IE40821L - Antibiotic 67-121 from actinoplanes caeruleus - Google Patents

Antibiotic 67-121 from actinoplanes caeruleus

Info

Publication number
IE40821L
IE40821L IE750491A IE49175A IE40821L IE 40821 L IE40821 L IE 40821L IE 750491 A IE750491 A IE 750491A IE 49175 A IE49175 A IE 49175A IE 40821 L IE40821 L IE 40821L
Authority
IE
Ireland
Prior art keywords
antibiotic
maxima
complex
absorption maxima
free form
Prior art date
Application number
IE750491A
Other versions
IE40821B1 (en
Original Assignee
Scherico Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Scherico Ltd filed Critical Scherico Ltd
Publication of IE40821L publication Critical patent/IE40821L/en
Publication of IE40821B1 publication Critical patent/IE40821B1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H17/00Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
    • C07H17/04Heterocyclic radicals containing only oxygen as ring hetero atoms
    • C07H17/08Hetero rings containing eight or more ring members, e.g. erythromycins
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07GCOMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G11/00Antibiotics

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

1474879 Antibiotic complex SCHERICO Ltd 6 March 1975 [11 March 1974] 9392/75 Heading C2A The invention is directed to a polyene antibiotic complex designated 67-121 complex, in free form or in the form of a pharmaceutically acceptable derivative. The complex in the free form has the following characteristics; ultraviolet absorption maxima in methanol at 342, 363, 382 and 403 mÁ with corresponding E<SP>1%</SP> 1cm values of 340, 475, 667 and 605, infra-red absorption maxima in mineral oil at 3350, 1725 and 1665 cm<SP>-1</SP> and nuclear magnetic resonance spectra in hexa-deutero-dimethylsulfoxide with maxima at 2À75, 6À56 and 7À64 p.p.m. The complex comprises antibiotic components 67- 121A, 67-121B, 67-121C and 67-121D. The complex or a component antibiotic thereof may be prepared by cultivating a microorganism of the species Actinoplanes coerulus in a nutrient medium under aerobic conditions until substantial antibiotic activity is generated. The preferred microoganism is the strain Actinoplanes coeruleus NRRL 5325. Antibiotic 67-121A, in the free form has the following characteristics, ultra-violet absorption maxima in a 4 : 1 tetrahydrofuran : water mixture of 408, 384 and 363 mÁ with corresponding E<SP>1%</SP> 1cm values of 950, 1100 and 680; infra-red absorption maxima in mineral oil at 3350, 1725 and 1665 cm<SP>-1</SP> and a nuclear magnetic resonance spectrum in hexa-deutero-dimethylsulphoxide with maxima at 2À73, 6À55 and 7À64 p.p.m. Antibiotic 67-121B, in the free form has the following characteristics ultra-violet absorption maxima in a 4 : 1 tetra hydrofuran : water mixture of 408, 383 and 362 mÁ with corresponding E<SP>1%</SP> 1cm values of 620, 750 and 490; infra-red absorption maxima in mineral oil at 3350, 1725 and 1665 cm<SP>-1</SP> and a nuclear magnetic resonance spectrum in hexa-deutro dimethylsulphoxide with maxima at 6À58 and 7À60 p.p.m. Antibiotic 67-121C, in the free form has the following characteristics, ultraviolet absorption maxima in 4 : 1 tetrahydrofuran : water mixture of 408, 383 and 362 mÁ with corresponding E<SP>1%</SP> 1cm value of 800, 910 and 600; infra-red absorption maxima in mineral oil at 3350, 1725 and 1665 cm<SP>-1</SP> and a nuclear magnetic resonance spectrum in hexa-deutero dimethylsulphoxide with maxima at 2À76, 6À57 and 7À65 p.p.m. The polyene antibiotics are further characterized as a heptaene subgroup II antibiotic and having an aromatic moiety of the formula in which for antibiotics 67-121A and C, R is methyl and/or antibiotic 67-121B, R is H. The antibiotics 67-121A and 67-121B are further characterized by a presence of a D- mycosamine sugar unit glycosidically attached to an allylic hydroxy group of the aglycone structure and antibiotic 67-121C is further characterized by the presence of the disaccharide unit [O-#-D-mannopyranosyl(1#4)-D- mycosamine]glycosidically attached to an allylic hydroxy group of the aglycore structure. The complex or components may be in a free form or in the form of a pharmaceutically acceptable derivative. The antibiotic substances may be admixed with a suitable pharmaceutically acceptable carrier. The antibiotic substance may be administered to animals having a fungal infection to elicit an anti-fungal response therefrom. [GB1474879A]
IE491/75A 1974-03-11 1975-03-06 Antibiotic 67-121 and process for the preparation thereof IE40821B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US45004074A 1974-03-11 1974-03-11

Publications (2)

Publication Number Publication Date
IE40821L true IE40821L (en) 1975-09-11
IE40821B1 IE40821B1 (en) 1979-08-29

Family

ID=23786522

Family Applications (1)

Application Number Title Priority Date Filing Date
IE491/75A IE40821B1 (en) 1974-03-11 1975-03-06 Antibiotic 67-121 and process for the preparation thereof

Country Status (9)

Country Link
JP (1) JPS50121496A (en)
BG (1) BG26542A3 (en)
DE (1) DE2509782A1 (en)
FR (1) FR2263782B1 (en)
GB (1) GB1474879A (en)
HU (1) HU175177B (en)
IE (1) IE40821B1 (en)
NL (1) NL7502666A (en)
SE (1) SE7502535L (en)

Also Published As

Publication number Publication date
FR2263782A1 (en) 1975-10-10
IE40821B1 (en) 1979-08-29
SE7502535L (en) 1975-10-03
JPS50121496A (en) 1975-09-23
NL7502666A (en) 1975-09-15
HU175177B (en) 1980-05-28
FR2263782B1 (en) 1978-12-01
BG26542A3 (en) 1979-04-12
DE2509782A1 (en) 1975-09-18
GB1474879A (en) 1977-05-25

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