ES8504830A1 - Procedimiento para la preparacion de n-fosfonometilglicina - Google Patents

Procedimiento para la preparacion de n-fosfonometilglicina

Info

Publication number
ES8504830A1
ES8504830A1 ES526547A ES526547A ES8504830A1 ES 8504830 A1 ES8504830 A1 ES 8504830A1 ES 526547 A ES526547 A ES 526547A ES 526547 A ES526547 A ES 526547A ES 8504830 A1 ES8504830 A1 ES 8504830A1
Authority
ES
Spain
Prior art keywords
hydantoin
derived
procedure
preparation
hydroximethyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES526547A
Other languages
English (en)
Other versions
ES526547A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stauffer Chemical Co
Original Assignee
Stauffer Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stauffer Chemical Co filed Critical Stauffer Chemical Co
Publication of ES526547A0 publication Critical patent/ES526547A0/es
Publication of ES8504830A1 publication Critical patent/ES8504830A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D233/72—Two oxygen atoms, e.g. hydantoin
    • C07D233/76—Two oxygen atoms, e.g. hydantoin with substituted hydrocarbon radicals attached to the third ring carbon atom
    • C07D233/78—Radicals substituted by oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/645—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having two nitrogen atoms as the only ring hetero atoms
    • C07F9/6503—Five-membered rings
    • C07F9/6506—Five-membered rings having the nitrogen atoms in positions 1 and 3

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Saccharide Compounds (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

PROCEDIMIENTO PARA LA PREPARACION DE N-FOSFONOMETILGLICINA.CONSISTE EN: A) LA REACCION DE HIDANTOINA O UNA HIDANTOINA-3-SUSTITUIDA DE FORMULA (I) CON PARAFORMALDEHIDO EN PRESENCIA DE UN ACIDO CARBOXILICO DE BAJO PESO MOLECULAR PARA PRODUCIR UNA MEZCLA DE PRODUCTOS INTERMEDIARIOS, INCLUYENDO EL 1-(HIDROXIMETIL) DERIVADO DE LA HIDANTOINA DE PARTIDA; B) CONVERTIR 1-(HIDROXIMETIL) DERIVADO A 1-FOSFONOMETILHIDANTOINA POR ADICION ULTERIOR A LA MEZCLA DE REACCION DE TRICLORURO DE FOSFORO Y TRIBROMURO DE FOSFORO O ACIDO FOSFORICO Y UN ANHIDRIDO DE ACIDO CARBOXILICO, Y CONTINUAR LA REACCION HASTA FORMAR EL 1-(FOSFONOMETIL) DERIVADO; C) HIDROLIZAR 1-(FOSFONOMETIL) DERIVADO ASI FORMADO CON UNA SOLUCION ACUOSA DE UNA BASE PARA PRODUCIR UNA SAL DE N-FOSFONOMETILGLICINA; Y D) NEUTRALIZAR LA SAL CON UN ACIDO FUERTE PARA PRODUCIR EL PRODUCTO FINAL, N-FOSFONOMETILGLICINA.
ES526547A 1982-10-18 1983-10-18 Procedimiento para la preparacion de n-fosfonometilglicina Expired ES8504830A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US43512282A 1982-10-18 1982-10-18

Publications (2)

Publication Number Publication Date
ES526547A0 ES526547A0 (es) 1985-04-16
ES8504830A1 true ES8504830A1 (es) 1985-04-16

Family

ID=23727074

Family Applications (1)

Application Number Title Priority Date Filing Date
ES526547A Expired ES8504830A1 (es) 1982-10-18 1983-10-18 Procedimiento para la preparacion de n-fosfonometilglicina

Country Status (19)

Country Link
EP (1) EP0107464B1 (es)
JP (1) JPS5989694A (es)
KR (1) KR840006489A (es)
AT (1) ATE17357T1 (es)
AU (1) AU559033B2 (es)
CA (1) CA1205817A (es)
CS (1) CS242887B2 (es)
DD (1) DD215555A5 (es)
DE (1) DE3361801D1 (es)
DK (1) DK467083A (es)
ES (1) ES8504830A1 (es)
FI (1) FI73694C (es)
IL (1) IL69983A (es)
NO (1) NO833774L (es)
NZ (1) NZ205983A (es)
PL (1) PL140413B1 (es)
RO (1) RO87968A (es)
YU (1) YU208983A (es)
ZA (1) ZA837693B (es)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4804499A (en) * 1985-09-23 1989-02-14 Monsanto Company Process for the preparation of N-substituted aminomethylphosphonic acids
US4694082A (en) * 1985-09-23 1987-09-15 Monsanto Company Compound 1,4-diisopropyl-2,5-diketopiperazine

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD123192A1 (es) * 1975-01-16 1976-12-05
US4400330A (en) * 1982-07-29 1983-08-23 Stauffer Chemical Company Method for preparation of N-phosphonomethylglycine

Also Published As

Publication number Publication date
AU559033B2 (en) 1987-02-19
FI73694B (fi) 1987-07-31
JPH0225917B2 (es) 1990-06-06
PL140413B1 (en) 1987-04-30
FI833760A7 (fi) 1984-04-19
KR840006489A (ko) 1984-11-30
NO833774L (no) 1984-04-24
YU208983A (en) 1986-06-30
PL244184A1 (en) 1984-09-24
NZ205983A (en) 1986-10-08
ES526547A0 (es) 1985-04-16
FI833760A0 (fi) 1983-10-17
CS242887B2 (en) 1986-05-15
IL69983A (en) 1987-10-20
CA1205817A (en) 1986-06-10
RO87968B (ro) 1985-12-01
AU2022483A (en) 1984-05-03
JPS5989694A (ja) 1984-05-23
EP0107464A1 (en) 1984-05-02
DK467083A (da) 1984-04-19
FI73694C (fi) 1987-11-09
CS756283A2 (en) 1985-08-15
DD215555A5 (de) 1984-11-14
DK467083D0 (da) 1983-10-11
DE3361801D1 (en) 1986-02-20
ZA837693B (en) 1985-02-27
ATE17357T1 (de) 1986-01-15
EP0107464B1 (en) 1986-01-08
IL69983A0 (en) 1984-01-31
RO87968A (ro) 1985-12-20

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