IE43206L - Separating crystallizable materials from a multi-component¹system - Google Patents
Separating crystallizable materials from a multi-component¹systemInfo
- Publication number
- IE43206L IE43206L IE752653A IE265375A IE43206L IE 43206 L IE43206 L IE 43206L IE 752653 A IE752653 A IE 752653A IE 265375 A IE265375 A IE 265375A IE 43206 L IE43206 L IE 43206L
- Authority
- IE
- Ireland
- Prior art keywords
- ice
- heat exchanger
- separating
- columns
- concentrate
- Prior art date
Links
- 239000000463 material Substances 0.000 title abstract 6
- 239000012141 concentrate Substances 0.000 abstract 5
- 238000000034 method Methods 0.000 abstract 3
- 239000013078 crystal Substances 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 238000002156 mixing Methods 0.000 abstract 2
- 238000005406 washing Methods 0.000 abstract 2
- 230000001427 coherent effect Effects 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 239000012527 feed solution Substances 0.000 abstract 1
- 238000007710 freezing Methods 0.000 abstract 1
- 230000008014 freezing Effects 0.000 abstract 1
- 235000015203 fruit juice Nutrition 0.000 abstract 1
- 239000011159 matrix material Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002002 slurry Substances 0.000 abstract 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25C—PRODUCING, WORKING OR HANDLING ICE
- F25C5/00—Working or handling ice
- F25C5/02—Apparatus for disintegrating, removing or harvesting ice
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
- A23F5/28—Drying or concentrating coffee extract
- A23F5/30—Drying or concentrating coffee extract by freezing out the water
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof containing fruit or vegetable juices
- A23L2/08—Concentrating or drying of juices
- A23L2/12—Concentrating or drying of juices by freezing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25C—PRODUCING, WORKING OR HANDLING ICE
- F25C1/00—Producing ice
- F25C1/04—Producing ice by using stationary moulds
- F25C1/06—Producing ice by using stationary moulds open or openable at both ends
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- General Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mechanical Engineering (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Tea And Coffee (AREA)
- Non-Alcoholic Beverages (AREA)
- Extraction Or Liquid Replacement (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
- Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
1507034 Crystallisation process DEJ INTERNATIONAL RESEARCH CO BV 26 Nov 1975 [6 Dec 1974] 52900/74 Heading BIG A process for separating crystallisable material out of a multi - component liquid system comprises the following steps performed in sequence latchwise: (a) confining a batch of liquid in a heat exchanger, (b) applying cooling to the heat exchanger to crystallise at least part of the crystallisable material and create a substantially coherent matrix of crystals, (c) removing the material formed in step (b) from the heat exchanger, (d) breaking up the material from step (c) into a predetermined size and (e) separating crystallised material from the remainder of the multi - component system. Suitable aparatus, as shown in Fig. 1, for the freeze concentration of e.g. aqueous systems such as coffee extract and fruit juices, comprises a storage vessel (1), a number of shell and tube heat exchangers (3-12) mounted in parallel and connected to a central feed line, below the heat exchangers are an equal number of grinding means for breaking up the columns of ice and concentrate and simultaneously mixing the broken ice with recirculated concentrate and a washing column (13) for separating ice and concentrate. The process is carried out so that at the end of each freeze cycle the pump (2) pumps feed solution into the heat exchanger and so forces the columns of ice crystals and concentrate which have formed in the heat exchanger out of the exchanger, the columns of ice having first been released from the tube walls by briefly applying heat. A new freezing cycle starts when only a small frozen plug (28) remains in each tube (27). The frozen columns are broken up upon leaving the tubes by the knives (30) driven by a motor (33). The mixture of ice and concentrates enters the mixing vessel (32) at regular intervals and is transformed into a slurry for processing by the separating apparatus i.e. a washing column (13).
[GB1507034A]
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB52900/74A GB1507034A (en) | 1974-12-06 | 1974-12-06 | Process and apparatus for separating crystallizable materials from a multi-component system |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IE43206L true IE43206L (en) | 1976-06-06 |
| IE43206B1 IE43206B1 (en) | 1981-01-14 |
Family
ID=10465753
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IE2653/75A IE43206B1 (en) | 1974-12-06 | 1975-12-05 | A process for separating crystallizable materials from a multi-component system |
Country Status (17)
| Country | Link |
|---|---|
| JP (1) | JPS5178784A (en) |
| AT (1) | AT362747B (en) |
| AU (1) | AU504996B2 (en) |
| BE (1) | BE836238A (en) |
| BR (1) | BR7508075A (en) |
| CA (1) | CA1033284A (en) |
| CH (1) | CH604803A5 (en) |
| DE (1) | DE2554878A1 (en) |
| DK (1) | DK551775A (en) |
| FR (1) | FR2293231A1 (en) |
| GB (1) | GB1507034A (en) |
| IE (1) | IE43206B1 (en) |
| IT (1) | IT1051299B (en) |
| LU (1) | LU73933A1 (en) |
| NL (1) | NL7514031A (en) |
| SE (1) | SE412993B (en) |
| ZA (1) | ZA757433B (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK138672B (en) * | 1976-09-28 | 1978-10-16 | Danske Sukkerfab | Crystallization apparatus. |
| US5304384A (en) | 1993-03-23 | 1994-04-19 | Labatt Brewing Company Limited | Improvements in production of fermented malt beverages |
| US5695795A (en) | 1993-03-23 | 1997-12-09 | Labatt Brewing Company Limited | Methods for chill-treating non-distilled malted barley beverages |
| USRE36897E (en) | 1993-03-23 | 2000-10-03 | Labatt Brewing Company Limited | Methods for chill treating non-distilled malted barley beverages |
| US5869114A (en) | 1994-03-18 | 1999-02-09 | Labatt Brewing Company Limited | Production of fermented malt beverages |
| EP2130572A1 (en) * | 2008-06-06 | 2009-12-09 | Nederlandse Organisatie voor toegepast- natuurwetenschappelijk onderzoek TNO | Rotating knife, washing column, and method for disintegrating a crystal bed in a washing column |
| DE102016202285B4 (en) * | 2016-02-15 | 2022-03-03 | Deutsches Zentrum für Luft- und Raumfahrt e.V. | Heat transfer device, heat storage device and method for transferring heat |
| RU192489U1 (en) * | 2019-04-26 | 2019-09-18 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Волгоградский государственный технический университет" (ВолгГТУ) | Tubular mold |
| RU198654U1 (en) * | 2020-04-23 | 2020-07-21 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Волгоградский государственный технический университет" (ВолгГТУ) | TUBULAR CRYSTALLIZER |
| CN115779483B (en) * | 2022-11-17 | 2026-04-14 | 安徽海华科技集团有限公司 | Synthetic L-menthol crystallization purification system and purification method thereof |
-
1974
- 1974-12-06 GB GB52900/74A patent/GB1507034A/en not_active Expired
-
1975
- 1975-11-26 JP JP50141527A patent/JPS5178784A/ja active Pending
- 1975-11-26 ZA ZA757433A patent/ZA757433B/en unknown
- 1975-11-27 IT IT69928/75A patent/IT1051299B/en active
- 1975-11-28 AU AU87088/75A patent/AU504996B2/en not_active Expired
- 1975-12-02 NL NL7514031A patent/NL7514031A/en not_active Application Discontinuation
- 1975-12-02 CH CH1567775A patent/CH604803A5/xx not_active IP Right Cessation
- 1975-12-03 AT AT0919375A patent/AT362747B/en not_active IP Right Cessation
- 1975-12-03 CA CA241,269A patent/CA1033284A/en not_active Expired
- 1975-12-03 BE BE162416A patent/BE836238A/en unknown
- 1975-12-04 SE SE7513699A patent/SE412993B/en unknown
- 1975-12-04 LU LU73933A patent/LU73933A1/xx unknown
- 1975-12-05 BR BR7508075*A patent/BR7508075A/en unknown
- 1975-12-05 DE DE19752554878 patent/DE2554878A1/en not_active Withdrawn
- 1975-12-05 DK DK551775A patent/DK551775A/en not_active Application Discontinuation
- 1975-12-05 IE IE2653/75A patent/IE43206B1/en unknown
- 1975-12-05 FR FR7537389A patent/FR2293231A1/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| AU8708875A (en) | 1977-06-02 |
| FR2293231B1 (en) | 1981-09-04 |
| NL7514031A (en) | 1976-06-09 |
| DK551775A (en) | 1976-06-07 |
| FR2293231A1 (en) | 1976-07-02 |
| SE412993B (en) | 1980-03-31 |
| SE7513699L (en) | 1976-06-08 |
| ZA757433B (en) | 1976-11-24 |
| JPS5178784A (en) | 1976-07-08 |
| AT362747B (en) | 1981-06-10 |
| IE43206B1 (en) | 1981-01-14 |
| BE836238A (en) | 1976-06-03 |
| CH604803A5 (en) | 1978-09-15 |
| CA1033284A (en) | 1978-06-20 |
| LU73933A1 (en) | 1976-07-01 |
| IT1051299B (en) | 1981-04-21 |
| DE2554878A1 (en) | 1976-06-16 |
| AU504996B2 (en) | 1979-11-08 |
| GB1507034A (en) | 1978-04-12 |
| BR7508075A (en) | 1976-08-24 |
| ATA919375A (en) | 1980-11-15 |
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