FI100254B - Menetelmä ja laitteisto vähintäin 80 % ksyloosia sisältävän sokeriseok sen jatkuvaksi valmistamiseksi lignoselluloosasubstraatista - Google Patents

Menetelmä ja laitteisto vähintäin 80 % ksyloosia sisältävän sokeriseok sen jatkuvaksi valmistamiseksi lignoselluloosasubstraatista Download PDF

Info

Publication number: FI100254B
Authority: FI; Finland
Prior art keywords: substrate; hydrolysis; reactor; impregnation; xylose
Prior art date: 1989-12-07

Application number

FI906037A

Other languages

English (en)

Finnish (fi)

Swedish (sv)

Other versions

FI906037A0 (fi

FI906037A7 (fi

Inventor

Daniel Ballerini

Francis Nativel

Original Assignee

Inst Francais Du Petrole

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-12-07

Filing date

1990-12-05

Publication date

1997-10-31

1990-12-05 Application filed by Inst Francais Du Petrole filed Critical Inst Francais Du Petrole

1990-12-05 Publication of FI906037A0 publication Critical patent/FI906037A0/fi

1991-06-08 Publication of FI906037A7 publication Critical patent/FI906037A7/fi

1997-10-31 Application granted granted Critical

1997-10-31 Publication of FI100254B publication Critical patent/FI100254B/fi

Links

239000000758 substrate Substances 0.000 title claims description 90
SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 title claims description 43
235000000346 sugar Nutrition 0.000 title claims description 25
PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 title claims description 22
SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 title claims description 22
238000000034 method Methods 0.000 title claims description 17
239000000203 mixture Substances 0.000 title claims description 12
238000002360 preparation method Methods 0.000 title claims description 5
230000007062 hydrolysis Effects 0.000 claims description 43
238000006460 hydrolysis reaction Methods 0.000 claims description 43
238000005470 impregnation Methods 0.000 claims description 28
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
239000002253 acid Substances 0.000 claims description 14
239000000243 solution Substances 0.000 claims description 14
239000007791 liquid phase Substances 0.000 claims description 12
238000012806 monitoring device Methods 0.000 claims description 10
238000000227 grinding Methods 0.000 claims description 8
238000000926 separation method Methods 0.000 claims description 8
150000008163 sugars Chemical class 0.000 claims description 6
230000002378 acidificating effect Effects 0.000 claims description 5
239000007864 aqueous solution Substances 0.000 claims description 4
238000010924 continuous production Methods 0.000 claims description 2
230000005484 gravity Effects 0.000 claims description 2
238000007789 sealing Methods 0.000 claims description 2
229910001220 stainless steel Inorganic materials 0.000 claims description 2
239000010935 stainless steel Substances 0.000 claims description 2
238000004519 manufacturing process Methods 0.000 claims 4
230000007423 decrease Effects 0.000 claims 1
238000007865 diluting Methods 0.000 claims 1
240000008042 Zea mays Species 0.000 description 14
235000002017 Zea mays subsp mays Nutrition 0.000 description 14
235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 11
235000005822 corn Nutrition 0.000 description 11
229920002488 Hemicellulose Polymers 0.000 description 5
239000001913 cellulose Substances 0.000 description 5
229920002678 cellulose Polymers 0.000 description 5
150000002972 pentoses Chemical class 0.000 description 5
235000013339 cereals Nutrition 0.000 description 4
229920005610 lignin Polymers 0.000 description 4
239000007788 liquid Substances 0.000 description 4
229920006395 saturated elastomer Polymers 0.000 description 4
239000010902 straw Substances 0.000 description 4
239000002023 wood Substances 0.000 description 4
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 3
238000005260 corrosion Methods 0.000 description 3
230000007797 corrosion Effects 0.000 description 3
238000009826 distribution Methods 0.000 description 3
239000008103 glucose Substances 0.000 description 3
235000009973 maize Nutrition 0.000 description 3
238000002156 mixing Methods 0.000 description 3
238000011144 upstream manufacturing Methods 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
238000002474 experimental method Methods 0.000 description 2
238000000855 fermentation Methods 0.000 description 2
230000004151 fermentation Effects 0.000 description 2
239000000706 filtrate Substances 0.000 description 2
239000004615 ingredient Substances 0.000 description 2
238000002347 injection Methods 0.000 description 2
239000007924 injection Substances 0.000 description 2
239000003456 ion exchange resin Substances 0.000 description 2
229920003303 ion-exchange polymer Polymers 0.000 description 2
239000000178 monomer Substances 0.000 description 2
239000000047 product Substances 0.000 description 2
239000007858 starting material Substances 0.000 description 2
235000008733 Citrus aurantifolia Nutrition 0.000 description 1
102000004190 Enzymes Human genes 0.000 description 1
108090000790 Enzymes Proteins 0.000 description 1
229920001503 Glucan Polymers 0.000 description 1
235000011941 Tilia x europaea Nutrition 0.000 description 1
TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 1
230000002745 absorbent Effects 0.000 description 1
239000002250 absorbent Substances 0.000 description 1
125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 1
238000005903 acid hydrolysis reaction Methods 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
239000004480 active ingredient Substances 0.000 description 1
PYMYPHUHKUWMLA-WDCZJNDASA-N arabinose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)C=O PYMYPHUHKUWMLA-WDCZJNDASA-N 0.000 description 1
WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
230000002051 biphasic effect Effects 0.000 description 1
238000005422 blasting Methods 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
238000011437 continuous method Methods 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
238000010586 diagram Methods 0.000 description 1
235000019621 digestibility Nutrition 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000004880 explosion Methods 0.000 description 1
239000002360 explosive Substances 0.000 description 1
238000000605 extraction Methods 0.000 description 1
238000001914 filtration Methods 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
239000004571 lime Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
239000011707 mineral Substances 0.000 description 1
238000012544 monitoring process Methods 0.000 description 1
235000021096 natural sweeteners Nutrition 0.000 description 1
229920000642 polymer Polymers 0.000 description 1
238000006116 polymerization reaction Methods 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
238000011084 recovery Methods 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
239000011347 resin Substances 0.000 description 1
229920005989 resin Polymers 0.000 description 1
230000035945 sensitivity Effects 0.000 description 1
239000007787 solid Substances 0.000 description 1
238000005507 spraying Methods 0.000 description 1
-1 steam hydrolysis Substances 0.000 description 1
239000000126 substance Substances 0.000 description 1
229920001864 tannin Polymers 0.000 description 1
239000001648 tannin Substances 0.000 description 1
235000018553 tannin Nutrition 0.000 description 1
238000005406 washing Methods 0.000 description 1
229920001221 xylan Polymers 0.000 description 1
150000004823 xylans Chemical class 0.000 description 1
239000000811 xylitol Substances 0.000 description 1
235000010447 xylitol Nutrition 0.000 description 1
HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
229960002675 xylitol Drugs 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Biochemistry (AREA)
Organic Chemistry (AREA)
Saccharide Compounds (AREA)
Seasonings (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)
Processing Of Solid Wastes (AREA)

FI906037A 1989-12-07 1990-12-05 Menetelmä ja laitteisto vähintäin 80 % ksyloosia sisältävän sokeriseok sen jatkuvaksi valmistamiseksi lignoselluloosasubstraatista FI100254B (fi)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
FR8916321A FR2655661B1 (fr)	1989-12-07	1989-12-07	Procede et unite de production en continu d'un melange de sucres contenant au moins 80% de xylose a partir d'un substrat lignocellulosique.
FR8916321		1989-12-07

Publications (3)

Publication Number	Publication Date
FI906037A0 FI906037A0 (fi)	1990-12-05
FI906037A7 FI906037A7 (fi)	1991-06-08
FI100254B true FI100254B (fi)	1997-10-31

Family

ID=9388341

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
FI906037A FI100254B (fi)	1989-12-07	1990-12-05	Menetelmä ja laitteisto vähintäin 80 % ksyloosia sisältävän sokeriseok sen jatkuvaksi valmistamiseksi lignoselluloosasubstraatista

Country Status (5)

Country	Link
EP (1)	EP0432015B1 (de)
DE (1)	DE69013652T2 (de)
ES (1)	ES2066173T3 (de)
FI (1)	FI100254B (de)
FR (1)	FR2655661B1 (de)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN1058996C (zh) *	1996-05-14	2000-11-29	安徽省科苑应用技术开发(集团)股份有限公司	由玉米芯提取木糖的改进方法
US6022419A (en) *	1996-09-30	2000-02-08	Midwest Research Institute	Hydrolysis and fractionation of lignocellulosic biomass
FR3027821B1 (fr)	2014-10-31	2018-11-16	Centralesupelec	Procede de purification d'oses.
JP6774494B2 (ja)	2016-02-19	2020-10-21	インターコンチネンタルグレートブランズエルエルシー	バイオマス源から複数の有用なストリームを形成するためのプロセス

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2413306B2 (de) *	1973-05-04	1976-09-30	Gebrüder Sulzer AG, Winterthur (Schweiz)	Verfahren zum herstellen von xyloseloesung
CH585794A5 (de) *	1974-12-03	1977-03-15	Sulzer Ag
US4136207A (en) *	1977-01-24	1979-01-23	Stake Technology Ltd.	Method of treating lignocellulose materials to produce ruminant feed
US4350766A (en) *	1980-08-01	1982-09-21	Purdue Research Foundation	Pentose syrup production from hemicellulose
FR2580669B1 (fr) *	1985-04-18	1987-09-18	Inst Francais Du Petrole	Procede de conversion de substrats lignocellulosiques en pentoses

1989
- 1989-12-07 FR FR8916321A patent/FR2655661B1/fr not_active Expired - Lifetime
1990
- 1990-11-28 ES ES90403374T patent/ES2066173T3/es not_active Expired - Lifetime
- 1990-11-28 DE DE69013652T patent/DE69013652T2/de not_active Expired - Lifetime
- 1990-11-28 EP EP90403374A patent/EP0432015B1/de not_active Expired - Lifetime
- 1990-12-05 FI FI906037A patent/FI100254B/fi active IP Right Grant

Also Published As

Publication number	Publication date
EP0432015A1 (de)	1991-06-12
DE69013652D1 (de)	1994-12-01
FR2655661A1 (fr)	1991-06-14
ES2066173T3 (es)	1995-03-01
FI906037A0 (fi)	1990-12-05
FI906037A7 (fi)	1991-06-08
FR2655661B1 (fr)	1994-06-03
DE69013652T2 (de)	1995-03-02
EP0432015B1 (de)	1994-10-26

Legal Events

Date	Code	Title	Description
2004-08-31	FG	Patent granted	Owner name: INSTITUT FRANCAIS DU PETROLE

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US10557105B1 (en)	2020-02-11	Extraction systems and methods
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Bonn et al.	1983	Hydrothermolysis—a new process for the utilization of biomass
US5756098A (en)	1998-05-26	Methods for the extraction of phytochemicals from fibrous plants in the absence of solvent
US4409032A (en)	1983-10-11	Organosolv delignification and saccharification process for lignocellulosic plant materials
US9624449B2 (en)	2017-04-18	Biorefinery process for extraction, separation and recovery of fermentable saccharides, other useful compounds, and yield of improved lignocellulosic material from plant biomass
CA1183788A (en)	1985-03-12	Process and installation for obtaining ethanol by the continuous acid hydrolysis of cellulosic materials
EP0649602A2 (de)	1995-04-26	Verfahren zur Herstellung vom löslichem Rühenfaser
CN102084055A (zh)	2011-06-01	生物质的处理方法
US20130210102A1 (en)	2013-08-15	Methods for detoxifying a lignocellulosic hydrolysate
BR112021004447A2 (pt)	2021-05-25	método de produção de etanol
US11420992B2 (en)	2022-08-23	Methods of recovering lignin and other products from biomass
WO2013041298A1 (en)	2013-03-28	Device for heating a feedstock
RS58648B1 (sr)	2019-05-31	Postupak za dobijanje bioproizvoda
CN1284586A (zh)	2001-02-21	生物基料纤维材料的处理方法
EP0432015B1 (de)	1994-10-26	Verfahren und Einrichtung zur Herstellung einer zumindest 80% Xylose enthaltende Zuckermischung aus einem lignocellulosischen Substrat
FI100255B (fi)	1997-10-31	Lignoselluloosasubstraatin jatkuvaan ja paineenalaiseen kyllästykseen ja hydrolyysiin käytettävä reaktori sekä menetelmä ja laitteisto soker iseoksen valmistamiseksi ksyloosista
CA2866826C (en)	2020-07-28	Process for the production of organic compounds from plant species
US10337075B2 (en)	2019-07-02	Process and apparatus for treatment of biomass
Funk	1975	Recovery of pentoses and hexoses from wood and other material containing hemicellulose and further processing of C5-and C6-components
Dunlap Jr	1969	Proteins from waste cellulose by chemical-microbial processing
Rolz et al.	1987	Effects of some physical and chemical pretreatments on the composition, enzymatic hydrolysis and digestibility of lignocellulosic sugar cane residue
RU2086151C1 (ru)	1997-08-10	Способ получения пищевой добавки из растительного сырья
Harris	1947	Wood-sugar molasses from wood waste