FR2967924B1 - Nanocharge d'un oxyde metallique, son procede de synthese et son utilisation dans un revetement antiadhesif a base de resine fluorocarbonee - Google Patents

Nanocharge d'un oxyde metallique, son procede de synthese et son utilisation dans un revetement antiadhesif a base de resine fluorocarbonee

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Publication number
FR2967924B1
FR2967924B1 FR1059949A FR1059949A FR2967924B1 FR 2967924 B1 FR2967924 B1 FR 2967924B1 FR 1059949 A FR1059949 A FR 1059949A FR 1059949 A FR1059949 A FR 1059949A FR 2967924 B1 FR2967924 B1 FR 2967924B1
Authority
FR
France
Prior art keywords
nanocharge
synthesis
metal oxide
adhesive coating
fluorocarbon resin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1059949A
Other languages
English (en)
Other versions
FR2967924A1 (fr
Inventor
Nelly Durand
Bernard Boutevin
Bruno Ameduri
Cedric Loubat
Barbara Gantillon
Jean-Luc Perillon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SEB SA
Ecole Nationale Superieure de Chimie de Montpellier ENSCM
SPECIFIC POLYMERS
Original Assignee
SEB SA
Ecole Nationale Superieure de Chimie de Montpellier ENSCM
SPECIFIC POLYMERS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1059949A priority Critical patent/FR2967924B1/fr
Application filed by SEB SA, Ecole Nationale Superieure de Chimie de Montpellier ENSCM, SPECIFIC POLYMERS filed Critical SEB SA
Priority to US13/990,431 priority patent/US9862843B2/en
Priority to PCT/FR2011/052829 priority patent/WO2012072953A1/fr
Priority to EP11801800.1A priority patent/EP2646513A1/fr
Priority to KR1020137013726A priority patent/KR101650614B1/ko
Priority to JP2013541410A priority patent/JP5931902B2/ja
Priority to CN201180057551.6A priority patent/CN103370379B/zh
Priority to BR112013013189A priority patent/BR112013013189A2/pt
Publication of FR2967924A1 publication Critical patent/FR2967924A1/fr
Priority to CO13132813A priority patent/CO6781479A2/es
Application granted granted Critical
Publication of FR2967924B1 publication Critical patent/FR2967924B1/fr
Priority to US15/818,799 priority patent/US20180086926A1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • A—HUMAN NECESSITIES
    • A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47J—KITCHEN EQUIPMENT; COFFEE MILLS; SPICE MILLS; APPARATUS FOR MAKING BEVERAGES
    • A47J36/00—Parts, details or accessories of cooking-vessels
    • A47J36/02—Selection of specific materials, e.g. heavy bottoms with copper inlay or with insulating inlay
    • A47J36/025—Vessels with non-stick features, e.g. coatings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3072—Treatment with macro-molecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3081—Treatment with organo-silicon compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/309—Combinations of treatments provided for in groups C09C1/3009 - C09C1/3081
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/40—Compounds of aluminium
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/40—Compounds of aluminium
    • C09C1/407—Aluminium oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/006—Combinations of treatments provided for in groups C09C3/04 - C09C3/12
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/10—Treatment with macromolecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/12—Treatment with organosilicon compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/41—Organic pigments; Organic dyes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D5/00—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures
    • B05D5/08—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures to obtain an anti-friction or anti-adhesive surface
    • B05D5/083—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures to obtain an anti-friction or anti-adhesive surface involving the use of fluoropolymers
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/86—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by NMR- or ESR-data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Food Science & Technology (AREA)
  • Composite Materials (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Paints Or Removers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Silicon Compounds (AREA)
  • Graft Or Block Polymers (AREA)
  • Polyethers (AREA)
FR1059949A 2010-11-30 2010-11-30 Nanocharge d'un oxyde metallique, son procede de synthese et son utilisation dans un revetement antiadhesif a base de resine fluorocarbonee Active FR2967924B1 (fr)

Priority Applications (10)

Application Number Priority Date Filing Date Title
FR1059949A FR2967924B1 (fr) 2010-11-30 2010-11-30 Nanocharge d'un oxyde metallique, son procede de synthese et son utilisation dans un revetement antiadhesif a base de resine fluorocarbonee
BR112013013189A BR112013013189A2 (pt) 2010-11-30 2011-11-30 nanocarga de óxido de metal, método para sintetização do mesmo e uso do mesmo em um revestimento não aderente de resina de fluorocarbono
EP11801800.1A EP2646513A1 (fr) 2010-11-30 2011-11-30 Nanocharge d'un oxyde métallique, son procédé de synthèse et son utilisation dans un revêtement antiadhésif à base de résine fluorocarbonée
KR1020137013726A KR101650614B1 (ko) 2010-11-30 2011-11-30 금속 산화물 나노충전제, 그의 제조 방법 및 플루오로카본 수지 비-점착성 코팅에서의 용도
JP2013541410A JP5931902B2 (ja) 2010-11-30 2011-11-30 金属酸化物ナノ充填剤、その合成法、およびそのフッ素樹脂焦げつき防止コーティング中での使用
CN201180057551.6A CN103370379B (zh) 2010-11-30 2011-11-30 金属氧化物纳米填料、其合成方法及其在碳氟化合物树脂不粘性涂料中的应用
US13/990,431 US9862843B2 (en) 2010-11-30 2011-11-30 Metal-oxide nanofiller, method for synthesising same, and use thereof in a fluorocarbon-resin non-stick coating
PCT/FR2011/052829 WO2012072953A1 (fr) 2010-11-30 2011-11-30 Nanocharge d'un oxyde métallique, son procédé de synthèse et son utilisation dans un revêtement antiadhésif à base de résine fluorocarbonée
CO13132813A CO6781479A2 (es) 2010-11-30 2013-05-30 Nanorelleno de oxido de metal, metodo para sintetizar el mismo, y su uso en un revestimiento antiadherente de resina de fluorocarbono
US15/818,799 US20180086926A1 (en) 2010-11-30 2017-11-21 Method for synthesising a metal-oxide nanofiller, and use thereof in a fluorocarbon-resin non-stick coating

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1059949A FR2967924B1 (fr) 2010-11-30 2010-11-30 Nanocharge d'un oxyde metallique, son procede de synthese et son utilisation dans un revetement antiadhesif a base de resine fluorocarbonee

Publications (2)

Publication Number Publication Date
FR2967924A1 FR2967924A1 (fr) 2012-06-01
FR2967924B1 true FR2967924B1 (fr) 2014-10-31

Family

ID=45406778

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1059949A Active FR2967924B1 (fr) 2010-11-30 2010-11-30 Nanocharge d'un oxyde metallique, son procede de synthese et son utilisation dans un revetement antiadhesif a base de resine fluorocarbonee

Country Status (9)

Country Link
US (2) US9862843B2 (fr)
EP (1) EP2646513A1 (fr)
JP (1) JP5931902B2 (fr)
KR (1) KR101650614B1 (fr)
CN (1) CN103370379B (fr)
BR (1) BR112013013189A2 (fr)
CO (1) CO6781479A2 (fr)
FR (1) FR2967924B1 (fr)
WO (1) WO2012072953A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106958019A (zh) * 2017-04-05 2017-07-18 邢台三厦铸铁有限公司 铸铁炊具的表面处理方法及铸铁炊具

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AU2012280626B2 (en) 2011-07-07 2016-11-10 Tata Steel Nederland Technology B.V. Coated steel substrate and method for making the same
WO2015055280A1 (fr) * 2013-10-15 2015-04-23 Merck Patent Gmbh Particules de silice revêtues pour impression au jet d'encre de dispositifs électroniques organiques, procédé pour leur production et dispositifs produits à l'aide de ces particules
JP6688734B2 (ja) * 2014-01-29 2020-04-28 スリーエム イノベイティブ プロパティズ カンパニー 水性表面コーティング組成物及び改質粒子
CN104962144B (zh) * 2015-06-10 2017-12-01 李吉学 一种高温耐磨不粘涂层材料及其制备方法
FR3037965B1 (fr) * 2015-06-24 2017-07-14 Seb Sa Compositions de primaire de revetement antiadhesif et leurs procedes de preparation
FR3039091B1 (fr) * 2015-07-20 2017-07-21 Seb Sa Inclusion d'oxydes de terres rares dans un revetement a base de resine fluorocarbonee
FR3039053B1 (fr) * 2015-07-21 2018-02-02 Seb S.A. Article culinaire comprenant une couche d'oxyde de terre rare
EP3312242B1 (fr) * 2016-10-24 2019-06-26 3M Innovative Properties Company Composition de revêtement protecteur à fonctionnalités mixtes
KR102522013B1 (ko) * 2018-04-04 2023-04-14 삼성전자주식회사 고분자 및 무기입자를 포함하는 조성물, 폴리이미드-무기입자 복합체, 상기 복합체를 포함하는 성형품, 및 상기 성형품을 포함하는 광학 장치
CN109401145B (zh) * 2018-09-06 2023-09-01 安徽腾龙泵阀制造有限公司 一种耐酸碱腐蚀的氟塑料泵用材料及其制备方法
CN109337412A (zh) * 2018-10-12 2019-02-15 安庆北化大科技园有限公司 一种在水溶性体系中可梯度分布的纳米二氧化硅的制备方法
CN116998889A (zh) * 2023-08-07 2023-11-07 广东万事泰集团有限公司 一种激光钛耐磨高硬度厨具及其制备方法

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106958019A (zh) * 2017-04-05 2017-07-18 邢台三厦铸铁有限公司 铸铁炊具的表面处理方法及铸铁炊具

Also Published As

Publication number Publication date
EP2646513A1 (fr) 2013-10-09
CN103370379A (zh) 2013-10-23
BR112013013189A2 (pt) 2016-09-06
CN103370379B (zh) 2015-09-30
JP5931902B2 (ja) 2016-06-08
WO2012072953A1 (fr) 2012-06-07
FR2967924A1 (fr) 2012-06-01
US9862843B2 (en) 2018-01-09
KR20140000701A (ko) 2014-01-03
KR101650614B1 (ko) 2016-08-23
US20140034651A1 (en) 2014-02-06
CO6781479A2 (es) 2013-10-31
US20180086926A1 (en) 2018-03-29
JP2014503622A (ja) 2014-02-13

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