JP3789193B2 - 耐水性を有する蓄光性蛍光体の製造方法 - Google Patents

耐水性を有する蓄光性蛍光体の製造方法 Download PDF

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Publication number: JP3789193B2
Authority: JP; Japan
Prior art keywords: phosphorescent phosphor; water resistance; phosphorescent; luminance; water
Prior art date: 1997-03-31
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

JP08111497A

Other languages

English (en)

Japanese (ja)

Other versions

JPH10273654A5 (cs

JPH10273654A (ja

Inventor

康充青木

米一平田

秀彦笠井

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Nemoto and Co Ltd

Original Assignee

Nemoto and Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1997-03-31

Filing date

1997-03-31

Publication date

2006-06-21

1997-03-31 Application filed by Nemoto and Co Ltd filed Critical Nemoto and Co Ltd

1997-03-31 Priority to JP08111497A priority Critical patent/JP3789193B2/ja

1998-10-13 Publication of JPH10273654A publication Critical patent/JPH10273654A/ja

2005-03-03 Publication of JPH10273654A5 publication Critical patent/JPH10273654A5/ja

2006-06-21 Application granted granted Critical

2006-06-21 Publication of JP3789193B2 publication Critical patent/JP3789193B2/ja

2017-03-31 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims description 89
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 title claims description 65
238000004519 manufacturing process Methods 0.000 title claims description 17
238000010438 heat treatment Methods 0.000 claims description 22
229910019142 PO4 Inorganic materials 0.000 claims description 17
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 16
239000010452 phosphate Substances 0.000 claims description 16
229910000287 alkaline earth metal oxide Inorganic materials 0.000 claims description 13
150000001342 alkaline earth metals Chemical class 0.000 claims description 13
229910052784 alkaline earth metal Inorganic materials 0.000 claims description 12
229910052693 Europium Inorganic materials 0.000 claims description 9
229910052779 Neodymium Inorganic materials 0.000 claims description 7
229910052761 rare earth metal Inorganic materials 0.000 claims description 7
229910052692 Dysprosium Inorganic materials 0.000 claims description 5
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 4
229910052788 barium Inorganic materials 0.000 claims description 4
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 4
229910052791 calcium Inorganic materials 0.000 claims description 4
239000011575 calcium Substances 0.000 claims description 4
229910052712 strontium Inorganic materials 0.000 claims description 4
CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 claims description 4
229910052684 Cerium Inorganic materials 0.000 claims description 3
229910052691 Erbium Inorganic materials 0.000 claims description 3
229910052688 Gadolinium Inorganic materials 0.000 claims description 3
229910052689 Holmium Inorganic materials 0.000 claims description 3
229910052765 Lutetium Inorganic materials 0.000 claims description 3
229910052777 Praseodymium Inorganic materials 0.000 claims description 3
229910052772 Samarium Inorganic materials 0.000 claims description 3
229910052771 Terbium Inorganic materials 0.000 claims description 3
229910052775 Thulium Inorganic materials 0.000 claims description 3
229910052769 Ytterbium Inorganic materials 0.000 claims description 3
229910052746 lanthanum Inorganic materials 0.000 claims description 3
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 2
229910001404 rare earth metal oxide Inorganic materials 0.000 claims description 2
238000001035 drying Methods 0.000 claims 1
230000007935 neutral effect Effects 0.000 claims 1
MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 30
229910000388 diammonium phosphate Inorganic materials 0.000 description 29
235000019838 diammonium phosphate Nutrition 0.000 description 29
238000005259 measurement Methods 0.000 description 16
235000021317 phosphate Nutrition 0.000 description 16
230000000052 comparative effect Effects 0.000 description 13
239000000203 mixture Substances 0.000 description 11
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 10
239000011574 phosphorus Substances 0.000 description 10
229910052698 phosphorus Inorganic materials 0.000 description 10
VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 8
238000002474 experimental method Methods 0.000 description 8
239000012535 impurity Substances 0.000 description 8
239000011347 resin Substances 0.000 description 7
229920005989 resin Polymers 0.000 description 7
238000006243 chemical reaction Methods 0.000 description 6
229910021529 ammonia Inorganic materials 0.000 description 5
230000000694 effects Effects 0.000 description 5
239000000463 material Substances 0.000 description 5
NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 4
AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 4
229910003668 SrAl Inorganic materials 0.000 description 4
210000003298 dental enamel Anatomy 0.000 description 4
238000000034 method Methods 0.000 description 4
OOSZCNKVJAVHJI-UHFFFAOYSA-N 1-[(4-fluorophenyl)methyl]piperazine Chemical compound C1=CC(F)=CC=C1CN1CCNCC1 OOSZCNKVJAVHJI-UHFFFAOYSA-N 0.000 description 3
LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 3
229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 description 3
235000019837 monoammonium phosphate Nutrition 0.000 description 3
239000002002 slurry Substances 0.000 description 3
229940074545 sodium dihydrogen phosphate dihydrate Drugs 0.000 description 3
GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 3
235000019982 sodium hexametaphosphate Nutrition 0.000 description 3
238000003756 stirring Methods 0.000 description 3
239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 3
SXAMGRAIZSSWIH-UHFFFAOYSA-N 2-[3-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-1,2,4-oxadiazol-5-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1=NOC(=N1)CC(=O)N1CC2=C(CC1)NN=N2 SXAMGRAIZSSWIH-UHFFFAOYSA-N 0.000 description 2
238000010521 absorption reaction Methods 0.000 description 2
238000007654 immersion Methods 0.000 description 2
229910052747 lanthanoid Inorganic materials 0.000 description 2
150000002602 lanthanoids Chemical class 0.000 description 2
CUXQLKLUPGTTKL-UHFFFAOYSA-M microcosmic salt Chemical compound [NH4+].[Na+].OP([O-])([O-])=O CUXQLKLUPGTTKL-UHFFFAOYSA-M 0.000 description 2
150000003839 salts Chemical class 0.000 description 2
229910001427 strontium ion Inorganic materials 0.000 description 2
BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
FPWJLQXCGHQXLL-UHFFFAOYSA-N [P].OP(O)(O)=O Chemical compound [P].OP(O)(O)=O FPWJLQXCGHQXLL-UHFFFAOYSA-N 0.000 description 1
239000002253 acid Substances 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
238000000576 coating method Methods 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
239000008367 deionised water Substances 0.000 description 1
229910021641 deionized water Inorganic materials 0.000 description 1
230000006866 deterioration Effects 0.000 description 1
230000001747 exhibiting effect Effects 0.000 description 1
BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000002245 particle Substances 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
229920003023 plastic Polymers 0.000 description 1
159000000001 potassium salts Chemical class 0.000 description 1
238000012545 processing Methods 0.000 description 1
238000007873 sieving Methods 0.000 description 1
IQTQISLCLWJRPM-UHFFFAOYSA-M sodium;azane;dihydrogen phosphate;tetrahydrate Chemical compound [NH4+].O.O.O.O.[Na+].OP([O-])([O-])=O IQTQISLCLWJRPM-UHFFFAOYSA-M 0.000 description 1
239000000126 substance Substances 0.000 description 1
238000012546 transfer Methods 0.000 description 1

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Luminescent Compositions (AREA)

JP08111497A 1997-03-31 1997-03-31 耐水性を有する蓄光性蛍光体の製造方法 Expired - Fee Related JP3789193B2 (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP08111497A JP3789193B2 (ja)	1997-03-31	1997-03-31	耐水性を有する蓄光性蛍光体の製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP08111497A JP3789193B2 (ja)	1997-03-31	1997-03-31	耐水性を有する蓄光性蛍光体の製造方法

Publications (3)

Publication Number	Publication Date
JPH10273654A JPH10273654A (ja)	1998-10-13
JPH10273654A5 JPH10273654A5 (cs)	2005-03-03
JP3789193B2 true JP3789193B2 (ja)	2006-06-21

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ID=13737359

Family Applications (1)

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JP08111497A Expired - Fee Related JP3789193B2 (ja)	1997-03-31	1997-03-31	耐水性を有する蓄光性蛍光体の製造方法

Country Status (1)

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JP (1)	JP3789193B2 (cs)

Cited By (1)

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WO2015083814A1 (ja)	2013-12-06	2015-06-11	堺化学工業株式会社	応力発光材料、応力発光材料の製造方法、応力発光性塗料組成物、樹脂組成物及び応力発光体

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US6264855B1 (en)	1999-10-07	2001-07-24	Matsui Shikiso Chemical Co., Ltd.	Process for preparing water resistant luminous pigments
RU2323955C1 (ru) *	2006-09-15	2008-05-10	Андриевский Александр Михайлович	Водостойкий люминесцентный пигмент и люминесцентная печатная краска на его основе
JP2012056095A (ja) *	2010-09-06	2012-03-22	Pilot Ink Co Ltd	蓄光性水変色体
JP5234080B2 (ja) *	2010-10-12	2013-07-10	日亜化学工業株式会社	発光装置、発光素子用蛍光体及びその製造方法
JP5967787B1 (ja) *	2016-02-12	2016-08-10	エルティーアイ株式会社	蓄光顔料の製造方法
US10153405B2 (en)	2016-02-26	2018-12-11	Nichia Corporation	Fluorescent material, light emitting device, and method for producing fluorescent material
JP7115112B2 (ja) *	2018-07-27	2022-08-09	堺化学工業株式会社	蓄光材料の製造方法

1997
- 1997-03-31 JP JP08111497A patent/JP3789193B2/ja not_active Expired - Fee Related

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WO2015083814A1 (ja)	2013-12-06	2015-06-11	堺化学工業株式会社	応力発光材料、応力発光材料の製造方法、応力発光性塗料組成物、樹脂組成物及び応力発光体
CN105793390A (zh) *	2013-12-06	2016-07-20	堺化学工业株式会社	应力发光材料、应力发光材料的制造方法、应力发光性涂料组合物、树脂组合物及应力发光体
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EP3078722A4 (en) *	2013-12-06	2017-07-12	Sakai Chemical Industry Co., Ltd.	Stress-induced light-emission material, method for manufacturing stress-induced light-emission material, stress-induced light-emission paint composition, resin composition, and stress-induced light-emission body
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Publication number	Publication date
JPH10273654A (ja)	1998-10-13

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