FR2395314A1 - Procede et appareil d'hydrolyse en continu de matieres lignocellulosiques - Google Patents
Procede et appareil d'hydrolyse en continu de matieres lignocellulosiquesInfo
- Publication number
- FR2395314A1 FR2395314A1 FR7809300A FR7809300A FR2395314A1 FR 2395314 A1 FR2395314 A1 FR 2395314A1 FR 7809300 A FR7809300 A FR 7809300A FR 7809300 A FR7809300 A FR 7809300A FR 2395314 A1 FR2395314 A1 FR 2395314A1
- Authority
- FR
- France
- Prior art keywords
- continuous hydrolysis
- sugars
- production
- lignocellulosic materials
- hydrolysis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 230000007062 hydrolysis Effects 0.000 title abstract 3
- 238000006460 hydrolysis reaction Methods 0.000 title abstract 3
- 239000012978 lignocellulosic material Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 235000000346 sugar Nutrition 0.000 abstract 2
- 150000008163 sugars Chemical class 0.000 abstract 2
- 238000005470 impregnation Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000011343 solid material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Saccharide Compounds (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
L'invention concerne la production de sucres par hydrolyse en continu de matières lignocellulosiques sous forme solide divisée, par contact avec de l'acide chlorhydrique concentré. Selon l'invention, on prévoit un réacteur tubulaire rotatif 1 avec une paroi tubulaire 2, des palettes internes 12, une paroi extrême transversale 5 avec entrée centrale 6 de la matière solide à hydrolyser, un distributeur 20 de liquide, une chicane hélicoïdale 13; le réacteur est divisé en une zone d'imprégnation I et une zone d'hydrolyse H. L'invention concerne la production de sucres à partir de matières végétales.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH412077A CH609092A5 (fr) | 1977-04-01 | 1977-04-01 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2395314A1 true FR2395314A1 (fr) | 1979-01-19 |
| FR2395314B1 FR2395314B1 (fr) | 1980-04-11 |
Family
ID=4270183
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7809300A Granted FR2395314A1 (fr) | 1977-04-01 | 1978-03-30 | Procede et appareil d'hydrolyse en continu de matieres lignocellulosiques |
Country Status (24)
| Country | Link |
|---|---|
| US (3) | US4199371A (fr) |
| JP (1) | JPS53124632A (fr) |
| AT (1) | AT361418B (fr) |
| AU (1) | AU518576B2 (fr) |
| BE (1) | BE865584A (fr) |
| BR (1) | BR7802044A (fr) |
| CA (1) | CA1100492A (fr) |
| CH (1) | CH609092A5 (fr) |
| CU (1) | CU21104A (fr) |
| DE (1) | DE2814067A1 (fr) |
| DK (1) | DK144578A (fr) |
| EG (1) | EG13177A (fr) |
| ES (1) | ES468437A1 (fr) |
| FI (1) | FI63965C (fr) |
| FR (1) | FR2395314A1 (fr) |
| GB (1) | GB1562682A (fr) |
| IT (1) | IT1093515B (fr) |
| MX (1) | MX5047E (fr) |
| NL (1) | NL7803360A (fr) |
| NO (1) | NO145694C (fr) |
| NZ (1) | NZ186826A (fr) |
| OA (1) | OA05924A (fr) |
| PL (1) | PL205735A1 (fr) |
| SE (1) | SE439648B (fr) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH625251A5 (fr) * | 1978-10-04 | 1981-09-15 | Battelle Memorial Institute | |
| NZ193139A (en) * | 1979-03-23 | 1982-05-25 | Univ California | Hydrolysis of cellulosic and lignocellulosic material to produce monosaccharides ethanol and methane |
| US4384897A (en) * | 1981-11-23 | 1983-05-24 | The Regents Of The University Of California | Method of treating biomass material |
| US4237110A (en) * | 1979-04-30 | 1980-12-02 | The Dow Chemical Company | Process for separating and recovering concentrated hydrochloric acid from the crude product obtained from the acid hydrolysis of cellulose |
| FI58346C (fi) * | 1979-12-18 | 1981-01-12 | Tampella Oy Ab | Foerfarande foer kontinuerlig foersockring av cellulosa av vaextmaterial |
| DE3437689A1 (de) * | 1984-10-15 | 1986-04-17 | Hoechst Ag, 6230 Frankfurt | Vorrichtung zur reduktion von eisen und vanadium in phosphorsaurer loesung |
| US4933283A (en) * | 1985-05-15 | 1990-06-12 | Mobil Oil Corporation | Process for converting cellulosic materials to hydrocarbon products |
| US6022419A (en) * | 1996-09-30 | 2000-02-08 | Midwest Research Institute | Hydrolysis and fractionation of lignocellulosic biomass |
| BR9902607B1 (pt) * | 1999-06-23 | 2010-08-24 | aparelho e processo de prÉ-hidràlise de biomassa. | |
| US20230304739A1 (en) * | 2004-05-04 | 2023-09-28 | Sibelco North America Inc. | Rotary batch reactor vessel |
| AU2005279145A1 (en) * | 2004-09-01 | 2006-03-09 | Shell Internationale Research Maatschappij B.V. | Horizontal reactor vessel |
| DK1828373T3 (da) * | 2004-11-29 | 2011-10-17 | Inbicon As | Enzymatisk hydrolyse af biomasser med et højt tørstof (DM) indhold |
| EP1690980A1 (fr) * | 2005-02-11 | 2006-08-16 | Agrotechnology and Food Innovations B.V. | Procédé et appareil pour la conversion de la biomasse |
| EP1869194A2 (fr) * | 2005-04-12 | 2007-12-26 | E.I.Du pont de nemours and company | Obtention de produit chimique cible par traitement de biomasse |
| US20070029252A1 (en) * | 2005-04-12 | 2007-02-08 | Dunson James B Jr | System and process for biomass treatment |
| US7585104B2 (en) * | 2005-09-12 | 2009-09-08 | Uop Llc | Rotary processor |
| US7815876B2 (en) | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
| US7815741B2 (en) * | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
| CN103201395B (zh) | 2010-06-26 | 2016-03-02 | 威尔迪亚有限公司 | 糖混合物及其生产和使用方法 |
| IL206678A0 (en) | 2010-06-28 | 2010-12-30 | Hcl Cleantech Ltd | A method for the production of fermentable sugars |
| IL207329A0 (en) | 2010-08-01 | 2010-12-30 | Robert Jansen | A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition |
| IL207945A0 (en) | 2010-09-02 | 2010-12-30 | Robert Jansen | Method for the production of carbohydrates |
| WO2012061085A2 (fr) * | 2010-10-24 | 2012-05-10 | Hcl Cleantech Ltd | Systèmes et procédés d'hydrolyse |
| WO2012137201A1 (fr) | 2011-04-07 | 2012-10-11 | Hcl Cleantech Ltd. | Procédés et produits de conversion de lignocellulose |
| WO2013055785A1 (fr) | 2011-10-10 | 2013-04-18 | Virdia Ltd | Compositions de sucre |
| EP2878614A1 (fr) | 2012-05-03 | 2015-06-03 | Virdia Ltd. | Procédés de traitement de matières lignocellulosiques |
| US9493851B2 (en) | 2012-05-03 | 2016-11-15 | Virdia, Inc. | Methods for treating lignocellulosic materials |
| DE102012020166A1 (de) * | 2012-10-13 | 2014-04-30 | Green Sugar Gmbh Produktinnovationen Aus Biomasse | Verfahren zur Hydrolyse von pelletierfähigen Biomassen mittels Halogenwasserstoffsäuren |
| WO2016082816A1 (fr) * | 2014-11-26 | 2016-06-02 | Green Sugar Gmbh Produktinnovationen Aus Biomasse | Procédé d'introduction d'acide dans des installations d'hydrolyse pour l'hydrolyse acide de biomasse végétale au moyen d'acide chlorhydrique concentré |
| EP3233876B1 (fr) | 2014-12-18 | 2019-02-20 | Avantium Knowledge Centre B.v. | Procédé de préparation d'une solution contenant un saccharide à partir de biomasse cellulosique torréfiée |
| US11078548B2 (en) | 2015-01-07 | 2021-08-03 | Virdia, Llc | Method for producing xylitol by fermentation |
| BR112017025322A8 (pt) | 2015-05-27 | 2022-08-23 | Virdia Inc | Processos integrados para recuperação de hidrolisato celulósico após hidrólise de polpa de celulose |
| GB2548386A (en) | 2016-03-17 | 2017-09-20 | Alkymar As | Mixing and processing apparatus |
| WO2018041975A1 (fr) | 2016-08-31 | 2018-03-08 | Avantium Knowledge Centre B.V. | Réacteur d'hydrolyse et hydrolyse |
| KR20190096357A (ko) | 2016-12-13 | 2019-08-19 | 아반티움 놀리지 센터 비.브이. | 오염된 염산 조성물 정제 공정 |
| FR3075202B1 (fr) | 2017-12-20 | 2020-08-28 | Ifp Energies Now | Procede de traitement de biomasse ligno-cellulosique |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR798559A (fr) * | 1934-04-23 | 1936-05-20 | Procédé et appareil pour l'hydrolyse des celluloses et ligno-celluloses | |
| FR904371A (fr) * | 1943-12-17 | 1945-11-05 | Procédé perfectionné d'hydrolyse des déchets de bois ou végétaux et appareil digesteur pour l'application du procédé | |
| GB681345A (en) * | 1948-07-27 | 1952-10-22 | Glucol Soc Du | Improvements in or relating to a method for the hydrolysis of cellulose materials |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1670727A (en) * | 1920-02-05 | 1928-05-22 | Kocher Rudolph Alfred | Process and apparatus for converting carbohydrates |
| DE524156C (de) * | 1929-11-05 | 1931-05-02 | Siller & Rodenkirchen G M B H | Rotierender Autoklav zur Gewinnung von Glukose aus Holzstoff |
| US1990097A (en) * | 1929-12-09 | 1935-02-05 | Scholler Heinrich | Process of converting cellulose and the like into sugar with dilute acids under pressure |
| US2086701A (en) * | 1933-08-30 | 1937-07-13 | Dreyfus Henry | Hydrolysis of cellulose |
| US2239095A (en) * | 1939-06-21 | 1941-04-22 | Eastman Kodak Co | Saccharification of wood |
| US2375499A (en) * | 1943-08-05 | 1945-05-08 | Dow Chemical Co | Rotary lime treating apparatus |
| US2538457A (en) * | 1946-11-02 | 1951-01-16 | Monie S Hudson | Treating wood |
| US2778751A (en) * | 1952-03-21 | 1957-01-22 | Bergin Ag Deutsche | Hydrolysis of wood with concentrated hydrochloric acid |
| US2969277A (en) * | 1956-05-17 | 1961-01-24 | Dano Ingeniorforretning Og Mas | Apparatus for the fermentation of solid organic materials |
| US2951775A (en) * | 1956-12-12 | 1960-09-06 | Udic Sa | Selective saccharification of cellulosic materials |
| US2948593A (en) * | 1957-04-15 | 1960-08-09 | Larson John David | Digester for converting inorganic material into assimilable plant food |
| US3212933A (en) * | 1963-04-12 | 1965-10-19 | Georgia Pacific Corp | Hydrolysis of lignocellulose materials with solvent extraction of the hydrolysate |
| US3523911A (en) * | 1969-02-26 | 1970-08-11 | Harald F Funk | Method of separating components of cellulosic material |
| US3676074A (en) * | 1969-06-30 | 1972-07-11 | Yamato Setubi Koji Kk | Apparatus for treating organic waste |
| US4018567A (en) * | 1973-05-14 | 1977-04-19 | James P. La Point, Jr. | Apparatus for separating the constituents of lead-acid storage batteries |
-
1977
- 1977-04-01 CH CH412077A patent/CH609092A5/xx not_active IP Right Cessation
-
1978
- 1978-03-29 EG EG218/78A patent/EG13177A/xx active
- 1978-03-29 AT AT220578A patent/AT361418B/de not_active IP Right Cessation
- 1978-03-29 MX MX786978U patent/MX5047E/es unknown
- 1978-03-29 DE DE19782814067 patent/DE2814067A1/de not_active Withdrawn
- 1978-03-29 FI FI780956A patent/FI63965C/fi not_active IP Right Cessation
- 1978-03-30 NZ NZ186826A patent/NZ186826A/xx unknown
- 1978-03-30 CA CA300,079A patent/CA1100492A/fr not_active Expired
- 1978-03-30 NL NL7803360A patent/NL7803360A/xx not_active Application Discontinuation
- 1978-03-30 FR FR7809300A patent/FR2395314A1/fr active Granted
- 1978-03-30 GB GB12429/78A patent/GB1562682A/en not_active Expired
- 1978-03-30 SE SE7803578A patent/SE439648B/sv not_active IP Right Cessation
- 1978-03-30 OA OA56453A patent/OA05924A/fr unknown
- 1978-03-31 PL PL20573578A patent/PL205735A1/xx unknown
- 1978-03-31 NO NO781128A patent/NO145694C/no unknown
- 1978-03-31 AU AU34664/78A patent/AU518576B2/en not_active Expired
- 1978-03-31 US US05/892,329 patent/US4199371A/en not_active Expired - Lifetime
- 1978-03-31 IT IT21847/78A patent/IT1093515B/it active
- 1978-03-31 DK DK144578A patent/DK144578A/da not_active IP Right Cessation
- 1978-03-31 BR BR7802044A patent/BR7802044A/pt unknown
- 1978-03-31 JP JP3694078A patent/JPS53124632A/ja active Pending
- 1978-03-31 BE BE186481A patent/BE865584A/fr not_active IP Right Cessation
- 1978-03-31 CU CU7834898A patent/CU21104A/es unknown
- 1978-03-31 ES ES468437A patent/ES468437A1/es not_active Expired
-
1979
- 1979-04-24 US US06/032,891 patent/US4257818A/en not_active Expired - Lifetime
-
1980
- 1980-09-03 US US06/183,817 patent/US4304608A/en not_active Expired - Lifetime
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR798559A (fr) * | 1934-04-23 | 1936-05-20 | Procédé et appareil pour l'hydrolyse des celluloses et ligno-celluloses | |
| FR904371A (fr) * | 1943-12-17 | 1945-11-05 | Procédé perfectionné d'hydrolyse des déchets de bois ou végétaux et appareil digesteur pour l'application du procédé | |
| GB681345A (en) * | 1948-07-27 | 1952-10-22 | Glucol Soc Du | Improvements in or relating to a method for the hydrolysis of cellulose materials |
Also Published As
| Publication number | Publication date |
|---|---|
| IT7821847A0 (it) | 1978-03-31 |
| BE865584A (fr) | 1978-10-02 |
| CA1100492A (fr) | 1981-05-05 |
| US4199371A (en) | 1980-04-22 |
| PL205735A1 (pl) | 1979-01-15 |
| FR2395314B1 (fr) | 1980-04-11 |
| NO145694C (no) | 1982-05-12 |
| FI63965C (fi) | 1983-09-12 |
| DK144578A (da) | 1978-10-02 |
| CH609092A5 (fr) | 1979-02-15 |
| FI780956A7 (fi) | 1978-10-02 |
| AU3466478A (en) | 1979-10-04 |
| AT361418B (de) | 1981-03-10 |
| ATA220578A (de) | 1980-07-15 |
| IT1093515B (it) | 1985-07-19 |
| EG13177A (en) | 1980-12-31 |
| MX5047E (es) | 1983-03-02 |
| SE7803578L (sv) | 1978-10-02 |
| SE439648B (sv) | 1985-06-24 |
| ES468437A1 (es) | 1979-01-01 |
| GB1562682A (en) | 1980-03-12 |
| US4257818A (en) | 1981-03-24 |
| US4304608A (en) | 1981-12-08 |
| NO781128L (no) | 1978-10-03 |
| BR7802044A (pt) | 1978-12-19 |
| CU21104A (es) | 1981-01-10 |
| AU518576B2 (en) | 1981-10-08 |
| DE2814067A1 (de) | 1978-10-12 |
| NZ186826A (en) | 1979-06-19 |
| FI63965B (fi) | 1983-05-31 |
| NO145694B (no) | 1982-02-01 |
| OA05924A (fr) | 1981-06-30 |
| NL7803360A (nl) | 1978-10-03 |
| JPS53124632A (en) | 1978-10-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |