FR2444663A1 - Procede pour la preparation de chlorhydrates d'aminoacides ou de dichlorhydrates d'acides diamines - Google Patents
Procede pour la preparation de chlorhydrates d'aminoacides ou de dichlorhydrates d'acides diaminesInfo
- Publication number
- FR2444663A1 FR2444663A1 FR7930682A FR7930682A FR2444663A1 FR 2444663 A1 FR2444663 A1 FR 2444663A1 FR 7930682 A FR7930682 A FR 7930682A FR 7930682 A FR7930682 A FR 7930682A FR 2444663 A1 FR2444663 A1 FR 2444663A1
- Authority
- FR
- France
- Prior art keywords
- amino acid
- acid
- diamine
- dichlorhydrates
- chlorhydrates
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000002253 acid Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 150000001413 amino acids Chemical class 0.000 title 1
- 150000004985 diamines Chemical class 0.000 title 1
- -1 amino acid hydrochlorides Chemical class 0.000 abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 abstract 1
- 239000004472 Lysine Substances 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001735 carboxylic acids Chemical class 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 238000007127 saponification reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
- C07C227/18—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Pour préparer des chlorhydrates d'acides aminés ou des dichlorhydrates d'acides diaminés, des esters d'acides carboxyliques halogénés sont tout d'abord convertis en le mono- ou diuréthane correspondant par réaction avec un cyanate de métal alcalin en présence d'un alcool, puis ce mono- ou diuréthane est converti en le mono- ou dichlorhydrate correspondant par saponification. Le nouveau procédé a une application relativement universelle et il ouvre avant tout une voie élégante de synthèse pour la lysine.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2854627A DE2854627C2 (de) | 1978-12-18 | 1978-12-18 | Verfahren zur Herstellung von Aminocarbonsäurehydrochloriden bzw. Diaminocarbonsäure-di-hydrochloriden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| FR2444663A1 true FR2444663A1 (fr) | 1980-07-18 |
Family
ID=6057536
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7930682A Withdrawn FR2444663A1 (fr) | 1978-12-18 | 1979-12-14 | Procede pour la preparation de chlorhydrates d'aminoacides ou de dichlorhydrates d'acides diamines |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4234744A (fr) |
| JP (1) | JPS582228B2 (fr) |
| BE (1) | BE880558A (fr) |
| DE (1) | DE2854627C2 (fr) |
| FR (1) | FR2444663A1 (fr) |
| IT (1) | IT1164027B (fr) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4988789A (en) * | 1990-01-05 | 1991-01-29 | Sandoz Ltd. | Process for preparing glycine hydrochloride |
| US5324747A (en) * | 1992-07-15 | 1994-06-28 | Hoffmann-La Roche Inc. | N-substituted anilines, inhibitors of phospholipases A2 |
| DE10048715A1 (de) * | 2000-09-30 | 2004-05-19 | Grünenthal GmbH | Verwendung von Aminosäure zur Behandlung von Schmerz |
| DE10158537A1 (de) * | 2001-11-29 | 2003-06-12 | Degussa | Verfahren zur Herstellung von Aminocarbonsäuren |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4924442A (fr) * | 1972-06-28 | 1974-03-04 | ||
| US3804844A (en) * | 1970-12-02 | 1974-04-16 | Dow Chemical Co | Process for preparing pyridylcarbamates |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2647916A (en) * | 1949-07-26 | 1953-08-04 | American Cyanamid Co | Method of preparing an nu-substituted carbamate |
| US3526655A (en) * | 1964-08-11 | 1970-09-01 | Marathon Oil Co | Preparation of isocyanate derivatives |
| US3674750A (en) * | 1971-01-14 | 1972-07-04 | Phillips Petroleum Co | Quarternary phosphonium salt catalyzed synthesis of urethanes and polyurethanes |
| US4147716A (en) * | 1978-06-05 | 1979-04-03 | Basf Wyandotte Corporation | Preparation of N-substituted carbamates |
-
1978
- 1978-12-18 DE DE2854627A patent/DE2854627C2/de not_active Expired
-
1979
- 1979-12-11 BE BE6/47033A patent/BE880558A/fr not_active IP Right Cessation
- 1979-12-14 FR FR7930682A patent/FR2444663A1/fr not_active Withdrawn
- 1979-12-17 US US06/104,064 patent/US4234744A/en not_active Expired - Lifetime
- 1979-12-17 IT IT51108/79A patent/IT1164027B/it active
- 1979-12-18 JP JP54163658A patent/JPS582228B2/ja not_active Expired
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3804844A (en) * | 1970-12-02 | 1974-04-16 | Dow Chemical Co | Process for preparing pyridylcarbamates |
| JPS4924442A (fr) * | 1972-06-28 | 1974-03-04 |
Non-Patent Citations (2)
| Title |
|---|
| CA1975 * |
| EXBK/79 * |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS582228B2 (ja) | 1983-01-14 |
| US4234744A (en) | 1980-11-18 |
| IT1164027B (it) | 1987-04-08 |
| BE880558A (fr) | 1980-06-11 |
| IT7951108A0 (it) | 1979-12-17 |
| DE2854627C2 (de) | 1980-07-03 |
| DE2854627B1 (de) | 1979-10-04 |
| JPS5583737A (en) | 1980-06-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |