IE32406L - Production of ammonium thiocyanate - Google Patents
Production of ammonium thiocyanateInfo
- Publication number
- IE32406L IE32406L IE118768A IE118768A IE32406L IE 32406 L IE32406 L IE 32406L IE 118768 A IE118768 A IE 118768A IE 118768 A IE118768 A IE 118768A IE 32406 L IE32406 L IE 32406L
- Authority
- IE
- Ireland
- Prior art keywords
- reaction tube
- reaction
- ammonium thiocyanate
- ammonia
- carbon disulphide
- Prior art date
Links
- SOIFLUNRINLCBN-UHFFFAOYSA-N ammonium thiocyanate Chemical compound [NH4+].[S-]C#N SOIFLUNRINLCBN-UHFFFAOYSA-N 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 abstract 10
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 8
- 229910021529 ammonia Inorganic materials 0.000 abstract 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 3
- 229910052799 carbon Inorganic materials 0.000 abstract 3
- 238000004821 distillation Methods 0.000 abstract 3
- 239000003513 alkali Substances 0.000 abstract 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 abstract 1
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 abstract 1
- -1 alkaline earth metal thiocyanates Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000003567 thiocyanates Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C3/00—Cyanogen; Compounds thereof
- C01C3/20—Thiocyanic acid; Salts thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Water Treatment By Sorption (AREA)
- Industrial Gases (AREA)
- Gas Separation By Absorption (AREA)
- Treating Waste Gases (AREA)
Abstract
1,232,310. Production of aqueous solutions of thiocyanates. GLANZSTOFF A.G. 1 Oct., 1968 [21 Oct., 1967 (3)], No. 46488/68. Heading C1A. Aqueous ammonium thiocyanate solutions are obtained by the reaction of ammonia and carbon disulphide in the presence of water, the reaction being carried out on active carbon at elevated temperature. The process is suitably effected in a reaction tube filled with granulated active carbon, a temperature of 60-100 C. being maintained in the reaction zone. In one mode of operation, ammonia and carbon disulphide in a molar ratio from 2:1À2 to 2: 2 are introduced between one quarter and one half the way up the reaction tube filled with granulated active carbon which is mounted on a distillation vessel, and simultaneously steam is supplied from the bottom of the reaction tube from a distillation vessel, the control of the heat supply to the distillation vessel being so effected that the major part of the steam condenses below the point at which ammonia and carbon disulphide are fed to the reaction tube, and the ammonium thiocyanate formed is drawn off at the bottom end of the reaction tube and hydrogen sulphide as well as excess carbon disulphide are drawn off from the top of the reaction tube. The ammonium thiocyanate may alternatively be converted to aqueous alkali or alkaline earth metal thiocyanates by providing an aqueous alkali or alkaline earth metal hydroxide solution in the reaction tube between the points of entry of the steam and the ammonia and carbon disulphide for reaction with the ammonium thiocyanate passing therethrough.
[GB1232310A]
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEG51396A DE1297088B (en) | 1967-10-21 | 1967-10-21 | Process for the production of aqueous ammonium rhodanide solutions |
| DEG0051397 | 1967-10-21 | ||
| DEG0051395 | 1967-10-21 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IE32406L true IE32406L (en) | 1969-04-21 |
| IE32406B1 IE32406B1 (en) | 1973-07-25 |
Family
ID=27210681
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IE118768A IE32406B1 (en) | 1967-10-21 | 1968-10-04 | Process for the production of aqueous ammonium thiocyanate solutions |
Country Status (13)
| Country | Link |
|---|---|
| BE (1) | BE721304A (en) |
| CH (1) | CH495287A (en) |
| CS (1) | CS149643B2 (en) |
| DE (3) | DE1592339B2 (en) |
| FI (1) | FI47082C (en) |
| FR (1) | FR1587154A (en) |
| GB (1) | GB1232310A (en) |
| IE (1) | IE32406B1 (en) |
| LU (1) | LU56978A1 (en) |
| NL (1) | NL156374B (en) |
| NO (1) | NO118270B (en) |
| SE (1) | SE328858B (en) |
| YU (1) | YU33004B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3508404A1 (en) * | 1985-03-08 | 1986-09-18 | Akzo Gmbh, 5600 Wuppertal | METHOD FOR PRODUCING AQUEOUS AMMONIUM RHODANIDE SOLUTIONS |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2249962A (en) * | 1940-01-27 | 1941-07-22 | American Cyanamid Co | Preparation of ammonium thiocyanate |
| US2850356A (en) * | 1956-07-23 | 1958-09-02 | American Cyanamid Co | Ammonium thiocyanate manufacture |
-
1967
- 1967-10-21 DE DE19671592339 patent/DE1592339B2/en not_active Withdrawn
- 1967-10-21 DE DEG51396A patent/DE1297088B/en active Pending
- 1967-10-21 DE DE19671592341 patent/DE1592341B1/en not_active Withdrawn
-
1968
- 1968-09-24 BE BE721304D patent/BE721304A/xx not_active IP Right Cessation
- 1968-09-25 CH CH1442268A patent/CH495287A/en not_active IP Right Cessation
- 1968-09-27 CS CS676468A patent/CS149643B2/cs unknown
- 1968-09-27 LU LU56978D patent/LU56978A1/xx unknown
- 1968-09-27 FI FI274468A patent/FI47082C/en active
- 1968-09-30 NO NO386468A patent/NO118270B/no unknown
- 1968-10-01 GB GB1232310D patent/GB1232310A/en not_active Expired
- 1968-10-04 YU YU232168A patent/YU33004B/en unknown
- 1968-10-04 IE IE118768A patent/IE32406B1/en unknown
- 1968-10-08 SE SE1355868A patent/SE328858B/xx unknown
- 1968-10-18 FR FR1587154D patent/FR1587154A/fr not_active Expired
- 1968-10-18 NL NL6814939A patent/NL156374B/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| IE32406B1 (en) | 1973-07-25 |
| NO118270B (en) | 1969-12-08 |
| BE721304A (en) | 1969-03-03 |
| NL6814939A (en) | 1969-04-23 |
| DE1592339A1 (en) | 1970-12-10 |
| YU33004B (en) | 1976-03-31 |
| NL156374B (en) | 1978-04-17 |
| CS149643B2 (en) | 1973-07-25 |
| DE1297088B (en) | 1969-06-12 |
| YU232168A (en) | 1975-08-31 |
| CH495287A (en) | 1970-08-31 |
| FI47082B (en) | 1973-05-31 |
| FR1587154A (en) | 1970-03-13 |
| LU56978A1 (en) | 1969-01-08 |
| SE328858B (en) | 1970-09-28 |
| GB1232310A (en) | 1971-05-19 |
| DE1592341B1 (en) | 1969-12-11 |
| FI47082C (en) | 1973-09-10 |
| DE1592339B2 (en) | 1975-08-21 |
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