FI20090090L - Menetelmä litiumbikarbonaatin puhdistamiseksi - Google Patents

Menetelmä litiumbikarbonaatin puhdistamiseksi Download PDF

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Publication number
FI20090090L
FI20090090L FI20090090A FI20090090A FI20090090L FI 20090090 L FI20090090 L FI 20090090L FI 20090090 A FI20090090 A FI 20090090A FI 20090090 A FI20090090 A FI 20090090A FI 20090090 L FI20090090 L FI 20090090L
Authority
FI
Finland
Prior art keywords
lithium bicarbonate
purifying lithium
purifying
bicarbonate
lithium
Prior art date
Application number
FI20090090A
Other languages
English (en)
Swedish (sv)
Other versions
FI20090090A0 (fi
FI121785B (fi
Inventor
Marika Tiihonen
Original Assignee
Outotec Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outotec Oyj filed Critical Outotec Oyj
Publication of FI20090090A0 publication Critical patent/FI20090090A0/fi
Priority to FI20090090A priority Critical patent/FI121785B/fi
Priority to CN201080011083.4A priority patent/CN102348817B/zh
Priority to ES201150014A priority patent/ES2379423B1/es
Priority to CA2755123A priority patent/CA2755123C/en
Priority to PT2010050158A priority patent/PT2010103173W/pt
Priority to AU2010223194A priority patent/AU2010223194B2/en
Priority to US13/255,099 priority patent/US9284626B2/en
Priority to BRPI1009523-3A priority patent/BRPI1009523B1/pt
Priority to PCT/FI2010/050158 priority patent/WO2010103173A1/en
Priority to EA201190148A priority patent/EA019279B9/ru
Priority to ARP100100727A priority patent/AR075734A1/es
Publication of FI20090090L publication Critical patent/FI20090090L/fi
Application granted granted Critical
Publication of FI121785B publication Critical patent/FI121785B/fi
Priority to CL2011002230A priority patent/CL2011002230A1/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
    • B01D15/361—Ion-exchange
    • B01D15/362—Cation-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04—Processes using organic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04—Processes using organic exchangers
    • B01J39/07—Processes using organic exchangers in the weakly acidic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B01J49/53—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for cationic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/60—Cleaning or rinsing ion-exchange beds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/08—Carbonates; Bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Removal Of Specific Substances (AREA)
FI20090090A 2009-03-11 2009-03-11 Menetelmä litiumbikarbonaatin puhdistamiseksi FI121785B (fi)

Priority Applications (12)

Application Number Priority Date Filing Date Title
FI20090090A FI121785B (fi) 2009-03-11 2009-03-11 Menetelmä litiumbikarbonaatin puhdistamiseksi
US13/255,099 US9284626B2 (en) 2009-03-11 2010-03-01 Method for purifying lithium bicarbonate
PCT/FI2010/050158 WO2010103173A1 (en) 2009-03-11 2010-03-01 Method for purifying lithium bicarbonate
CA2755123A CA2755123C (en) 2009-03-11 2010-03-01 Method for purifying lithium bicarbonate
PT2010050158A PT2010103173W (pt) 2009-03-11 2010-03-01 Processo para a purificação bicarbonato de lítio
AU2010223194A AU2010223194B2 (en) 2009-03-11 2010-03-01 Method for purifying lithium bicarbonate
CN201080011083.4A CN102348817B (zh) 2009-03-11 2010-03-01 提纯碳酸氢锂的方法
BRPI1009523-3A BRPI1009523B1 (pt) 2009-03-11 2010-03-01 Method for the purification of lithium bicarbonate.
ES201150014A ES2379423B1 (es) 2009-03-11 2010-03-01 Método para purificar bicarbonato de litio.
EA201190148A EA019279B9 (ru) 2009-03-11 2010-03-01 Способ очистки бикарбоната лития
ARP100100727A AR075734A1 (es) 2009-03-11 2010-03-10 Metodo para purificar bicarbonato de litio
CL2011002230A CL2011002230A1 (es) 2009-03-11 2011-09-09 Metodo para purificar bicarbonato de litio impuro mediante una resina de intercambio ionico en donde ademas se incluye la regeneracion de metales enlazados a la resina que comprende lavar la resina con agua, eluir con solucion acida, lavado y neutralizacion con hidroxido de sodio.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI20090090 2009-03-11
FI20090090A FI121785B (fi) 2009-03-11 2009-03-11 Menetelmä litiumbikarbonaatin puhdistamiseksi

Publications (3)

Publication Number Publication Date
FI20090090A0 FI20090090A0 (fi) 2009-03-11
FI20090090L true FI20090090L (fi) 2010-09-12
FI121785B FI121785B (fi) 2011-04-15

Family

ID=40510167

Family Applications (1)

Application Number Title Priority Date Filing Date
FI20090090A FI121785B (fi) 2009-03-11 2009-03-11 Menetelmä litiumbikarbonaatin puhdistamiseksi

Country Status (12)

Country Link
US (1) US9284626B2 (fi)
CN (1) CN102348817B (fi)
AR (1) AR075734A1 (fi)
AU (1) AU2010223194B2 (fi)
BR (1) BRPI1009523B1 (fi)
CA (1) CA2755123C (fi)
CL (1) CL2011002230A1 (fi)
EA (1) EA019279B9 (fi)
ES (1) ES2379423B1 (fi)
FI (1) FI121785B (fi)
PT (1) PT2010103173W (fi)
WO (1) WO2010103173A1 (fi)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8936770B2 (en) 2010-01-22 2015-01-20 Molycorp Minerals, Llc Hydrometallurgical process and method for recovering metals
CN103958412A (zh) 2011-09-15 2014-07-30 奥若可博有限公司 用于从浓锂卤水制备碳酸锂的方法
EA201491632A1 (ru) 2012-03-19 2015-03-31 Оутотек (Финлэнд) Ой Способ извлечения карбоната лития
EP2841623B1 (en) 2012-04-23 2020-10-28 Nemaska Lithium Inc. Processes for preparing lithium hydroxide
RS57299B1 (sr) 2012-05-30 2018-08-31 Nemaska Lithium Inc Postupci za dobijanje litijum karbonata
HRP20210506T1 (hr) 2013-03-15 2021-06-11 Nemaska Lithium Inc. Postupak za pripremu litijevog hidroksida
RU2564806C2 (ru) * 2013-08-28 2015-10-10 Общество с ограниченной ответственностью "Экостар-Наутех" (ООО"Экостар-Наутех") Способ получения ультрачистого карбоната лития из технического карбоната лития и установка для его осуществления
EP3060522B1 (en) 2013-10-23 2019-06-12 Nemaska Lithium Inc. Processes for preparing lithium carbonate
CA3275949A1 (en) 2014-02-24 2025-10-31 Nemaska Lithium Inc. Methods for treating lithium-containing materials
FI127782B (fi) 2014-12-02 2019-02-15 Keliber Oy Menetelmä litiummetallifosfaattien tuottamiseksi
CN108367933B (zh) 2015-08-27 2020-10-09 内玛斯卡锂公司 用于处理含锂材料的方法
CN105347364A (zh) * 2015-10-30 2016-02-24 华陆工程科技有限责任公司 一种碳酸锂生产中沉锂母液闭环回收的方法
FI128092B (fi) 2016-06-01 2019-09-13 Keliber Oy Menetelmä johtamattomien litiummetallifosfaattien tuottamiseksi
CA2940509A1 (en) 2016-08-26 2018-02-26 Nemaska Lithium Inc. Processes for treating aqueous compositions comprising lithium sulfate and sulfuric acid
CN107777712A (zh) * 2016-08-27 2018-03-09 湖南金源新材料股份有限公司 用粗制氟化锂制取工业级碳酸锂的方法及碳酸锂产品
EP4438749A3 (en) 2016-11-14 2025-01-08 Lilac Solutions, Inc. Lithium extraction with coated ion exchange particles
CN106892443B (zh) * 2017-03-30 2019-03-15 山西北斗星新材料有限公司 利用离子交换法制取高纯碳酸锂的工艺方法
AR112663A1 (es) 2017-08-02 2019-11-27 Lilac Solutions Inc Extracción de litio con perlas porosas de intercambio iónico
US10439200B2 (en) 2017-08-02 2019-10-08 Lilac Solutions, Inc. Ion exchange system for lithium extraction
KR20240075840A (ko) 2017-11-22 2024-05-29 네마스카 리튬 인코포레이션 다양한 금속의 하이드록사이드와 옥사이드 및 이들의 유도체를 제조하는 방법
KR20200116526A (ko) 2018-02-28 2020-10-12 리락 솔루션즈, 인크. 리튬 추출을 위한 입자 트랩을 가진 이온 교환 반응기
CA3141478A1 (en) 2019-05-22 2020-11-26 Nemaska Lithium Inc. Processes for preparing hydroxides and oxides of various metals and derivatives thereof
KR20220119166A (ko) 2020-01-09 2022-08-26 리락 솔루션즈, 인크. 바람직하지 않은 금속의 분리 방법
WO2021146417A1 (en) * 2020-01-17 2021-07-22 Bl Technologies, Inc. Ion exchange system and method for conversion of aqueous lithium solution
CA3178825A1 (en) 2020-06-09 2021-12-16 David Henry SNYDACKER Lithium extraction in the presence of scalants
CA3199218A1 (en) 2020-11-20 2022-05-27 David Henry SNYDACKER Lithium production with volatile acid
CN112717468A (zh) * 2020-12-09 2021-04-30 西安蓝晓科技新材料股份有限公司 一种用于沉锂母液中锂回收的方法
KR20240014047A (ko) 2021-04-23 2024-01-31 리락 솔루션즈, 인크. 리튬 추출을 위한 이온 교환 장치
EP4499260A4 (en) 2022-03-28 2026-04-01 Lilac Solutions Inc DEVICES FOR THE EFFICIENT USE OF SORBANTS IN LITHIUM EXTRACTION
AR128953A1 (es) 2022-04-01 2024-06-26 Lilac Solutions Inc Extracción de litio con aditivos químicos
CN121941781A (zh) * 2023-08-31 2026-04-28 澳源泰科有限责任公司 一种方法及设备
CN117125729B (zh) * 2023-09-25 2025-09-30 唐山鑫丰锂业有限公司 一种锂矿石制备碳酸锂的方法
WO2025120255A1 (en) 2023-12-08 2025-06-12 Metso Finland Oy Leaching of lithium concentrates
WO2025120256A1 (en) 2023-12-08 2025-06-12 Metso Finland Oy A novel leaching process of lithium concentrates
CN120648917A (zh) 2024-03-15 2025-09-16 美卓芬兰有限公司 未煅烧的锂精矿的新型大气压浸出方法

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FR2743798B1 (fr) * 1996-01-18 1998-02-27 Air Liquide Procede de purification d'une solution de sels de lithium contaminee par des cations metalliques et utilisation de ce procede dans la fabrication de zeolites echangees au lithium
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CN1312040C (zh) * 2005-06-22 2007-04-25 广州锐鑫锂能新材料科技有限公司 工业级氢氧化锂生产高纯高清氢氧化锂的提纯方法
CN101177288B (zh) * 2007-10-30 2010-08-11 中国科学院青海盐湖研究所 一种利用盐湖锂资源制取高纯碳酸锂的工艺方法

Also Published As

Publication number Publication date
CN102348817A (zh) 2012-02-08
AU2010223194B2 (en) 2014-08-07
BRPI1009523B1 (pt) 2017-08-01
AR075734A1 (es) 2011-04-20
FI20090090A0 (fi) 2009-03-11
CL2011002230A1 (es) 2012-02-17
ES2379423B1 (es) 2013-01-24
US9284626B2 (en) 2016-03-15
EA201190148A1 (ru) 2012-03-30
CA2755123A1 (en) 2010-09-16
BRPI1009523A2 (pt) 2016-03-15
CN102348817B (zh) 2014-10-08
PT2010103173W (pt) 2014-08-11
US20110318253A1 (en) 2011-12-29
FI121785B (fi) 2011-04-15
ES2379423A1 (es) 2012-04-26
EA019279B9 (ru) 2014-06-30
CA2755123C (en) 2016-08-23
AU2010223194A1 (en) 2011-09-08
WO2010103173A1 (en) 2010-09-16
EA019279B1 (ru) 2014-02-28

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