FR3135979B1 - Procede de separation de l’acide levulinique par separation thermique en presence d’un fluxant - Google Patents

Procede de separation de l’acide levulinique par separation thermique en presence d’un fluxant Download PDF

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Publication number
FR3135979B1
FR3135979B1 FR2205179A FR2205179A FR3135979B1 FR 3135979 B1 FR3135979 B1 FR 3135979B1 FR 2205179 A FR2205179 A FR 2205179A FR 2205179 A FR2205179 A FR 2205179A FR 3135979 B1 FR3135979 B1 FR 3135979B1
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FR
France
Prior art keywords
flux
levulinic acid
separating
acid
thermal separation
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2205179A
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English (en)
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FR3135979A1 (fr
Inventor
Pierre-Alain Breuil
Espada Pastor Maria Fernandez
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IFP Energies Nouvelles IFPEN
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IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to FR2205179A priority Critical patent/FR3135979B1/fr
Priority to PCT/EP2023/062613 priority patent/WO2023232426A1/fr
Priority to US18/869,545 priority patent/US20250296908A1/en
Publication of FR3135979A1 publication Critical patent/FR3135979A1/fr
Application granted granted Critical
Publication of FR3135979B1 publication Critical patent/FR3135979B1/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La présente invention concerne un procédé de séparation d’acide lévulinique à partir d'une composition comprenant de l'acide lévulinique et des humines dans lequel on soumet ladite composition à une étape de séparation thermique en présence d’un fluxant ayant un point d’ébullition supérieur à celui de l’acide lévulinique de manière à obtenir une fraction légère contenant l’acide lévulinique et une fraction lourde contenant les humines et ledit fluxant. La présence d’un fluxant permet de réduire la viscosité des humines et d’augmenter le taux de récupération de l’acide lévulinique.
FR2205179A 2022-05-31 2022-05-31 Procede de separation de l’acide levulinique par separation thermique en presence d’un fluxant Active FR3135979B1 (fr)

Priority Applications (3)

Application Number Priority Date Filing Date Title
FR2205179A FR3135979B1 (fr) 2022-05-31 2022-05-31 Procede de separation de l’acide levulinique par separation thermique en presence d’un fluxant
PCT/EP2023/062613 WO2023232426A1 (fr) 2022-05-31 2023-05-11 Procede de separation de l'acide levulinique par separation thermique en presence d'un fluxant
US18/869,545 US20250296908A1 (en) 2022-05-31 2023-05-11 Method for separating levulinic acid by thermal separation in the presence of a flux

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2205179A FR3135979B1 (fr) 2022-05-31 2022-05-31 Procede de separation de l’acide levulinique par separation thermique en presence d’un fluxant
FR2205179 2022-05-31

Publications (2)

Publication Number Publication Date
FR3135979A1 FR3135979A1 (fr) 2023-12-01
FR3135979B1 true FR3135979B1 (fr) 2024-04-26

Family

ID=82319780

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2205179A Active FR3135979B1 (fr) 2022-05-31 2022-05-31 Procede de separation de l’acide levulinique par separation thermique en presence d’un fluxant

Country Status (3)

Country Link
US (1) US20250296908A1 (fr)
FR (1) FR3135979B1 (fr)
WO (1) WO2023232426A1 (fr)

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2780588A (en) 1954-12-08 1957-02-05 Quaker Oats Co Stabilization of levulinic acid
US3752849A (en) 1970-03-18 1973-08-14 Otsuka Kagaku Yakuhin Manufacture of levulinic acid
FR2640263B1 (fr) 1988-12-09 1991-06-14 Organo Synthese Ste Fse Preparation d'acide levulinique
CN103209951B (zh) 2010-11-11 2016-04-20 赛格提斯公司 酮基羧酸、酮基羧酸酯、其制造和使用方法
US8389761B2 (en) 2011-05-25 2013-03-05 Wisconsin Alumni Research Foundation Method to produce and recover levulinic acid and/or gamma-valerolactone from aqueous solutions using alkylphenols
MX2016000623A (es) 2013-07-17 2016-05-26 Dsm Ip Assets Bv Proceso para aislar acido levulinico.
CN107867996B (zh) 2016-09-23 2021-02-09 中国石油化工股份有限公司 乙酰丙酸类化合物的分离方法
IT201700068744A1 (it) 2017-06-21 2018-12-21 Bio On Spa Processo per la produzione di acido levulinico.

Also Published As

Publication number Publication date
WO2023232426A1 (fr) 2023-12-07
US20250296908A1 (en) 2025-09-25
FR3135979A1 (fr) 2023-12-01

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