GR1003453B - Μεθοδος παραγωγης κοκκωδους θειικου αμμωνιου - Google Patents
Μεθοδος παραγωγης κοκκωδους θειικου αμμωνιουInfo
- Publication number
- GR1003453B GR1003453B GR990100232A GR990100232A GR1003453B GR 1003453 B GR1003453 B GR 1003453B GR 990100232 A GR990100232 A GR 990100232A GR 990100232 A GR990100232 A GR 990100232A GR 1003453 B GR1003453 B GR 1003453B
- Authority
- GR
- Greece
- Prior art keywords
- production
- fertilisers
- reaction tank
- tubular reactor
- ordinary
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C3/00—Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/24—Sulfates of ammonium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/24—Sulfates of ammonium
- C01C1/242—Preparation from ammonia and sulfuric acid or sulfur trioxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/24—Sulfates of ammonium
- C01C1/248—Preventing coalescing or controlling form or size of the crystals
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/20—Powder free flowing behaviour
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Μία νέα μέθοδος για την παραγωγή κοκκώδους θειϊκού αμμωνίου, το οποίο ρέει ελεύθερα και δεν συσσωματώνεται, με τίτλο κατ'ελάχιστον 20,5 % και με κοκκομετρική σύσταση και σκληρότητα όμοια των κοινών κοκκωδών λιπασμάτων.Η μέθοδος χαρακτηρίζεται από τον συνδυασμό της κλασσικής δεξαμενής αντίδρασης και του αυλωτού αντιδραστήρα (χωρίς να στερεί την δυνατότητα χρήσης ενός εκάστου εξ αυτών). Γίνεται χρήση θειϊκού οξέος, υγρής ή αέριας αμμωνίας και νερών πλύσης των απαερίων της αντίδρασης. Ο παραγόμενος πολτός στην δεξαμενή αντίδρασης και στον αυλωτό αντιδραστήρα έχει τις κατάλληλες συνθήκες θερμοκρασίας, πίεσης, υγρασίας, πυκνότητας και pH, έτσι ώστε εισερχόμενος σε κοκκοποιητή να μετατρέπεται σε κόκκους της επιθυμητής κοκκομετρίας και σκληρότητας. Σημασία για την επιτυχία της μεθόδους έχει η κατανομή της τροφοδοσίας των πρώτων υλών και του νερού στα δύο στάδια της παραγωγής.Η μέθοδος χρησιμοποιείται για την παραγωγή λιπάσματος με υψηλό ρυθμό, με καλά χαρακτηριστικά ποιότητας και ελαχιστοποίηση επίδρασης στο περιβάλλον.ΰ
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GR99100232 | 1999-07-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GR1003453B true GR1003453B (el) | 2000-10-12 |
Family
ID=10943870
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GR990100232A GR1003453B (el) | 1999-07-07 | 1999-07-07 | Μεθοδος παραγωγης κοκκωδους θειικου αμμωνιου |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP1067093B1 (el) |
| AT (1) | ATE284841T1 (el) |
| DE (1) | DE60016673T2 (el) |
| ES (1) | ES2234551T3 (el) |
| GR (1) | GR1003453B (el) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7258848B1 (en) | 2006-07-31 | 2007-08-21 | E. I. Du Pont De Nemours And Company | Process for scrubbing ammonia from acid gases comprising ammonia and hydrogen sulfide |
| CN101850989B (zh) * | 2009-04-02 | 2013-01-16 | 河北天人化工股份有限公司 | 一种大颗粒硫酸铵的制备方法 |
| CN102328936B (zh) * | 2011-09-07 | 2012-11-21 | 四川明晶光电科技有限公司 | 一种处理氨气废水的方法 |
| CN103395803A (zh) * | 2013-08-01 | 2013-11-20 | 瓮福(集团)有限责任公司 | 一种粉状硫酸铵的生产方法 |
| US8974763B1 (en) | 2013-12-18 | 2015-03-10 | Rentech, Inc. | System and method for production of granular ammonium sulfate |
| CN103664300B (zh) * | 2013-12-20 | 2016-02-17 | 青海云天化国际化肥有限公司 | 氨酸法转鼓喷浆造粒生产颗粒合成硫铵的方法 |
| EP4474370A3 (en) | 2014-05-05 | 2025-02-19 | SABIC Global Technologies B.V. | Coated granular fertilizers, methods of manufacture thereof, and uses |
| CN104446754A (zh) * | 2014-11-10 | 2015-03-25 | 瓮福(集团)有限责任公司 | 一种高硫元素硫铵的生产方法 |
| RU2618763C2 (ru) * | 2015-03-10 | 2017-05-11 | Акционерное общество "Научно-исследовательский институт по удобрениям и инсектофунгицидам имени профессора Я.В. Самойлова" (АО "НИУИФ") | Способ получения гранулированного сульфата аммония |
| US11104618B2 (en) | 2015-07-20 | 2021-08-31 | Sabic Global Technologies B.V. | Fertilizer composition and methods of making and using same |
| WO2017087265A1 (en) | 2015-11-16 | 2017-05-26 | Sabic Global Technologies B.V. | Methods of manufacture for coated granular fertilizers |
| EP3377461B1 (en) | 2015-11-16 | 2025-08-06 | Sabic Agri-Nutrients Company | Coated granular fertilizers, methods of manufacture thereof, and uses thereof |
| EP3414214A1 (en) | 2016-02-08 | 2018-12-19 | SABIC Global Technologies B.V. | Method of making a fertilizer seed core |
| WO2018193344A1 (en) | 2017-04-19 | 2018-10-25 | Sabic Global Technologies B.V. | Enhanced efficiency fertilizer with urease inhibitor and nitrification inhibitor separated within the same particle |
| EP3612508B1 (en) | 2017-04-19 | 2026-01-28 | Sabic Agri-Nutrients Company | Enhanced efficiency fertilizer with urease inhibitor and nitrification inhibitor in separate particles |
| US11345645B2 (en) | 2017-04-20 | 2022-05-31 | Sabic Global Technologies B.V. | Enhanced efficiency fertilizer with embedded powder composition |
| US11021409B2 (en) | 2017-08-09 | 2021-06-01 | Sabic Global Technologies B.V. | Extruded fertilizer granules with urease and/or nitrification inhibitors |
| CN115367795B (zh) * | 2022-09-01 | 2024-02-20 | 山东东佳集团股份有限公司 | 催化剂钛白粉水洗液回用于制酸尾气系统制备硫酸铵的新工艺 |
| CN116768235A (zh) * | 2023-06-15 | 2023-09-19 | 山东省冶金设计院股份有限公司 | 一种硫酸铵生产系统及方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3351455A (en) * | 1964-08-28 | 1967-11-07 | Arizona Agrochemical Corp | Ammonium sulfate-ammonium bisulfate fertilizer and method of making |
| US3464809A (en) * | 1966-07-14 | 1969-09-02 | Tennessee Valley Authority | Process for production of granular ammonium sulfate |
| GB2116159A (en) * | 1982-02-20 | 1983-09-21 | Toyo Engineering Corp | A process for manufacturing granular compound fertilizers |
| WO1993019826A1 (en) * | 1992-03-27 | 1993-10-14 | Allied-Signal Inc. | Process for crystallization in a draft tube baffle crystallizer |
-
1999
- 1999-07-07 GR GR990100232A patent/GR1003453B/el not_active IP Right Cessation
-
2000
- 2000-07-07 DE DE60016673T patent/DE60016673T2/de not_active Expired - Lifetime
- 2000-07-07 ES ES00600009T patent/ES2234551T3/es not_active Expired - Lifetime
- 2000-07-07 AT AT00600009T patent/ATE284841T1/de not_active IP Right Cessation
- 2000-07-07 EP EP00600009A patent/EP1067093B1/en not_active Expired - Lifetime
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3351455A (en) * | 1964-08-28 | 1967-11-07 | Arizona Agrochemical Corp | Ammonium sulfate-ammonium bisulfate fertilizer and method of making |
| US3464809A (en) * | 1966-07-14 | 1969-09-02 | Tennessee Valley Authority | Process for production of granular ammonium sulfate |
| GB2116159A (en) * | 1982-02-20 | 1983-09-21 | Toyo Engineering Corp | A process for manufacturing granular compound fertilizers |
| WO1993019826A1 (en) * | 1992-03-27 | 1993-10-14 | Allied-Signal Inc. | Process for crystallization in a draft tube baffle crystallizer |
Non-Patent Citations (1)
| Title |
|---|
| ED. H.J. ARPE: "Ullmann's encyclopedia of industrial chemistry, 4th Edition, volume 7, pages 514 and 521-525", 1974, VCH-VERLAG, WEINHEIM (DE), XP002132376 * |
Also Published As
| Publication number | Publication date |
|---|---|
| DE60016673D1 (de) | 2005-01-20 |
| ATE284841T1 (de) | 2005-01-15 |
| ES2234551T3 (es) | 2005-07-01 |
| DE60016673T2 (de) | 2005-12-08 |
| EP1067093B1 (en) | 2004-12-15 |
| EP1067093A1 (en) | 2001-01-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ML | Lapse due to non-payment of fees |
Effective date: 20140204 |