FI57273C - Foerfarande foer framstaellning av titantetrafluorid - Google Patents

Foerfarande foer framstaellning av titantetrafluorid Download PDF

Info

Publication number: FI57273C
Authority: FI; Finland
Prior art keywords: titanium; ferrous; temperature; ferric; iron
Prior art date: 1972-06-27

Application number

FI991/73A

Other languages

English (en)

Finnish (fi)

Other versions

FI57273B (fi

Inventor

John Hickman Moss

Barrie Leng

Original Assignee

British Titan Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1972-06-27

Filing date

1973-03-30

Publication date

1980-07-10

1973-03-30 Application filed by British Titan Ltd filed Critical British Titan Ltd

1980-03-31 Application granted granted Critical

1980-03-31 Publication of FI57273B publication Critical patent/FI57273B/fi

1980-07-10 Publication of FI57273C publication Critical patent/FI57273C/fi

Links

XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 30
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 20
238000000034 method Methods 0.000 claims description 19
239000010936 titanium Substances 0.000 claims description 19
229910052719 titanium Inorganic materials 0.000 claims description 19
XROWMBWRMNHXMF-UHFFFAOYSA-J titanium tetrafluoride Chemical compound [F-].[F-].[F-].[F-].[Ti+4] XROWMBWRMNHXMF-UHFFFAOYSA-J 0.000 claims description 15
239000000463 material Substances 0.000 claims description 13
229910052742 iron Inorganic materials 0.000 claims description 12
238000004519 manufacturing process Methods 0.000 claims description 7
239000000126 substance Substances 0.000 claims description 6
239000003153 chemical reaction reagent Substances 0.000 claims description 5
YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical group O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 claims description 5
SHXXPRJOPFJRHA-UHFFFAOYSA-K iron(iii) fluoride Chemical compound F[Fe](F)F SHXXPRJOPFJRHA-UHFFFAOYSA-K 0.000 claims description 4
230000003647 oxidation Effects 0.000 claims description 2
238000007254 oxidation reaction Methods 0.000 claims description 2
CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims 3
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
230000015572 biosynthetic process Effects 0.000 claims 1
229910052739 hydrogen Inorganic materials 0.000 claims 1
239000001257 hydrogen Substances 0.000 claims 1
FZGIHSNZYGFUGM-UHFFFAOYSA-L iron(ii) fluoride Chemical compound [F-].[F-].[Fe+2] FZGIHSNZYGFUGM-UHFFFAOYSA-L 0.000 claims 1
239000013618 particulate matter Substances 0.000 claims 1
239000011541 reaction mixture Substances 0.000 claims 1
238000011144 upstream manufacturing Methods 0.000 claims 1
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 21
238000006243 chemical reaction Methods 0.000 description 12
239000004408 titanium dioxide Substances 0.000 description 9
239000002245 particle Substances 0.000 description 7
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 6
239000000049 pigment Substances 0.000 description 6
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
239000007787 solid Substances 0.000 description 5
238000010438 heat treatment Methods 0.000 description 4
NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 4
239000007864 aqueous solution Substances 0.000 description 3
239000007795 chemical reaction product Substances 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
239000002516 radical scavenger Substances 0.000 description 3
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
229910017855 NH 4 F Inorganic materials 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
238000001354 calcination Methods 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
238000009833 condensation Methods 0.000 description 2
230000005494 condensation Effects 0.000 description 2
235000003891 ferrous sulphate Nutrition 0.000 description 2
239000007789 gas Substances 0.000 description 2
239000000203 mixture Substances 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
239000000243 solution Substances 0.000 description 2
239000007858 starting material Substances 0.000 description 2
238000009283 thermal hydrolysis Methods 0.000 description 2
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
239000012298 atmosphere Substances 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
239000012159 carrier gas Substances 0.000 description 1
238000001816 cooling Methods 0.000 description 1
239000007857 degradation product Substances 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
239000011790 ferrous sulphate Substances 0.000 description 1
239000011874 heated mixture Substances 0.000 description 1
229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
230000007062 hydrolysis Effects 0.000 description 1
238000006460 hydrolysis reaction Methods 0.000 description 1
-1 ilmenite Chemical compound 0.000 description 1
230000001939 inductive effect Effects 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 1
229910000359 iron(II) sulfate Inorganic materials 0.000 description 1
229910000462 iron(III) oxide hydroxide Inorganic materials 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
GEPDYQSQVLXLEU-AATRIKPKSA-N methyl (e)-3-dimethoxyphosphoryloxybut-2-enoate Chemical compound COC(=O)\C=C(/C)OP(=O)(OC)OC GEPDYQSQVLXLEU-AATRIKPKSA-N 0.000 description 1
239000011707 mineral Substances 0.000 description 1
235000010755 mineral Nutrition 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
239000012299 nitrogen atmosphere Substances 0.000 description 1
JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
239000000047 product Substances 0.000 description 1
238000000746 purification Methods 0.000 description 1
239000002994 raw material Substances 0.000 description 1
238000011084 recovery Methods 0.000 description 1
239000004576 sand Substances 0.000 description 1
239000002002 slurry Substances 0.000 description 1
XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 1
239000012808 vapor phase Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
230000004584 weight gain Effects 0.000 description 1
235000019786 weight gain Nutrition 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/028—Titanium fluoride
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
- C22B34/1222—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes using a halogen containing agent
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
General Life Sciences & Earth Sciences (AREA)
Geology (AREA)
Environmental & Geological Engineering (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Inorganic Chemistry (AREA)
Manufacturing & Machinery (AREA)
Materials Engineering (AREA)
Mechanical Engineering (AREA)
Metallurgy (AREA)
Inorganic Compounds Of Heavy Metals (AREA)
Compounds Of Iron (AREA)

FI991/73A 1972-06-27 1973-03-30 Foerfarande foer framstaellning av titantetrafluorid FI57273C (fi)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
GB2994472		1972-06-27
GB2994472A GB1357499A (en)	1972-06-27	1972-06-27	Production of titanium tetrafluoride

Publications (2)

Publication Number	Publication Date
FI57273B FI57273B (fi)	1980-03-31
FI57273C true FI57273C (fi)	1980-07-10

Family

ID=10299742

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
FI991/73A FI57273C (fi)	1972-06-27	1973-03-30	Foerfarande foer framstaellning av titantetrafluorid

Country Status (12)

Country	Link
US (1)	US3925531A (fr)
AU (1)	AU468091B2 (fr)
BE (1)	BE801460A (fr)
CA (1)	CA990048A (fr)
DE (1)	DE2314923A1 (fr)
FI (1)	FI57273C (fr)
FR (1)	FR2190734B1 (fr)
GB (1)	GB1357499A (fr)
NL (1)	NL7304445A (fr)
NO (1)	NO134903C (fr)
SE (1)	SE399411B (fr)
ZA (1)	ZA731440B (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4359449A (en) *	1980-12-15	1982-11-16	Occidental Research Corporation	Process for making titanium oxide from titanium ore
US4401467A (en) *	1980-12-15	1983-08-30	Jordan Robert K	Continuous titanium process
US4917872A (en) *	1987-12-04	1990-04-17	Nkk Corporation	Method for producing titanium fluoride
AU7827300A (en) *	1999-09-09	2001-04-10	Starmet Corporation	Method for producing titanium tetrafluoride from uranium tetrafluoride
CN104803413A (zh) *	2015-03-16	2015-07-29	多氟多化工股份有限公司	一种四氟化钛的制备方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2167784A (en) *	1936-01-13	1939-08-01	Sherwin Williams Co	Method of treating iron fluoride
US2816815A (en) *	1955-02-16	1957-12-17	Mallinckrodt Chemical Works	Process for separating values of titanium from columbium and tantalum values
US2900234A (en) *	1957-02-11	1959-08-18	Allied Chem	Manufacture of titanium tetrafluoride
GB881532A (en) *	1958-11-27	1961-11-08	Atomic Energy Authority Uk	Improvements in or relating to the recovery of hydrogen fluoride from its azeotrope with water
US3416885A (en) *	1966-03-01	1968-12-17	Nat Lead Co	Process for producing a titanium sulfate solution and a tio2 concentrate from a titaniferous ore
US3705007A (en) *	1970-08-25	1972-12-05	Allied Chem	Process for the preparation of ammonium bifluoride from ammonium fluoride

1972
- 1972-06-27 GB GB2994472A patent/GB1357499A/en not_active Expired
1973
- 1973-03-01 ZA ZA731440A patent/ZA731440B/xx unknown
- 1973-03-07 AU AU53015/73A patent/AU468091B2/en not_active Expired
- 1973-03-09 CA CA166,582A patent/CA990048A/en not_active Expired
- 1973-03-26 DE DE19732314923 patent/DE2314923A1/de not_active Ceased
- 1973-03-30 NL NL7304445A patent/NL7304445A/xx not_active Application Discontinuation
- 1973-03-30 FI FI991/73A patent/FI57273C/fi active
- 1973-04-09 US US349454A patent/US3925531A/en not_active Expired - Lifetime
- 1973-06-22 NO NO2609/73A patent/NO134903C/no unknown
- 1973-06-26 BE BE132738A patent/BE801460A/fr unknown
- 1973-06-26 SE SE7308957A patent/SE399411B/xx unknown
- 1973-06-26 FR FR7323307A patent/FR2190734B1/fr not_active Expired

Also Published As

Publication number	Publication date
FR2190734B1 (fr)	1976-05-28
ZA731440B (en)	1974-10-30
FR2190734A1 (fr)	1974-02-01
SE399411B (sv)	1978-02-13
NO134903B (fr)	1976-09-27
GB1357499A (en)	1974-06-19
US3925531A (en)	1975-12-09
AU5301573A (en)	1974-09-12
BE801460A (fr)	1973-12-26
CA990048A (en)	1976-06-01
NO134903C (fr)	1977-01-05
AU468091B2 (en)	1975-12-18
FI57273B (fi)	1980-03-31
DE2314923A1 (de)	1974-01-17
NL7304445A (fr)	1974-01-02

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