IL78603A - Preparation of methylcarbamate insecticides via an oxime or phenol and methyl isocyanate - Google Patents
Preparation of methylcarbamate insecticides via an oxime or phenol and methyl isocyanateInfo
- Publication number
- IL78603A IL78603A IL78603A IL7860386A IL78603A IL 78603 A IL78603 A IL 78603A IL 78603 A IL78603 A IL 78603A IL 7860386 A IL7860386 A IL 7860386A IL 78603 A IL78603 A IL 78603A
- Authority
- IL
- Israel
- Prior art keywords
- methyl isocyanate
- oxime
- phenol
- water
- preparation
- Prior art date
Links
- HAMGRBXTJNITHG-UHFFFAOYSA-N methyl isocyanate Chemical compound CN=C=O HAMGRBXTJNITHG-UHFFFAOYSA-N 0.000 title abstract 9
- 150000002923 oximes Chemical class 0.000 title abstract 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 title abstract 3
- 239000002917 insecticide Substances 0.000 title abstract 2
- GTCAXTIRRLKXRU-UHFFFAOYSA-N methyl carbamate Chemical compound COC(N)=O GTCAXTIRRLKXRU-UHFFFAOYSA-N 0.000 title 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- ATHHXGZTWNVVOU-UHFFFAOYSA-N N-methylformamide Chemical compound CNC=O ATHHXGZTWNVVOU-UHFFFAOYSA-N 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- 239000012808 vapor phase Substances 0.000 abstract 2
- 238000001816 cooling Methods 0.000 abstract 1
- 238000007865 diluting Methods 0.000 abstract 1
- 239000011261 inert gas Substances 0.000 abstract 1
- 238000005839 oxidative dehydrogenation reaction Methods 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C269/00—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
- C07C269/02—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups from isocyanates with formation of carbamate groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US72781285A | 1985-04-26 | 1985-04-26 | |
| US06/827,517 US4698438A (en) | 1985-04-26 | 1986-02-11 | Process for the preparation of methyl carbamates and thioimidates |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IL78603A0 IL78603A0 (en) | 1986-08-31 |
| IL78603A true IL78603A (en) | 1989-09-28 |
Family
ID=27111584
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL78603A IL78603A (en) | 1985-04-26 | 1986-04-23 | Preparation of methylcarbamate insecticides via an oxime or phenol and methyl isocyanate |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4698438A (de) |
| EP (1) | EP0200506B1 (de) |
| KR (1) | KR940006766B1 (de) |
| AT (1) | ATE67179T1 (de) |
| BR (1) | BR8601803A (de) |
| CA (1) | CA1247113A (de) |
| DE (1) | DE3681331D1 (de) |
| IL (1) | IL78603A (de) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5284962A (en) * | 1992-10-09 | 1994-02-08 | E. I. Du Pont De Nemours And Company | Multistage process for making methyl carbamates |
| FR2768516B1 (fr) * | 1997-09-16 | 1999-10-29 | Inst Bouisson Bertrand | Utilisation d'isocyanates pour le dosage de fonctions nucleophiles a l'etat de traces en milieu humide |
| CN111377843B (zh) * | 2020-04-02 | 2022-03-18 | 湖南海利常德农药化工有限公司 | 一种灭多威的制备方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2870057A (en) * | 1957-11-26 | 1959-01-20 | Gulf Research Development Co | 4- or 5-indanyl n-methyl carbamate |
| NL130985C (de) * | 1967-02-09 | |||
| US3576834A (en) * | 1967-08-31 | 1971-04-27 | Du Pont | Substituted o-carbamylhydroxamates |
| US4207251A (en) * | 1977-08-02 | 1980-06-10 | Akzona Incorporated | Catalytic oxidation of formamides to form isocyanates |
| JPS56100751A (en) * | 1980-01-17 | 1981-08-12 | Asahi Chem Ind Co Ltd | Preparation of isocyanate |
-
1986
- 1986-02-11 US US06/827,517 patent/US4698438A/en not_active Expired - Lifetime
- 1986-04-22 CA CA000507229A patent/CA1247113A/en not_active Expired
- 1986-04-23 IL IL78603A patent/IL78603A/xx not_active IP Right Cessation
- 1986-04-23 BR BR8601803A patent/BR8601803A/pt not_active IP Right Cessation
- 1986-04-25 EP EP86303168A patent/EP0200506B1/de not_active Expired - Lifetime
- 1986-04-25 AT AT86303168T patent/ATE67179T1/de not_active IP Right Cessation
- 1986-04-25 DE DE8686303168T patent/DE3681331D1/de not_active Expired - Lifetime
- 1986-04-26 KR KR1019860003233A patent/KR940006766B1/ko not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE3681331D1 (de) | 1991-10-17 |
| US4698438A (en) | 1987-10-06 |
| BR8601803A (pt) | 1986-12-23 |
| ATE67179T1 (de) | 1991-09-15 |
| EP0200506B1 (de) | 1991-09-11 |
| EP0200506A2 (de) | 1986-11-05 |
| CA1247113A (en) | 1988-12-20 |
| KR860008128A (ko) | 1986-11-12 |
| IL78603A0 (en) | 1986-08-31 |
| EP0200506A3 (en) | 1988-07-13 |
| KR940006766B1 (ko) | 1994-07-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| KB | Patent renewed | ||
| KB | Patent renewed | ||
| KB | Patent renewed | ||
| EXP | Patent expired |