JP2007508551A - 検体をイオンモビリティスペクトロメーターの中に導入するための方法およびシステム - Google Patents
検体をイオンモビリティスペクトロメーターの中に導入するための方法およびシステム Download PDFInfo
- Publication number
- JP2007508551A JP2007508551A JP2006534408A JP2006534408A JP2007508551A JP 2007508551 A JP2007508551 A JP 2007508551A JP 2006534408 A JP2006534408 A JP 2006534408A JP 2006534408 A JP2006534408 A JP 2006534408A JP 2007508551 A JP2007508551 A JP 2007508551A
- Authority
- JP
- Japan
- Prior art keywords
- sample
- temperature
- ion mobility
- split ratio
- sample unit
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims abstract description 36
- 239000012491 analyte Substances 0.000 title claims description 53
- 239000002904 solvent Substances 0.000 claims description 48
- 238000003795 desorption Methods 0.000 claims description 36
- 239000012159 carrier gas Substances 0.000 claims description 26
- 239000007789 gas Substances 0.000 claims description 24
- 238000004458 analytical method Methods 0.000 claims description 19
- 238000009835 boiling Methods 0.000 claims description 12
- 238000012546 transfer Methods 0.000 claims description 11
- 238000012512 characterization method Methods 0.000 claims description 8
- 238000010926 purge Methods 0.000 claims description 6
- 230000000704 physical effect Effects 0.000 claims description 5
- 238000001704 evaporation Methods 0.000 claims description 4
- 229910052757 nitrogen Inorganic materials 0.000 claims description 3
- 150000002500 ions Chemical class 0.000 description 49
- 238000010438 heat treatment Methods 0.000 description 7
- 238000001871 ion mobility spectroscopy Methods 0.000 description 7
- 238000010586 diagram Methods 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 230000005684 electric field Effects 0.000 description 3
- 238000004811 liquid chromatography Methods 0.000 description 3
- 230000002093 peripheral effect Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 230000006978 adaptation Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/62—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating the ionisation of gases, e.g. aerosols; by investigating electric discharges, e.g. emission of cathode
- G01N27/622—Ion mobility spectrometry
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Electrochemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Sampling And Sample Adjustment (AREA)
- Measuring Volume Flow (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US50975403P | 2003-10-08 | 2003-10-08 | |
| PCT/US2004/033332 WO2005036130A2 (en) | 2003-10-08 | 2004-10-08 | Method and system for introducing an analyte into an ion mobility spectrometer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2007508551A true JP2007508551A (ja) | 2007-04-05 |
| JP2007508551A5 JP2007508551A5 (2) | 2011-07-07 |
Family
ID=34435020
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006534408A Pending JP2007508551A (ja) | 2003-10-08 | 2004-10-08 | 検体をイオンモビリティスペクトロメーターの中に導入するための方法およびシステム |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US7129479B2 (2) |
| EP (1) | EP1673606A4 (2) |
| JP (1) | JP2007508551A (2) |
| WO (1) | WO2005036130A2 (2) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080101995A1 (en) * | 2005-12-16 | 2008-05-01 | Smiths Detection Inc. | Ion mobility spectrometer having improved sample receiving device |
| US20120143515A1 (en) * | 2006-09-28 | 2012-06-07 | Smiths Detection Inc. | Multi-detector gas identification system |
| WO2009018305A1 (en) | 2007-07-30 | 2009-02-05 | Particle Measuring Systems, Inc. | Detection of analytes using ion mobility spectrometry |
| JP2010540965A (ja) | 2007-12-05 | 2010-12-24 | オールテック・アソシエイツ・インコーポレーテッド | サンプルの画分を収集しサンプルを分析するための方法および装置 |
| WO2010068276A1 (en) | 2008-12-10 | 2010-06-17 | Alltech Associates Inc. | Chromatography systems and system components |
| AU2009325052A1 (en) * | 2008-12-10 | 2011-06-30 | Alltech Associates, Inc. | Components suitable for use in devices such as an evaporative light scattering detector |
| US8314934B2 (en) | 2009-09-01 | 2012-11-20 | Alltech Associates, Inc. | Methods and apparatus for analyzing samples and collecting sample fractions |
| JP5815533B2 (ja) * | 2010-08-31 | 2015-11-17 | アトナープ株式会社 | イオン移動度センサーに供給するサンプルを調製する装置 |
| CN103887140A (zh) * | 2012-12-19 | 2014-06-25 | 中国科学院大连化学物理研究所 | 一种离子迁移谱仪 |
| GB201314252D0 (en) | 2013-08-08 | 2013-09-25 | Smiths Detection Watford Ltd | Apparatus and method |
| CN112284822B (zh) * | 2020-09-30 | 2024-07-09 | 深圳市锐拓分析仪器有限公司 | 一种流池法溶出度仪自动取样装置 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0933502A (ja) * | 1995-07-18 | 1997-02-07 | Shimadzu Corp | ガスクロマトグラフ装置 |
| JPH0943214A (ja) * | 1995-07-31 | 1997-02-14 | Shimadzu Corp | ガスクロマトグラフの試料導入方法 |
| JP2002503808A (ja) * | 1998-02-11 | 2002-02-05 | ヘイリー、ローレンス・ブイ | Gc/imsを使用する手持ち型検出システム |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5163979A (en) * | 1991-06-27 | 1992-11-17 | The Dow Chemical Company | Pressure programmable gas chromatograph regulator |
| US7057168B2 (en) * | 1999-07-21 | 2006-06-06 | Sionex Corporation | Systems for differential ion mobility analysis |
-
2004
- 2004-10-08 JP JP2006534408A patent/JP2007508551A/ja active Pending
- 2004-10-08 US US10/961,612 patent/US7129479B2/en not_active Expired - Lifetime
- 2004-10-08 EP EP04794631A patent/EP1673606A4/en not_active Withdrawn
- 2004-10-08 WO PCT/US2004/033332 patent/WO2005036130A2/en not_active Ceased
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0933502A (ja) * | 1995-07-18 | 1997-02-07 | Shimadzu Corp | ガスクロマトグラフ装置 |
| JPH0943214A (ja) * | 1995-07-31 | 1997-02-14 | Shimadzu Corp | ガスクロマトグラフの試料導入方法 |
| JP2002503808A (ja) * | 1998-02-11 | 2002-02-05 | ヘイリー、ローレンス・ブイ | Gc/imsを使用する手持ち型検出システム |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2005036130A3 (en) | 2006-12-28 |
| EP1673606A4 (en) | 2010-05-05 |
| WO2005036130A2 (en) | 2005-04-21 |
| EP1673606A2 (en) | 2006-06-28 |
| US20050127286A1 (en) | 2005-06-16 |
| US7129479B2 (en) | 2006-10-31 |
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