FR2365556A2 - Preparation de l'a-amino-g-methylmercaptobutyronitrile - Google Patents
Preparation de l'a-amino-g-methylmercaptobutyronitrileInfo
- Publication number
- FR2365556A2 FR2365556A2 FR7628786A FR7628786A FR2365556A2 FR 2365556 A2 FR2365556 A2 FR 2365556A2 FR 7628786 A FR7628786 A FR 7628786A FR 7628786 A FR7628786 A FR 7628786A FR 2365556 A2 FR2365556 A2 FR 2365556A2
- Authority
- FR
- France
- Prior art keywords
- butyronitrile
- alpha
- mercapto
- methyl
- gamma
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title 2
- 229910021529 ammonia Inorganic materials 0.000 title 1
- VWWOJJANXYSACS-UHFFFAOYSA-N 2-hydroxy-4-methylsulfanylbutanenitrile Chemical compound CSCCC(O)C#N VWWOJJANXYSACS-UHFFFAOYSA-N 0.000 abstract 7
- FFEARJCKVFRZRR-BYPYZUCNSA-N L-methionine Chemical compound CSCC[C@H](N)C(O)=O FFEARJCKVFRZRR-BYPYZUCNSA-N 0.000 abstract 1
- 238000005576 amination reaction Methods 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229930182817 methionine Natural products 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C07C323/23—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
- C07C323/24—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
- C07C323/25—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procédé pour la préparation de l' alpha -amino- alpha -méthyl-mercaptobutyronitrile. Il consiste à aminer l' alpha -hydroxy-y-méthylmercaptobutyronitrile par de l'ammoniac en présence d'une proportion d'eau, de préférence égale à plus d'une mole H 2 O pour 1 mole NH3 ; l'opération se fait en continu entre 50 et 100 degrés C, en 1 à 30 minutes, sous 1 à 10 bars. Le nitrile est un intermédiaire important pour la fabrication de la méthionine.
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7628786A FR2365556A2 (fr) | 1976-09-24 | 1976-09-24 | Preparation de l'a-amino-g-methylmercaptobutyronitrile |
| GB7641519A GB1542488A (en) | 1975-10-10 | 1976-10-06 | Process for preparing alpha-amino-gamma-methylmercaptobutyronitrile |
| BR7606776A BR7606776A (pt) | 1975-10-10 | 1976-10-08 | Processo para preparacao de alfa-amino-gama-metil-mercaptobutiro-nitrila |
| MX10081276U MX5231E (es) | 1975-10-10 | 1976-10-08 | Procedimiento para preparar alfa-amino-gamma-metilmer-captobutironitrilo |
| DE19762645544 DE2645544A1 (de) | 1975-10-10 | 1976-10-08 | Herstellung von alpha-amino-gamma- methylmerkaptobutyronitril |
| JP51120853A JPS6026779B2 (ja) | 1975-10-10 | 1976-10-09 | α‐アミノ‐r‐メチルメルカプトブチロニトリルの製造方法 |
| IT28176/76A IT1068443B (it) | 1975-10-10 | 1976-10-11 | Procedimento di preparazione dell'alfa ammino gamma metilmercaptobutirronitrile |
| US05/731,628 US4064159A (en) | 1975-10-10 | 1976-10-12 | Process for preparing alpha-amino-gamma-methylmercaptobutyronitrile |
| ES452377A ES452377A1 (es) | 1975-10-10 | 1976-10-14 | Procedimiento para la preparacion de alfa amino-y metilmer- capto-butironitrilo. |
| PT6575876A PT65758B (fr) | 1976-09-24 | 1976-10-25 | Procede pour la preparation de 1'alpha-amino-gama-methylmercaptobutyronitrilo |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7628786A FR2365556A2 (fr) | 1976-09-24 | 1976-09-24 | Preparation de l'a-amino-g-methylmercaptobutyronitrile |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2365556A2 true FR2365556A2 (fr) | 1978-04-21 |
| FR2365556B2 FR2365556B2 (fr) | 1979-06-01 |
Family
ID=9178056
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7628786A Granted FR2365556A2 (fr) | 1975-10-10 | 1976-09-24 | Preparation de l'a-amino-g-methylmercaptobutyronitrile |
Country Status (2)
| Country | Link |
|---|---|
| FR (1) | FR2365556A2 (fr) |
| PT (1) | PT65758B (fr) |
-
1976
- 1976-09-24 FR FR7628786A patent/FR2365556A2/fr active Granted
- 1976-10-25 PT PT6575876A patent/PT65758B/fr unknown
Non-Patent Citations (1)
| Title |
|---|
| NEANT * |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2365556B2 (fr) | 1979-06-01 |
| PT65758B (fr) | 1978-04-27 |
| PT65758A (fr) | 1976-11-01 |
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