FI104383B - Förfarande för beläggning av insidan av en anläggning - Google Patents

Förfarande för beläggning av insidan av en anläggning Download PDF

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Publication number
FI104383B
FI104383B FI974472A FI974472A FI104383B FI 104383 B FI104383 B FI 104383B FI 974472 A FI974472 A FI 974472A FI 974472 A FI974472 A FI 974472A FI 104383 B FI104383 B FI 104383B
Authority
FI
Finland
Prior art keywords
coating
coated
reagent
gas
volume
Prior art date
Application number
FI974472A
Other languages
English (en)
Finnish (fi)
Other versions
FI974472A0 (fi
FI974472L (sv
Inventor
Tuomo Suntola
Markku Leskelae
Mikko Ritala
Original Assignee
Fortum Oil & Gas Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fortum Oil & Gas Oy filed Critical Fortum Oil & Gas Oy
Priority to FI974472A priority Critical patent/FI104383B/sv
Publication of FI974472A0 publication Critical patent/FI974472A0/fi
Priority to PCT/FI1998/000955 priority patent/WO1999029924A1/en
Priority to US09/581,020 priority patent/US6416577B1/en
Priority to AU14898/99A priority patent/AU1489899A/en
Publication of FI974472L publication Critical patent/FI974472L/sv
Application granted granted Critical
Publication of FI104383B publication Critical patent/FI104383B/sv

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Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
    • C23C16/45523Pulsed gas flow or change of composition over time
    • C23C16/45525Atomic layer deposition [ALD]
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/04Coating on selected surface areas, e.g. using masks
    • C23C16/045Coating cavities or hollow spaces, e.g. interior of tubes; Infiltration of porous substrates
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/46Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for heating the substrate
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B35/00Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T117/00Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
    • Y10T117/10Apparatus

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mechanical Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Vapour Deposition (AREA)

Claims (14)

1. Förfarande för beläggning av innerytoma av en anläggning med ett materialskikt, kännetecknat avatt 5 - ätminstone en del av det inre rum som avgränsas av anläggningens innerytor tillsluts, - ängfaspulser av minst tvä olika reaktanter altemerande och upprepande inmatas i nämnda slutna inre rum, och - ett materialskikt utbildas pä de inre ytoma enligt ALE-tekniken genom att 10 utsätta ytoma för altemerande ytreaktioner orsakade av reaktantema.
2. Förfarande enligt krav 1, kännetecknat av att man som reaktanter använder flyktiga föreningar, säsom oorganiska föreningar av metaller, metallorganiska föreningar eller rena metaller, vatten, väteperoxid, syre, ozon, alkoholer, ammoniak eller organiska 15 föreningar av kväve.
3. Förfarande enligt krav 1 eller 2, kännetecknat av en kombination av följande steg: a. den av innerytoma (2; 13) begränsade volymen töms medelst en pump (3; 13) 20 pä gaser som möjligen stör beläggningsreaktionema, b. ytoma (2; 12) bringas i en temperatur som förutsätts av ytreaktionema använda i beläggningsprocessen, c. ett första reagens (A) leds in i den av ytoma (2; 12) begränsade volymen * * « · :\ ätminstone i en sädan mängd, att det räcker tili för att fylla ytbindningsplatsema • · · .•:\25 pä ytoma, d. ett eventuellt överskott av det första reagenset (A) avlägsnas frän nämda :Ts volym, e. ett andra reagens (B) leds in i den av ytoma begränsade volymen ätminstone i : ·. en sädan mängd, att det räcker tili för att fylla ytbindningsplatsema pä ytoma 1 : ":30 (2; 12), ! '1' f. ett eventuellt överskott av det andra reagenset avlägsnas frän nämnda volym, • · · • · • · · • Φ I • i 13 104383 och g. stegen c - f upprepas cykliskt i en sädan mängd som behövs för att beläggning-en erhäller önskad tjocklek. 5
4. Förfarande enligt krav 3, kännetecknat av att den för beläggning avsedda ytan bringas i en temperatur som förutsätts av ytreaktionema använda i beläggningspro-cessen medelst värmare anordnade utanför stycket.
5. Förfarande enligt krav 3, kännetecknat av att den för beläggning avsedda 10 ytan bringas i en temperatur som förutsätts av ytreaktionema använda i beläggningspro-cessen genom ledning av värmeöverföringsvätska eller gas i det utrymme som begränsas av den för beläggning avsedda ytan (2; 12) före beläggningsstegen.
6. Förfarande enligt krav 5, kännetecknat av att man leder värmeöverförings- 15 vätska eller gas i det utrymme som begränsas av den för beläggning avsedda ytan (2; 12) ett flertal gänger efler den cykliska perioden som utgörs av stegen c - f.
7. Förfarande enligt nägot av kraven 3-6, kännetecknat av att avlägsnandet av överskotten pä reagensema (A, B) vid stegen d och f effektiveras medelst en skydds- 20 gasströmning.
... 8. Förfarande enligt nägot av kraven 3-7, kännetecknat av att atminstone ett • · · · .:. reagens tili utöver det första och det andra reagenset inmatas i volymen begränsad av • ·« t |\ den för beläggning avsedda ytan (2; 12) för säkerställande och/eller kompletterande av 25 ytreaktionema ästadkomna av det första och det andra reagenset. :T:
9. Förfarande enligt nägot av de föregäende kraven, kännetecknat av att ett inre ·»» ' ' ' rum eller ett gasutrymme, som begränsas av de för beläggning avsedda innerytoma och som tillsluts medelst ventilmekanismer (6, 7; 16, 17, 19), utformas i anläggningen. 30 .'.'.
10. Förfarande enligt krav 9, kännetecknat av att atminstone en ventilmekanism f I I w ’ • « • · • · » « 14 104383 (6, 7; 16, 17) används för inmatningen av reaktantema, varvid ätminstone tvä reaktant-källor (A, B) förenas tili ifrägavarande ventilmekanism.
11. Förfarande enligt krav 9 eller 10, kännetecknat avatt ätminstone en 5 ventilmekanism (18) används för avlägsnande av gasöverskottet.
12. Förfarande enligt nägot av de föregäende kraven, kännetecknat avatt innerytan av processanläggningen, säsom rörsystemet eller behällaren (1, 11), förses med en beläggning. 10
13. Förfarande enligt nägot av kraven 1-12, kännetecknat avatt korrosions-eller belastningshällfasthetsförmägan eller optiska eller elektriska egenskaper hos innerytan av anläggningen förbättras medelst beläggningen, eller att friktionen minskas. 15
14. Förfarande enligt nägot av de föregäende kraven, kännetecknat av att ett oxid-, nitrid- och/eller kalkogenidskikt utbildas pä innerytan. • · · • · · · • · · • « · · • « • 9 • 99 • « 1 f • 99 • 9 n • · · • · · · 1 I < · · 0 9 9
FI974472A 1997-12-09 1997-12-09 Förfarande för beläggning av insidan av en anläggning FI104383B (sv)

Priority Applications (4)

Application Number Priority Date Filing Date Title
FI974472A FI104383B (sv) 1997-12-09 1997-12-09 Förfarande för beläggning av insidan av en anläggning
PCT/FI1998/000955 WO1999029924A1 (en) 1997-12-09 1998-12-09 Method for coating inner surfaces of equipment
US09/581,020 US6416577B1 (en) 1997-12-09 1998-12-09 Method for coating inner surfaces of equipment
AU14898/99A AU1489899A (en) 1997-12-09 1998-12-09 Method for coating inner surfaces of equipment

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI974472A FI104383B (sv) 1997-12-09 1997-12-09 Förfarande för beläggning av insidan av en anläggning
FI974472 1997-12-09

Publications (3)

Publication Number Publication Date
FI974472A0 FI974472A0 (fi) 1997-12-09
FI974472L FI974472L (sv) 1999-06-10
FI104383B true FI104383B (sv) 2000-01-14

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
FI974472A FI104383B (sv) 1997-12-09 1997-12-09 Förfarande för beläggning av insidan av en anläggning

Country Status (4)

Country Link
US (1) US6416577B1 (sv)
AU (1) AU1489899A (sv)
FI (1) FI104383B (sv)
WO (1) WO1999029924A1 (sv)

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