FR3097863B1 - Séparation en phase liquide des sucres 2G par adsorption sur une zéolithe de type FAU de ratio atomique Si/Al supérieur à 1,5 - Google Patents

Séparation en phase liquide des sucres 2G par adsorption sur une zéolithe de type FAU de ratio atomique Si/Al supérieur à 1,5 Download PDF

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Publication number
FR3097863B1
FR3097863B1 FR1907089A FR1907089A FR3097863B1 FR 3097863 B1 FR3097863 B1 FR 3097863B1 FR 1907089 A FR1907089 A FR 1907089A FR 1907089 A FR1907089 A FR 1907089A FR 3097863 B1 FR3097863 B1 FR 3097863B1
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France
Prior art keywords
liquid phase
glucose
sugars
adsorption
atomic ratio
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FR1907089A
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English (en)
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FR3097863A1 (fr
Inventor
Catherine Laroche
Maria Manko
Emmanuelle BRACCO
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IFP Energies Nouvelles IFPEN
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IFP Energies Nouvelles IFPEN
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Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to FR1907089A priority Critical patent/FR3097863B1/fr
Priority to PCT/EP2020/066154 priority patent/WO2020260027A1/fr
Priority to EP20732833.7A priority patent/EP3990464A1/fr
Priority to US17/621,987 priority patent/US20220242895A1/en
Priority to BR112021020811A priority patent/BR112021020811A2/pt
Publication of FR3097863A1 publication Critical patent/FR3097863A1/fr
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Publication of FR3097863B1 publication Critical patent/FR3097863B1/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/265—Adsorption chromatography
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
    • C07H3/02—Monosaccharides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/185—Simulated moving beds characterised by the components to be separated

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Sustainable Development (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

L’invention concerne un procédé de séparation du glucose en phase liquide à partir d’un mélange de sucres en C5 et C6 comprenant au moins du xylose et du glucose, par adsorption du glucose sur un adsorbant zéolithique à base de cristaux de zéolithe de type FAU de ratio atomique Si/Al strictement supérieur à 1,5 comprenant du baryum, dans lequel :-on met en contact ledit mélange avec ledit adsorbant, en chromatographie liquide, pour obtenir une phase liquide enrichie en xylose et une phase adsorbée enrichie en glucose ;-on récupère d’une part ladite phase liquide enrichie en xylose et on désorbe au moyen d’un solvant de désorption ladite phase adsorbée sur ledit adsorbant pour récupérer d’autre part le glucose. Figure à publier : néant
FR1907089A 2019-06-28 2019-06-28 Séparation en phase liquide des sucres 2G par adsorption sur une zéolithe de type FAU de ratio atomique Si/Al supérieur à 1,5 Active FR3097863B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR1907089A FR3097863B1 (fr) 2019-06-28 2019-06-28 Séparation en phase liquide des sucres 2G par adsorption sur une zéolithe de type FAU de ratio atomique Si/Al supérieur à 1,5
PCT/EP2020/066154 WO2020260027A1 (fr) 2019-06-28 2020-06-11 Séparation en phase liquide des sucres 2g par adsorption sur une zéolithe de type fau de ratio atomique si/al supérieur à 1,5
EP20732833.7A EP3990464A1 (fr) 2019-06-28 2020-06-11 Séparation en phase liquide des sucres 2g par adsorption sur une zéolithe de type fau de ratio atomique si/al supérieur à 1,5
US17/621,987 US20220242895A1 (en) 2019-06-28 2020-06-11 Liquid phase separation of 2g sugars by adsorption on a fau zeolite having a si/al atomic ratio greater than 1.5
BR112021020811A BR112021020811A2 (pt) 2019-06-28 2020-06-11 Separação em fase líquida de açúcares 2g por adsorção sobre um zeólito do tipo fau de razão atômica si/al superior a 1,5

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1907089A FR3097863B1 (fr) 2019-06-28 2019-06-28 Séparation en phase liquide des sucres 2G par adsorption sur une zéolithe de type FAU de ratio atomique Si/Al supérieur à 1,5
FR1907089 2019-06-28

Publications (2)

Publication Number Publication Date
FR3097863A1 FR3097863A1 (fr) 2021-01-01
FR3097863B1 true FR3097863B1 (fr) 2023-04-14

Family

ID=67515005

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1907089A Active FR3097863B1 (fr) 2019-06-28 2019-06-28 Séparation en phase liquide des sucres 2G par adsorption sur une zéolithe de type FAU de ratio atomique Si/Al supérieur à 1,5

Country Status (5)

Country Link
US (1) US20220242895A1 (fr)
EP (1) EP3990464A1 (fr)
BR (1) BR112021020811A2 (fr)
FR (1) FR3097863B1 (fr)
WO (1) WO2020260027A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3142492A1 (fr) 2022-11-28 2024-05-31 IFP Energies Nouvelles Procédé de traitement d’un mélange en phase aqueuse de composés comprenant des sucres à 5 et 6 atomes de carbone.
FR3144994A1 (fr) 2023-01-18 2024-07-19 IFP Energies Nouvelles Procédé de traitement d’une biomasse lignocellulosique

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2882244A (en) 1953-12-24 1959-04-14 Union Carbide Corp Molecular sieve adsorbents
US3130007A (en) 1961-05-12 1964-04-21 Union Carbide Corp Crystalline zeolite y
US4340724A (en) 1976-05-27 1982-07-20 Uop Inc. Process for separating a ketose from an aldose by selective adsorption
ZA774573B (en) * 1976-08-02 1978-06-28 Uop Inc Process for separating a monosaccharide from an oligosaccharide by selective adsorption
JPS5326336A (en) 1976-08-24 1978-03-11 Toray Industries Method of fractional absorption for saccharides
US4293346A (en) 1979-11-05 1981-10-06 Uop Inc. Simulated countercurrent sorption process employing ion exchange resins with backflushing
US4516566A (en) * 1982-12-30 1985-05-14 Union Carbide Corporation Separation of arabinose by selective adsorption on zeolitic molecular sieves
CA2454823A1 (fr) * 2001-07-24 2003-02-06 Arkenol, Inc. Separation du xylose et du glucose
EP3230480B1 (fr) * 2014-12-09 2018-10-03 BIOeCON International Holding N.V. Procédé d'isolement de monosaccharides
FR3038528B1 (fr) * 2015-07-09 2020-10-23 Ifp Energies Now Adsorbants zeolithiques, leur procede de preparation et leurs utilisations

Also Published As

Publication number Publication date
US20220242895A1 (en) 2022-08-04
WO2020260027A1 (fr) 2020-12-30
FR3097863A1 (fr) 2021-01-01
EP3990464A1 (fr) 2022-05-04
BR112021020811A2 (pt) 2022-01-18

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