FR3087351B1 - Synthese hors equilibre haute et basse temperature par synthese spray flash - Google Patents

Synthese hors equilibre haute et basse temperature par synthese spray flash Download PDF

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Publication number
FR3087351B1
FR3087351B1 FR1859736A FR1859736A FR3087351B1 FR 3087351 B1 FR3087351 B1 FR 3087351B1 FR 1859736 A FR1859736 A FR 1859736A FR 1859736 A FR1859736 A FR 1859736A FR 3087351 B1 FR3087351 B1 FR 3087351B1
Authority
FR
France
Prior art keywords
synthesis
compound
low temperature
balance
temperature out
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1859736A
Other languages
English (en)
Other versions
FR3087351A1 (fr
Inventor
Denis Spitzer
Marc Comet
Valerie Keller
Martin Klaumunzer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Centre National de la Recherche Scientifique CNRS
Universite de Strasbourg
Institut Franco Allemand de Recherches de Saint Louis ISL
Original Assignee
Centre National de la Recherche Scientifique CNRS
Universite de Strasbourg
Institut Franco Allemand de Recherches de Saint Louis ISL
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Centre National de la Recherche Scientifique CNRS, Universite de Strasbourg, Institut Franco Allemand de Recherches de Saint Louis ISL filed Critical Centre National de la Recherche Scientifique CNRS
Priority to FR1859736A priority Critical patent/FR3087351B1/fr
Priority to US17/286,932 priority patent/US12251673B2/en
Priority to PCT/EP2019/078770 priority patent/WO2020083942A1/fr
Priority to EP19787305.2A priority patent/EP3870351A1/fr
Priority to JP2021546476A priority patent/JP7528104B2/ja
Publication of FR3087351A1 publication Critical patent/FR3087351A1/fr
Application granted granted Critical
Publication of FR3087351B1 publication Critical patent/FR3087351B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002—Nozzle-type elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/14—Production of inert gas mixtures; Use of inert gases in general
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B01J8/0055—Separating solid material from the gas/liquid stream using cyclones
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)

Abstract

L'invention concerne un procédé de synthèse chimique, ledit procédé comprenant une brumisation par évaporation flash, également connue sous le sigle SFE pour l'acronyme anglais « Spray Flash Evaporation », comprenant la réaction chimique d'au moins un premier composé avec au moins un deuxième composé, dans des conditions dans lesquelles le premier composé et le deuxième composé réagissent pour former au moins un troisième composé. L'invention concerne un dispositif de mise en œuvre de ce procédé et les composés obtenus par ce procédé.
FR1859736A 2018-10-22 2018-10-22 Synthese hors equilibre haute et basse temperature par synthese spray flash Active FR3087351B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR1859736A FR3087351B1 (fr) 2018-10-22 2018-10-22 Synthese hors equilibre haute et basse temperature par synthese spray flash
US17/286,932 US12251673B2 (en) 2018-10-22 2019-10-22 Synthesis outside high and low temperature equilibrium by spray flash synthesis
PCT/EP2019/078770 WO2020083942A1 (fr) 2018-10-22 2019-10-22 Synthèse hors équilibre haute et basse température par synthèse spray flash
EP19787305.2A EP3870351A1 (fr) 2018-10-22 2019-10-22 Synthèse hors équilibre haute et basse température par synthèse spray flash
JP2021546476A JP7528104B2 (ja) 2018-10-22 2019-10-22 スプレーフラッシュ合成による高温及び低温平衡外の合成

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1859736A FR3087351B1 (fr) 2018-10-22 2018-10-22 Synthese hors equilibre haute et basse temperature par synthese spray flash

Publications (2)

Publication Number Publication Date
FR3087351A1 FR3087351A1 (fr) 2020-04-24
FR3087351B1 true FR3087351B1 (fr) 2021-07-16

Family

ID=66530080

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1859736A Active FR3087351B1 (fr) 2018-10-22 2018-10-22 Synthese hors equilibre haute et basse temperature par synthese spray flash

Country Status (5)

Country Link
US (1) US12251673B2 (fr)
EP (1) EP3870351A1 (fr)
JP (1) JP7528104B2 (fr)
FR (1) FR3087351B1 (fr)
WO (1) WO2020083942A1 (fr)

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2048740A1 (fr) 1990-12-24 1992-06-25 John A. Deluca Methode d'application de films d'oxyde metallique
JP2005177662A (ja) 2003-12-22 2005-07-07 Hitachi Instruments Service Co Ltd フラッシュ蒸発を用いたナノ粒子生成方法およびその製造装置
ES2751337T3 (es) * 2012-02-07 2020-03-31 Centre Nat Rech Scient Procedimiento y dispositivo de preparación de nanopartículas por evaporación súbita
JP2014035809A (ja) 2012-08-07 2014-02-24 Dow Corning Toray Co Ltd 粒子の製造方法
FR3023177B1 (fr) 2014-07-04 2016-08-12 Centre Nat De La Rech Scient (C N R S) Procede de preparation de co-cristaux par evaporation flash
FR3061439A1 (fr) * 2016-09-20 2018-07-06 Centre National De La Recherche Scientifique Particules du type coeur-ecorce

Also Published As

Publication number Publication date
US20210354103A1 (en) 2021-11-18
WO2020083942A1 (fr) 2020-04-30
JP7528104B2 (ja) 2024-08-05
FR3087351A1 (fr) 2020-04-24
JP2022508902A (ja) 2022-01-19
US12251673B2 (en) 2025-03-18
EP3870351A1 (fr) 2021-09-01

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