FI112363B - Menetelmä peretikkahapon valmistamiseksi - Google Patents

Menetelmä peretikkahapon valmistamiseksi Download PDF

Info

Publication number: FI112363B
Authority: FI; Finland
Prior art keywords: acid; weight; reaction medium; att; peracetic acid
Prior art date: 2001-04-04

Application number

FI20010706A

Other languages

English (en)

Finnish (fi)

Swedish (sv)

Other versions

FI20010706L (fi

FI20010706A0 (fi

Inventor

Eva-Liisa Mustonen

Arto Pukkinen

Seppo Pohjanvesi

Reino Lehtinen

Original Assignee

Kemira Chemicals Oy

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2001-04-04

Filing date

2001-04-04

Publication date

2003-11-28

2001-04-04 Application filed by Kemira Chemicals Oy filed Critical Kemira Chemicals Oy

2001-04-04 Publication of FI20010706A0 publication Critical patent/FI20010706A0/fi

2001-04-04 Priority to FI20010706A priority Critical patent/FI112363B/fi

2002-04-03 Priority to JP2002101289A priority patent/JP4268783B2/ja

2002-04-03 Priority to CA2380163A priority patent/CA2380163C/en

2002-04-03 Priority to US10/114,295 priority patent/US6677478B2/en

2002-04-04 Priority to BRPI0201118-2A priority patent/BR0201118B1/pt

2002-04-04 Priority to ES02396043T priority patent/ES2383748T3/es

2002-04-04 Priority to AT02396043T priority patent/ATE551321T1/de

2002-04-04 Priority to EP02396043A priority patent/EP1247801B1/de

2002-04-04 Priority to KR1020020018626A priority patent/KR100902677B1/ko

2002-10-05 Publication of FI20010706L publication Critical patent/FI20010706L/fi

2003-11-28 Application granted granted Critical

2003-11-28 Publication of FI112363B publication Critical patent/FI112363B/fi

Links

KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 title claims abstract description 122
238000000034 method Methods 0.000 title claims description 33
238000002360 preparation method Methods 0.000 title description 14
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 111
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 64
239000012429 reaction media Substances 0.000 claims abstract description 43
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
239000003377 acid catalyst Substances 0.000 claims abstract description 25
238000004821 distillation Methods 0.000 claims abstract description 18
238000004519 manufacturing process Methods 0.000 claims abstract description 14
239000012141 concentrate Substances 0.000 claims abstract description 7
239000000463 material Substances 0.000 claims abstract description 5
239000012431 aqueous reaction media Substances 0.000 claims abstract 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 64
239000000203 mixture Substances 0.000 claims description 26
238000006243 chemical reaction Methods 0.000 claims description 12
150000007522 mineralic acids Chemical group 0.000 claims description 8
239000002253 acid Substances 0.000 claims description 7
150000002978 peroxides Chemical class 0.000 claims description 6
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
150000007513 acids Chemical class 0.000 claims description 4
244000005700 microbiome Species 0.000 claims description 4
229910052739 hydrogen Inorganic materials 0.000 claims description 3
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
235000008504 concentrate Nutrition 0.000 claims 4
239000006188 syrup Substances 0.000 claims 2
235000020357 syrup Nutrition 0.000 claims 2
239000003638 chemical reducing agent Substances 0.000 claims 1
239000001257 hydrogen Substances 0.000 claims 1
125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
125000000864 peroxy group Chemical group O(O*)* 0.000 claims 1
238000009736 wetting Methods 0.000 claims 1
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 abstract 2
239000000047 product Substances 0.000 description 47
SCKXCAADGDQQCS-UHFFFAOYSA-N Performic acid Chemical compound OOC=O SCKXCAADGDQQCS-UHFFFAOYSA-N 0.000 description 16
239000012535 impurity Substances 0.000 description 14
239000000243 solution Substances 0.000 description 13
239000007864 aqueous solution Substances 0.000 description 5
239000011541 reaction mixture Substances 0.000 description 5
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
239000003054 catalyst Substances 0.000 description 3
239000002994 raw material Substances 0.000 description 3
239000007858 starting material Substances 0.000 description 3
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
238000004458 analytical method Methods 0.000 description 2
150000001732 carboxylic acid derivatives Chemical class 0.000 description 2
229910052804 chromium Inorganic materials 0.000 description 2
239000011651 chromium Substances 0.000 description 2
XLJMAIOERFSOGZ-UHFFFAOYSA-N cyanic acid Chemical compound OC#N XLJMAIOERFSOGZ-UHFFFAOYSA-N 0.000 description 2
WJJMNDUMQPNECX-UHFFFAOYSA-N dipicolinic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=N1 WJJMNDUMQPNECX-UHFFFAOYSA-N 0.000 description 2
238000002474 experimental method Methods 0.000 description 2
229910052742 iron Inorganic materials 0.000 description 2
229910052751 metal Inorganic materials 0.000 description 2
239000002184 metal Substances 0.000 description 2
239000003960 organic solvent Substances 0.000 description 2
239000003381 stabilizer Substances 0.000 description 2
238000003860 storage Methods 0.000 description 2
239000012808 vapor phase Substances 0.000 description 2
239000002699 waste material Substances 0.000 description 2
RPAJSBKBKSSMLJ-DFWYDOINSA-N (2s)-2-aminopentanedioic acid;hydrochloride Chemical class Cl.OC(=O)[C@@H](N)CCC(O)=O RPAJSBKBKSSMLJ-DFWYDOINSA-N 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
239000000498 cooling water Substances 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
230000007423 decrease Effects 0.000 description 1
238000006731 degradation reaction Methods 0.000 description 1
238000004332 deodorization Methods 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
239000011707 mineral Substances 0.000 description 1
238000002156 mixing Methods 0.000 description 1
FWFGVMYFCODZRD-UHFFFAOYSA-N oxidanium;hydrogen sulfate Chemical compound O.OS(O)(=O)=O FWFGVMYFCODZRD-UHFFFAOYSA-N 0.000 description 1
238000012856 packing Methods 0.000 description 1
-1 peracetic acid Chemical compound 0.000 description 1
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
239000010452 phosphate Substances 0.000 description 1
CZPZWMPYEINMCF-UHFFFAOYSA-N propaneperoxoic acid Chemical compound CCC(=O)OO CZPZWMPYEINMCF-UHFFFAOYSA-N 0.000 description 1
238000000926 separation method Methods 0.000 description 1
238000004659 sterilization and disinfection Methods 0.000 description 1
239000011550 stock solution Substances 0.000 description 1
238000012360 testing method Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/24—Peroxy compounds the —O—O— group being bound between a >C=O group and hydrogen, i.e. peroxy acids
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/24—Peroxy compounds the —O—O— group being bound between a >C=O group and hydrogen, i.e. peroxy acids
- C07C409/26—Peracetic acid

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Agricultural Chemicals And Associated Chemicals (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

FI20010706A 2001-04-04 2001-04-04 Menetelmä peretikkahapon valmistamiseksi FI112363B (fi)

Priority Applications (9)

Application Number	Priority Date	Filing Date	Title
FI20010706A FI112363B (fi)	2001-04-04	2001-04-04	Menetelmä peretikkahapon valmistamiseksi
JP2002101289A JP4268783B2 (ja)	2001-04-04	2002-04-03	過カルボン酸の製造方法
CA2380163A CA2380163C (en)	2001-04-04	2002-04-03	Process for the production of percarboxylic acid
US10/114,295 US6677478B2 (en)	2001-04-04	2002-04-03	Process for the production of percarboxylic acid
BRPI0201118-2A BR0201118B1 (pt)	2001-04-04	2002-04-04	processo para produÇço de Ácido percarboxÍilico.
ES02396043T ES2383748T3 (es)	2001-04-04	2002-04-04	Procedimiento de producción de ácido percaboxilico
AT02396043T ATE551321T1 (de)	2001-04-04	2002-04-04	Verfahren zur herstellung von percarbonsäuren
EP02396043A EP1247801B1 (de)	2001-04-04	2002-04-04	Verfahren zur Herstellung von Percarbonsäuren
KR1020020018626A KR100902677B1 (ko)	2001-04-04	2002-04-04	과카르복실산의 생산 방법

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
FI20010706A FI112363B (fi)	2001-04-04	2001-04-04	Menetelmä peretikkahapon valmistamiseksi
FI20010706		2001-04-04

Publications (3)

Publication Number	Publication Date
FI20010706A0 FI20010706A0 (fi)	2001-04-04
FI20010706L FI20010706L (fi)	2002-10-05
FI112363B true FI112363B (fi)	2003-11-28

Family

ID=8560921

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
FI20010706A FI112363B (fi)	2001-04-04	2001-04-04	Menetelmä peretikkahapon valmistamiseksi

Country Status (9)

Country	Link
US (1)	US6677478B2 (de)
EP (1)	EP1247801B1 (de)
JP (1)	JP4268783B2 (de)
KR (1)	KR100902677B1 (de)
AT (1)	ATE551321T1 (de)
BR (1)	BR0201118B1 (de)
CA (1)	CA2380163C (de)
ES (1)	ES2383748T3 (de)
FI (1)	FI112363B (de)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FI116466B (fi) *	2001-10-30	2005-11-30	Kemira Oyj	Menetelmä perkarboksyylihapon valmistamiseksi
US7012154B2 (en) *	2004-07-28	2006-03-14	Peragen Systems, Llc	Continuous process for on-site and on-demand production of aqueous peracteic acid
KR100722635B1 (ko)	2005-09-27	2007-05-28	삼성전기주식회사	와이어 본딩 패드면과 볼패드면의 회로층이 다른 두께를갖는 반도체 패키지 기판 및 그 제조방법
US7547421B2 (en) *	2006-10-18	2009-06-16	Ecolab Inc.	Apparatus and method for making a peroxycarboxylic acid
CN101496702B (zh) *	2008-01-30	2011-03-30	德昌电机(深圳)有限公司	自动翻盖装置及具有所述自动翻盖装置的组合
WO2009099925A2 (en) *	2008-02-04	2009-08-13	Fmc Corporation	Rapid dilution of peracid solutions to equilibrated solutions
RU2425030C1 (ru) *	2010-02-09	2011-07-27	Государственное образовательное учреждение высшего профессионального образования Уральский государственный лесотехнический университет	Способ получения раствора пероксикислот для делигнификации и отбеливания
WO2014072143A1 (de) *	2012-11-08	2014-05-15	Evonik Industries Ag	Verfahren zur herstellung von gleichgewichtsperessigsäure und mit dem verfahren erhältliche gleichgewichtsperessigsäure
JP6728382B2 (ja)	2015-12-16	2020-07-22	エコラブユーエスエイインク	膜濾過浄化のためのペルオキシギ酸組成物
CN105503685B (zh) *	2016-01-19	2017-10-13	黎明化工研究设计院有限责任公司	一种制备无水过氧乙酸溶液的方法及其装置
EP3442334B9 (de)	2016-04-15	2023-08-02	Ecolab USA Inc.	Verhinderung von biofilmen in industriellen co2-gaswäschern mit perameisensäure
WO2018111341A1 (en)	2016-12-15	2018-06-21	Ecolab Usa Inc.	Peroxyformic acid compositions for membrane filtration cleaning in energy services
EP4211110A4 (de) *	2020-09-10	2024-05-15	Symbient Environmental Technologies	Verfahren und vorrichtung zur herstellung von perameisensäure

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
BE630363A (de)	1962-04-04
FR1432773A (fr)	1965-02-11	1966-03-25	Melle Usines Sa	Procédé de fabrication d'acides organiques percarboxyliques
DE3720562A1 (de)	1987-06-22	1989-01-05	Degussa	Verfahren zur herstellung von peressigsaeure
SE8903773L (sv) *	1989-11-10	1991-05-11	Eka Nobel Ab	Peraettiksyrakomposition
JP2871124B2 (ja) *	1991-01-23	1999-03-17	日本パーオキサイド株式会社	安全な過酢酸組成物
JPH08183766A (ja) *	1994-12-28	1996-07-16	Mitsubishi Gas Chem Co Inc	過酢酸水溶液の製造方法
SE9600347L (sv)	1996-01-31	1997-08-01	Eka Chemicals Ab	Sätt att framställa kemisk produkt
DE19752801A1 (de) *	1997-11-28	1999-07-01	Degussa	Verfahren zur chemothermischen Wäschedesinfektion und Mittel zu seiner Durchführung
EP1004576A1 (de)	1998-11-23	2000-05-31	SOLVAY (Société Anonyme)	Verfahren zur Herstellung von Peressigsäure
JP4412428B2 (ja) *	1999-04-19	2010-02-10	三菱瓦斯化学株式会社	過酢酸組成物

2001
- 2001-04-04 FI FI20010706A patent/FI112363B/fi not_active IP Right Cessation
2002
- 2002-04-03 JP JP2002101289A patent/JP4268783B2/ja not_active Expired - Fee Related
- 2002-04-03 US US10/114,295 patent/US6677478B2/en not_active Expired - Lifetime
- 2002-04-03 CA CA2380163A patent/CA2380163C/en not_active Expired - Lifetime
- 2002-04-04 EP EP02396043A patent/EP1247801B1/de not_active Expired - Lifetime
- 2002-04-04 BR BRPI0201118-2A patent/BR0201118B1/pt active IP Right Grant
- 2002-04-04 ES ES02396043T patent/ES2383748T3/es not_active Expired - Lifetime
- 2002-04-04 KR KR1020020018626A patent/KR100902677B1/ko not_active Expired - Fee Related
- 2002-04-04 AT AT02396043T patent/ATE551321T1/de active

Also Published As

Publication number	Publication date
ATE551321T1 (de)	2012-04-15
EP1247801B1 (de)	2012-03-28
JP2003012640A (ja)	2003-01-15
ES2383748T3 (es)	2012-06-26
KR100902677B1 (ko)	2009-06-15
BR0201118A (pt)	2003-05-27
CA2380163C (en)	2011-10-11
US6677478B2 (en)	2004-01-13
BR0201118B1 (pt)	2013-01-22
FI20010706L (fi)	2002-10-05
EP1247801A1 (de)	2002-10-09
US20020177732A1 (en)	2002-11-28
FI20010706A0 (fi)	2001-04-04
CA2380163A1 (en)	2002-10-04
JP4268783B2 (ja)	2009-05-27
KR20020079492A (ko)	2002-10-19

Legal Events

Date	Code	Title	Description
2021-05-27	MA	Patent expired

Publication	Publication Date	Title
FI112363B (fi)	2003-11-28	Menetelmä peretikkahapon valmistamiseksi
EP3630719B1 (de)	2023-11-22	Verfahren zur herstellung von alkansulfonsäuren
KR101477938B1 (ko)	2014-12-30	과산화수소 수용액의 농축 방법
ES2440468T3 (es)	2014-01-29	Procedimiento para la eliminación de acetol a partir de fenol
AU616095B2 (en)	1991-10-17	Recovery of hydrogen peroxide
KR20000049104A (ko)	2000-07-25	폐황산의 농축 방법
US7217849B2 (en)	2007-05-15	Method for the preparation of n-propyl bromide
JPH03223267A (ja)	1991-10-02	エピクロルヒドリンの製造方法
EP0789016B2 (de)	2001-06-13	Verfahren zur Herstellung von Peressigsäure
KR860000134B1 (ko)	1986-02-26	ε-카프로락톤의 제조방법
EP1004576A1 (de)	2000-05-31	Verfahren zur Herstellung von Peressigsäure
EP2024314B1 (de)	2011-08-10	Trennung und/oder wiederherstellung von propylbromid
KR101380032B1 (ko)	2014-04-01	1,2-디클로로에탄 정제 및 연관된 수산화나트륨액 증발농축을 위한 증류탑 가동 방법
US5043481A (en)	1991-08-27	Cyclohexane oxidation
EP1016657B1 (de)	2002-01-30	Verfahren zur Herstellung von Peressigsäure
KR20000053661A (ko)	2000-08-25	하이드록시아세톤-함유 페놀로부터 하이드록시아세톤을제거하는 방법
JPS6127938A (ja)	1986-02-07	ソルビン酸の製法
CA2292299C (en)	2004-09-07	Method for producing peracetic acid
JP2913123B2 (ja)	1999-06-28	変色のないビスフェノールａの分離方法
EP0551929A1 (de)	1993-07-21	Herstellung von Wasserstoffperoxid
EP1932822A1 (de)	2008-06-18	Entwässerungsverfahren
EP1773798A1 (de)	2007-04-18	Rückgewinnung optisch aktiver epoxyalkohole