FR3089134B1 - Procédé de préparation d’un matériau catalytique d’électrode pour des réactions de réduction électrochimique préparé par électroréduction. - Google Patents

Procédé de préparation d’un matériau catalytique d’électrode pour des réactions de réduction électrochimique préparé par électroréduction. Download PDF

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Publication number
FR3089134B1
FR3089134B1 FR1872181A FR1872181A FR3089134B1 FR 3089134 B1 FR3089134 B1 FR 3089134B1 FR 1872181 A FR1872181 A FR 1872181A FR 1872181 A FR1872181 A FR 1872181A FR 3089134 B1 FR3089134 B1 FR 3089134B1
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Prior art keywords
catalytic material
precursor
reduction reactions
electrochemical reduction
electroreduction
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FR1872181A
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FR3089134A1 (fr
Inventor
Audrey Bonduelle-Skrzypczak
Sofiane Belaid
David Pasquier
Emmanuelle Trela-Baudot
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IFP Energies Nouvelles IFPEN
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IFP Energies Nouvelles IFPEN
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Priority to FR1872181A priority Critical patent/FR3089134B1/fr
Priority to US17/295,775 priority patent/US20220018033A1/en
Priority to EP19806186.3A priority patent/EP3887572A1/fr
Priority to PCT/EP2019/081705 priority patent/WO2020109062A1/fr
Publication of FR3089134A1 publication Critical patent/FR3089134A1/fr
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    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/073—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
    • C25B11/091—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of at least one catalytic element and at least one catalytic compound; consisting of two or more catalytic elements or catalytic compounds
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/02—Hydrogen or oxygen
    • C25B1/04—Hydrogen or oxygen by electrolysis of water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/02—Hydrogen or oxygen
    • C25B1/04—Hydrogen or oxygen by electrolysis of water
    • C25B1/044—Hydrogen or oxygen by electrolysis of water producing mixed hydrogen and oxygen gas, e.g. Brown's gas [HHO]
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/27—Ammonia
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/055—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the substrate or carrier material
    • C25B11/057—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the substrate or carrier material consisting of a single element or compound
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/055—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the substrate or carrier material
    • C25B11/057—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the substrate or carrier material consisting of a single element or compound
    • C25B11/065—Carbon
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/073—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
    • C25B11/075—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of a single catalytic element or catalytic compound
    • C25B11/077—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of a single catalytic element or catalytic compound the compound being a non-noble metal oxide
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B13/00—Diaphragms; Spacing elements
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00—Electrolytic production of organic compounds
    • C25B3/01—Products
    • C25B3/07—Oxygen containing compounds
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/17—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
    • C25B9/19—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/9041—Metals or alloys
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/9075—Catalytic material supported on carriers, e.g. powder carriers
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/98—Raney-type electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/06—Combination of fuel cells with means for production of reactants or for treatment of residues
    • H01M8/0606—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants
    • H01M8/0656—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants by electrochemical means
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/133—Renewable energy sources, e.g. sunlight

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Sustainable Development (AREA)
  • Sustainable Energy (AREA)
  • Catalysts (AREA)
  • Inert Electrodes (AREA)

Abstract

Procédé de préparation d’un matériau catalytique d’une électrode pour des réactions de réduction électrochimique, ledit matériau comprenant au moins une phase active à base d’un métal du groupe VIB et un support électro-conducteur, lequel procédé comprend: a) une étape d’électrolyse d’au moins une solution aqueuse et/ou organique comprenant au moins un précurseur de la phase active comprenant au moins un métal du groupe VIB pour obtenir une solution comprenant au moins un précurseur comprenant au moins un métal du groupe VIB partiellement réduit ; b) une étape d’imprégnation dudit support avec ladite solution obtenue à l’étape a) pour obtenir un précurseur de matériau catalytique ; c) une étape de séchage dudit précurseur obtenu à l’étape b) à une température inférieure à 250°C, sans calcination ultérieure ; d) une étape de sulfuration du précurseur de matériau catalytique obtenu à l’étape c) à une température comprise entre 100°C et 600°C.
FR1872181A 2018-11-30 2018-11-30 Procédé de préparation d’un matériau catalytique d’électrode pour des réactions de réduction électrochimique préparé par électroréduction. Active FR3089134B1 (fr)

Priority Applications (4)

Application Number Priority Date Filing Date Title
FR1872181A FR3089134B1 (fr) 2018-11-30 2018-11-30 Procédé de préparation d’un matériau catalytique d’électrode pour des réactions de réduction électrochimique préparé par électroréduction.
US17/295,775 US20220018033A1 (en) 2018-11-30 2019-11-19 Method for preparing a catalytic material of an electrode for electrochemical reduction reactions prepared by electroreduction
EP19806186.3A EP3887572A1 (fr) 2018-11-30 2019-11-19 Procede de preparation d'un materiau catalytique d'electrode pour des reactions de reduction electrochimique prepare par electroreduction
PCT/EP2019/081705 WO2020109062A1 (fr) 2018-11-30 2019-11-19 Procede de preparation d'un materiau catalytique d'electrode pour des reactions de reduction electrochimique prepare par electroreduction

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1872181A FR3089134B1 (fr) 2018-11-30 2018-11-30 Procédé de préparation d’un matériau catalytique d’électrode pour des réactions de réduction électrochimique préparé par électroréduction.

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FR3089134A1 FR3089134A1 (fr) 2020-06-05
FR3089134B1 true FR3089134B1 (fr) 2020-11-13

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FR1872181A Active FR3089134B1 (fr) 2018-11-30 2018-11-30 Procédé de préparation d’un matériau catalytique d’électrode pour des réactions de réduction électrochimique préparé par électroréduction.

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US (1) US20220018033A1 (fr)
EP (1) EP3887572A1 (fr)
FR (1) FR3089134B1 (fr)
WO (1) WO2020109062A1 (fr)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115039260A (zh) * 2020-03-23 2022-09-09 恩亿凯嘉股份有限公司 电极用催化剂的制造系统和制造方法
CN113755879B (zh) * 2021-09-06 2023-03-14 无锡隆基氢能科技有限公司 一种δ相氮化钨电极材料及其制备方法和应用
FR3133544B1 (fr) 2022-03-18 2024-03-08 Ifp Energies Now Matériau catalytique à base d’un élément du groupe VIB et d’un élément du groupe IVB pour la production d’hydrogène par électrolyse de l’eau
CN117085683A (zh) * 2022-05-13 2023-11-21 天津大学 一种二维钴掺杂碳纳米片催化剂的制备方法和应用
CN114908375B (zh) * 2022-05-25 2024-08-13 中国科学技术大学 电催化co2还原中具有稳定活性位点的铜催化剂及其制备方法与应用
CN115821294B (zh) * 2022-11-17 2025-03-11 河南省高新技术实业有限公司 一种碳材催化电极材料及其制备方法和应用
FR3162052A1 (fr) 2024-05-13 2025-11-14 IFP Energies Nouvelles Procédé de préparation d’une électrode activée électrochimiquement à base de MoS2 fluoré pour des réactions de réduction électrochimique
FR3162008A1 (fr) 2024-05-13 2025-11-14 IFP Energies Nouvelles Procédé de préparation d’une couche active d’électrode à base de MoS2 fluoré pour des réactions de réduction électrochimique
CN119657232B (zh) * 2025-01-01 2025-11-04 南通大学 一种表面羟基化铂镍双金属海水制氢催化剂的制备方法及应用
CN120400894B (zh) * 2025-06-30 2025-10-17 西湖大学 一种电化学催化剂及其制备方法和应用

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US2547380A (en) 1945-10-01 1951-04-03 Union Oil Co Catalyst for hydrocarbon conversion
JP5732470B2 (ja) * 2009-12-16 2015-06-10 イエフペ エネルジ ヌヴェルＩｆｐ Ｅｎｅｒｇｉｅｓ Ｎｏｕｖｅｌｌｅｓ 第ｖｉｉｉ族および第ｖｉｂ族金属を含み、酢酸およびｃ１−ｃ４ジアルキルスクシナートを有する、水素化処理において使用可能な触媒および調製
JP5802085B2 (ja) * 2011-08-31 2015-10-28 株式会社バンテック アルカリ水電解用電極の製造方法
FR2984763B1 (fr) * 2011-12-22 2013-12-20 IFP Energies Nouvelles Procede de preparation d'un catalyseur utilisable en hydroconversion comprenant au moins une zeolithe nu-86
FR3004967B1 (fr) * 2013-04-30 2016-12-30 Ifp Energies Now Procede de preparation d'un catalyseur a base de molybdene utilisable en hydrotraitement ou en hydrocraquage
FR3004968B1 (fr) * 2013-04-30 2016-02-05 IFP Energies Nouvelles Procede de preparation d'un catalyseur a base de tungstene utilisable en hydrotraitement ou en hydrocraquage
FR3007427B1 (fr) 2013-06-20 2016-07-01 Ifp Energies Now Couche active a base de particules metalliques sur support conducteur poreux, methode de fabrication et utilisation en tant que cathode pour l'electroreduction de dioxyde de carbone.
CN106917105B (zh) * 2017-01-13 2019-05-31 太原理工大学 一种水分解用自支撑过渡金属硫化物泡沫电极的制备方法
JP6315532B1 (ja) * 2017-07-18 2018-04-25 国立大学法人弘前大学 電極触媒の製造方法及び水素の製造方法
KR101894964B1 (ko) * 2017-08-08 2018-09-05 한국과학기술원 그래핀 액정섬유-전이금속계 촉매 섬유복합체 및 이의 제조방법
FR3075664A1 (fr) * 2017-12-22 2019-06-28 IFP Energies Nouvelles Catalyseur d'hydrotraitement et/ou d'hydrocraquage prepare par electroreduction
CN108855146B (zh) * 2018-06-27 2020-05-05 北京师范大学 NiFeMoS复合体及其制备方法

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Publication number Publication date
FR3089134A1 (fr) 2020-06-05
WO2020109062A1 (fr) 2020-06-04
EP3887572A1 (fr) 2021-10-06
US20220018033A1 (en) 2022-01-20

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