JP4105241B2 - 新規な化学化合物、当該化合物を含有する爆薬および、ガス発生器における当該化合物の使用 - Google Patents
新規な化学化合物、当該化合物を含有する爆薬および、ガス発生器における当該化合物の使用 Download PDFInfo
- Publication number
- JP4105241B2 JP4105241B2 JP55078098A JP55078098A JP4105241B2 JP 4105241 B2 JP4105241 B2 JP 4105241B2 JP 55078098 A JP55078098 A JP 55078098A JP 55078098 A JP55078098 A JP 55078098A JP 4105241 B2 JP4105241 B2 JP 4105241B2
- Authority
- JP
- Japan
- Prior art keywords
- compounds
- dinitramide
- propellants
- gudn
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 150000001875 compounds Chemical class 0.000 title claims abstract description 25
- 239000002360 explosive Substances 0.000 title claims abstract description 16
- 239000003380 propellant Substances 0.000 claims abstract description 31
- MJVUDZGNBKFOBF-UHFFFAOYSA-N n-nitronitramide Chemical compound [O-][N+](=O)N[N+]([O-])=O MJVUDZGNBKFOBF-UHFFFAOYSA-N 0.000 claims abstract description 23
- SQSPRWMERUQXNE-UHFFFAOYSA-N Guanylurea Chemical compound NC(=N)NC(N)=O SQSPRWMERUQXNE-UHFFFAOYSA-N 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 17
- 239000007789 gas Substances 0.000 description 13
- 238000002485 combustion reaction Methods 0.000 description 9
- 239000000243 solution Substances 0.000 description 8
- BRUFJXUJQKYQHA-UHFFFAOYSA-O ammonium dinitramide Chemical compound [NH4+].[O-][N+](=O)[N-][N+]([O-])=O BRUFJXUJQKYQHA-UHFFFAOYSA-O 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 235000015842 Hesperis Nutrition 0.000 description 6
- 235000012633 Iberis amara Nutrition 0.000 description 6
- 239000011230 binding agent Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- POCJOGNVFHPZNS-ZJUUUORDSA-N (6S,7R)-2-azaspiro[5.5]undecan-7-ol Chemical compound O[C@@H]1CCCC[C@]11CNCCC1 POCJOGNVFHPZNS-ZJUUUORDSA-N 0.000 description 4
- GDDNTTHUKVNJRA-UHFFFAOYSA-N 3-bromo-3,3-difluoroprop-1-ene Chemical compound FC(F)(Br)C=C GDDNTTHUKVNJRA-UHFFFAOYSA-N 0.000 description 4
- BSPUVYFGURDFHE-UHFFFAOYSA-N Nitramine Natural products CC1C(O)CCC2CCCNC12 BSPUVYFGURDFHE-UHFFFAOYSA-N 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- POCJOGNVFHPZNS-UHFFFAOYSA-N isonitramine Natural products OC1CCCCC11CNCCC1 POCJOGNVFHPZNS-UHFFFAOYSA-N 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- KNIKDPRISVIPBU-UHFFFAOYSA-N 1,2-dichloro-4-[isocyano-(4-methylphenyl)sulfonylmethyl]benzene Chemical compound C1=CC(C)=CC=C1S(=O)(=O)C([N+]#[C-])C1=CC=C(Cl)C(Cl)=C1 KNIKDPRISVIPBU-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000000567 combustion gas Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000008188 pellet Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 230000035945 sensitivity Effects 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 150000001540 azides Chemical class 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- -1 dinitramide ions Chemical class 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- HGUFODBRKLSHSI-UHFFFAOYSA-N 2,3,7,8-tetrachloro-dibenzo-p-dioxin Chemical compound O1C2=CC(Cl)=C(Cl)C=C2OC2=C1C=C(Cl)C(Cl)=C2 HGUFODBRKLSHSI-UHFFFAOYSA-N 0.000 description 1
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 239000000020 Nitrocellulose Substances 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000003915 air pollution Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000005474 detonation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- XSUZSAMSJKGENR-UHFFFAOYSA-N nitramide;potassium Chemical compound [K].N[N+]([O-])=O.N[N+]([O-])=O XSUZSAMSJKGENR-UHFFFAOYSA-N 0.000 description 1
- 238000006396 nitration reaction Methods 0.000 description 1
- 229920001220 nitrocellulos Polymers 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 239000005011 phenolic resin Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
- C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06D—MEANS FOR GENERATING SMOKE OR MIST; GAS-ATTACK COMPOSITIONS; GENERATION OF GAS FOR BLASTING OR PROPULSION (CHEMICAL PART)
- C06D5/00—Generation of pressure gas, e.g. for blasting cartridges, starting cartridges, rockets
- C06D5/06—Generation of pressure gas, e.g. for blasting cartridges, starting cartridges, rockets by reaction of two or more solids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9701897A SE509312C2 (sv) | 1997-05-21 | 1997-05-21 | Förening som utgöres av guanylureadinitramid, explosivämne innehållande föreningen samt användning av föreningen i gasgeneratorer. |
| SE9701897-2 | 1997-05-21 | ||
| PCT/SE1998/000949 WO1998055428A1 (en) | 1997-05-21 | 1998-05-20 | New chemical compound, explosive containing the compound and use of the compound in gas generators |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2001527575A JP2001527575A (ja) | 2001-12-25 |
| JP4105241B2 true JP4105241B2 (ja) | 2008-06-25 |
Family
ID=20407027
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP55078098A Expired - Fee Related JP4105241B2 (ja) | 1997-05-21 | 1998-05-20 | 新規な化学化合物、当該化合物を含有する爆薬および、ガス発生器における当該化合物の使用 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6291711B2 (de) |
| EP (1) | EP1007496B1 (de) |
| JP (1) | JP4105241B2 (de) |
| AT (1) | ATE225328T1 (de) |
| AU (1) | AU7561698A (de) |
| DE (1) | DE69808494T2 (de) |
| ES (1) | ES2182310T3 (de) |
| SE (1) | SE509312C2 (de) |
| WO (1) | WO1998055428A1 (de) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6117255A (en) * | 1998-07-28 | 2000-09-12 | Trw Inc. | Gas generating composition comprising guanylurea dinitramide |
| SE513315C2 (sv) * | 1998-12-30 | 2000-08-21 | Nexplo Bofors Ab | Sätt att framställa gasbildare för gasdrivna bilsäkerhetsdetaljer och pyrotekiska gasbildare framställd i enlighet med sättet |
| SE514336C2 (sv) * | 1999-05-12 | 2001-02-12 | Bofors Bepab Ab | Sammansatt gasbildare för gasdrivna bilsäkerhetsdetaljer |
| SE515717C2 (sv) * | 2000-01-03 | 2001-10-01 | Nexplo Bofors Ab | Sätt att framställa gasdrivna bilsäkerhetsdetaljer samt i enlighet därmed framställda pyrotekniska gasbildare |
| SE526402C2 (sv) * | 2004-01-21 | 2005-09-06 | Foersvarets Materielverk | Sätt att framställa salt av dinitramidsyra |
| WO2007012348A1 (en) * | 2005-07-26 | 2007-02-01 | Dalphi Metal España, S.A. | Gas generating composition for automotive use manufactured by pellet formation |
| US7857920B1 (en) * | 2005-08-22 | 2010-12-28 | The United States Of America As Represented By The Secretary Of The Navy | Low temperature clean burning pyrotechnic gas generators |
| FR2902783B1 (fr) * | 2006-06-27 | 2008-10-24 | Snpe Materiaux Energetiques Sa | Compositions pyrotechniques thermo-initiables, utilisation. |
| US8778104B1 (en) | 2008-04-22 | 2014-07-15 | The United States Of America As Represented By The Secretary Of The Navy | Insensitive gun propellant, ammunition round assembly, armament system, and related methods |
| US8425703B1 (en) | 2010-03-24 | 2013-04-23 | The United States of Amierica as Represented by the Secretary of the Navy | Insensitive munitions primers |
| DE102011100113B4 (de) | 2010-06-28 | 2019-10-24 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Gasgenerator-Treibstoffzusammensetzung, Verfahrenzu ihrer Herstellung und deren Verwendung |
| CN102731345A (zh) * | 2011-12-29 | 2012-10-17 | 湖北航天化学技术研究所 | 一种合成n-脒基脲二硝酰胺盐的方法 |
| CN109824549A (zh) * | 2019-04-02 | 2019-05-31 | 西安近代化学研究所 | 一种n-脒基脲二硝酰胺盐的制备方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2953448A (en) * | 1953-01-14 | 1960-09-20 | Ici Ltd | Compositions for safety heating elements |
| US3758555A (en) * | 1965-01-08 | 1973-09-11 | Minnesota Mining & Mfg | Difluoroamino compounds |
| US5198204A (en) | 1990-06-18 | 1993-03-30 | Sri International | Method of forming dinitramide salts |
| US5254324A (en) | 1990-06-18 | 1993-10-19 | Sri International | Dinitramide salts and method of making same |
| DE4220019A1 (de) * | 1991-06-21 | 1992-12-24 | Dynamit Nobel Ag | Treibmittel fuer gasgeneratoren |
| US5415852A (en) | 1992-01-29 | 1995-05-16 | Sri International | Process for forming a dinitramide salt or acid by reaction of a salt or free acid of an N(alkoxycarbonyl)N-nitroamide with a nitronium-containing compound followed by reaction of the intermediate product respectively with a base or alcohol |
| WO1994001381A1 (fr) * | 1992-07-13 | 1994-01-20 | Nippon Koki Co., Ltd. | Agent generateur de gaz pour sacs gonflables |
| DE19505568A1 (de) | 1995-02-18 | 1996-08-22 | Dynamit Nobel Ag | Gaserzeugende Mischungen |
| JP3719614B2 (ja) * | 1995-05-26 | 2005-11-24 | 株式会社アイ・エイチ・アイ・エアロスペース | Adnの合成法 |
| SE516719C2 (sv) | 1995-08-08 | 2002-02-19 | Totalfoersvarets Forskningsins | Sätt att framställa dinitramidsyra och salter därav |
| US6004410A (en) * | 1998-07-28 | 1999-12-21 | Trw Inc. | Apparatus comprising an inflatable vehicle occupant protection device and a gas generating composition therefor |
-
1997
- 1997-05-21 SE SE9701897A patent/SE509312C2/sv not_active IP Right Cessation
-
1998
- 1998-05-20 EP EP98923290A patent/EP1007496B1/de not_active Expired - Lifetime
- 1998-05-20 US US09/423,636 patent/US6291711B2/en not_active Expired - Lifetime
- 1998-05-20 DE DE69808494T patent/DE69808494T2/de not_active Expired - Lifetime
- 1998-05-20 AU AU75616/98A patent/AU7561698A/en not_active Abandoned
- 1998-05-20 ES ES98923290T patent/ES2182310T3/es not_active Expired - Lifetime
- 1998-05-20 WO PCT/SE1998/000949 patent/WO1998055428A1/en not_active Ceased
- 1998-05-20 AT AT98923290T patent/ATE225328T1/de not_active IP Right Cessation
- 1998-05-20 JP JP55078098A patent/JP4105241B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE69808494T2 (de) | 2003-07-17 |
| SE9701897D0 (sv) | 1997-05-21 |
| SE9701897L (sv) | 1998-11-22 |
| ATE225328T1 (de) | 2002-10-15 |
| US6291711B2 (en) | 2001-09-18 |
| WO1998055428A1 (en) | 1998-12-10 |
| DE69808494D1 (de) | 2002-11-07 |
| US20010007913A1 (en) | 2001-07-12 |
| SE509312C2 (sv) | 1999-01-11 |
| EP1007496A1 (de) | 2000-06-14 |
| JP2001527575A (ja) | 2001-12-25 |
| EP1007496B1 (de) | 2002-10-02 |
| AU7561698A (en) | 1998-12-21 |
| ES2182310T3 (es) | 2003-03-01 |
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