FR2432013A1 - Procede d'obtention de dinitro-1,5 anthraquinone de haute purete - Google Patents
Procede d'obtention de dinitro-1,5 anthraquinone de haute pureteInfo
- Publication number
- FR2432013A1 FR2432013A1 FR7822215A FR7822215A FR2432013A1 FR 2432013 A1 FR2432013 A1 FR 2432013A1 FR 7822215 A FR7822215 A FR 7822215A FR 7822215 A FR7822215 A FR 7822215A FR 2432013 A1 FR2432013 A1 FR 2432013A1
- Authority
- FR
- France
- Prior art keywords
- dinitro
- obtaining high
- purity
- anthraquinone
- degrees
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/16—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2603/00—Systems containing at least three condensed rings
- C07C2603/02—Ortho- or ortho- and peri-condensed systems
- C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
- C07C2603/22—Ortho- or ortho- and peri-condensed systems containing three rings containing only six-membered rings
- C07C2603/24—Anthracenes; Hydrogenated anthracenes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
L'invention a pour objet un procédé d'obtention de dinitro-1,5 anthraquinone de haute pureté à partir de mélanges bruts de dinitro-anthraquinones. On traite un tel mélange à une température allant de 150 à 200 degrés C au moyen d'un ester de point d'ébullition supérieur à 150 degrés C dérivé d'un alcool aliphatique contenant 1 à 4 atomes de carbone et d'un acide mono- ou dicarboxylique ou d'acide phosphorique, puis, après refroidissement éventuel sans descendre en-dessous de 150 degrés C, on sépare l'insoluble constitué essentiellement par la dinitro-1,5 anthraquinone.
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7822215A FR2432013A1 (fr) | 1978-07-27 | 1978-07-27 | Procede d'obtention de dinitro-1,5 anthraquinone de haute purete |
| US06/052,883 US4307021A (en) | 1978-07-27 | 1979-06-28 | Process for obtaining 1,5-dinitro-anthraquinone of high purity |
| IN508/DEL/79A IN152548B (fr) | 1978-07-27 | 1979-07-13 | |
| GB7925758A GB2026489B (en) | 1978-07-27 | 1979-07-24 | Process for obtaining 1,5-dinitro-anthraquinone |
| DE19792930367 DE2930367A1 (de) | 1978-07-27 | 1979-07-26 | Verfahren zur gewinnung von 1,5- dinitroanthrachinon |
| JP9432179A JPS5520764A (en) | 1978-07-27 | 1979-07-26 | Method of obtaining highly pure 1*55dinitroo anthraquinone |
| DD79214636A DD145097A5 (de) | 1978-07-27 | 1979-07-26 | Verfahren zur gewinnung von 1,5-dinitroanthrachinon |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7822215A FR2432013A1 (fr) | 1978-07-27 | 1978-07-27 | Procede d'obtention de dinitro-1,5 anthraquinone de haute purete |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2432013A1 true FR2432013A1 (fr) | 1980-02-22 |
| FR2432013B1 FR2432013B1 (fr) | 1980-12-12 |
Family
ID=9211236
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7822215A Granted FR2432013A1 (fr) | 1978-07-27 | 1978-07-27 | Procede d'obtention de dinitro-1,5 anthraquinone de haute purete |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4307021A (fr) |
| JP (1) | JPS5520764A (fr) |
| DD (1) | DD145097A5 (fr) |
| DE (1) | DE2930367A1 (fr) |
| FR (1) | FR2432013A1 (fr) |
| GB (1) | GB2026489B (fr) |
| IN (1) | IN152548B (fr) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6411009A (en) * | 1987-07-06 | 1989-01-13 | Nippon Steel Corp | Manufacture of seamless steel pipe |
| JPH02232400A (ja) * | 1989-03-07 | 1990-09-14 | Fujitsu Ltd | 電解処理装置 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2170119A1 (fr) * | 1972-02-01 | 1973-09-14 | Sandoz Sa | |
| FR2307793A1 (fr) * | 1975-04-19 | 1976-11-12 | Bayer Ag | Procede de preparation de la 1,8-dinitroanthraquinone pure |
| DE2530067A1 (de) * | 1975-07-05 | 1977-02-03 | Basf Ag | Verfahren zur abtrennung von 1,5- dinitroanthrachinon aus dinitroanthrachinongemischen |
| FR2372788A1 (fr) * | 1976-12-02 | 1978-06-30 | Bayer Ag | Procede pour isoler la 1,6- et la 1,7-dinitroanthraquinone de melanges de ces composes contenant d'autres derives nitres de l'anthraquinone |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2524747C3 (de) * | 1975-06-04 | 1980-12-18 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Isolierung von 1,5-/1,8-Dinitroanthrachinon mit einem hohen Gehalt an a , a '-Duutroverbindungen |
| DE2545699A1 (de) * | 1975-10-11 | 1977-04-21 | Basf Ag | Verfahren zur trennung von 1,5- und 1,8-dinitroanthrachinon |
-
1978
- 1978-07-27 FR FR7822215A patent/FR2432013A1/fr active Granted
-
1979
- 1979-06-28 US US06/052,883 patent/US4307021A/en not_active Expired - Lifetime
- 1979-07-13 IN IN508/DEL/79A patent/IN152548B/en unknown
- 1979-07-24 GB GB7925758A patent/GB2026489B/en not_active Expired
- 1979-07-26 DE DE19792930367 patent/DE2930367A1/de not_active Withdrawn
- 1979-07-26 JP JP9432179A patent/JPS5520764A/ja active Pending
- 1979-07-26 DD DD79214636A patent/DD145097A5/de unknown
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2170119A1 (fr) * | 1972-02-01 | 1973-09-14 | Sandoz Sa | |
| FR2307793A1 (fr) * | 1975-04-19 | 1976-11-12 | Bayer Ag | Procede de preparation de la 1,8-dinitroanthraquinone pure |
| DE2530067A1 (de) * | 1975-07-05 | 1977-02-03 | Basf Ag | Verfahren zur abtrennung von 1,5- dinitroanthrachinon aus dinitroanthrachinongemischen |
| FR2372788A1 (fr) * | 1976-12-02 | 1978-06-30 | Bayer Ag | Procede pour isoler la 1,6- et la 1,7-dinitroanthraquinone de melanges de ces composes contenant d'autres derives nitres de l'anthraquinone |
Also Published As
| Publication number | Publication date |
|---|---|
| GB2026489B (en) | 1982-09-08 |
| IN152548B (fr) | 1984-02-11 |
| DD145097A5 (de) | 1980-11-19 |
| US4307021A (en) | 1981-12-22 |
| FR2432013B1 (fr) | 1980-12-12 |
| DE2930367A1 (de) | 1980-02-14 |
| JPS5520764A (en) | 1980-02-14 |
| GB2026489A (en) | 1980-02-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |