JPS5549362A (en) | 1980-04-09 |
| DE2939552A1 (de) | 1980-04-17 |
| GB2032426A (en) | 1980-05-08 |
| IT1099671B (it) | 1985-09-28 |
| IL58212A0 (en) | 1979-12-30 |
| IT7828220A0 (it) | 1978-09-29 |
| FR2437407B1 (es) | 1981-05-29 |
| GB2032426B (en) | 1982-11-17 |
| JPS5817750B2 (ja) | 1983-04-09 |
| FR2437407A1 (fr) | 1980-04-25 |
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