JPH01101100A - Thin film array ultrasonic converter - Google Patents

Thin film array ultrasonic converter

Info

Publication number
JPH01101100A
JPH01101100A JP62257223A JP25722387A JPH01101100A JP H01101100 A JPH01101100 A JP H01101100A JP 62257223 A JP62257223 A JP 62257223A JP 25722387 A JP25722387 A JP 25722387A JP H01101100 A JPH01101100 A JP H01101100A
Authority
JP
Japan
Prior art keywords
thin film
array ultrasonic
matching layer
ultrasonic transducer
film array
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP62257223A
Other languages
Japanese (ja)
Other versions
JP2620945B2 (en
Inventor
Keiko Kushida
恵子 櫛田
Hiroyuki Takeuchi
裕之 竹内
Hiroshi Kanda
浩 神田
Kiyoshi Ishikawa
潔 石川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hitachi Construction Machinery Co Ltd
Original Assignee
Hitachi Construction Machinery Co Ltd
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Filing date
Publication date
Application filed by Hitachi Construction Machinery Co Ltd filed Critical Hitachi Construction Machinery Co Ltd
Priority to JP62257223A priority Critical patent/JP2620945B2/en
Publication of JPH01101100A publication Critical patent/JPH01101100A/en
Application granted granted Critical
Publication of JP2620945B2 publication Critical patent/JP2620945B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。
(57) [Summary] This bulletin contains application data before electronic filing, so abstract data is not recorded.

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は超音波変換器に係り、特に微細な構造を非破壊
で観察するのに好適な薄膜アレイ超音波変換器に関する
DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] The present invention relates to an ultrasonic transducer, and particularly to a thin film array ultrasonic transducer suitable for nondestructively observing fine structures.

〔従来の技術〕[Conventional technology]

従来、超音波断層装置には周波数1〜10MHzの超音
波を送受するアレイセンサが使用されている。しかし最
近では、半導体のパッケージ検査や材料の欠陥検査など
、より*、Wな構造を見る必要ができており、そのため
には周波数50〜100MHzの高周波超音波を用いて
分解能を向上させる必要がある。この領域の超音波を送
受する圧電体は厚さ50μm以下となるため、薄膜とし
て形成された圧電体を使用する。
Conventionally, an array sensor that transmits and receives ultrasonic waves with a frequency of 1 to 10 MHz has been used in an ultrasonic tomography apparatus. However, recently, it has become necessary to see more *W structures, such as in semiconductor package inspection and material defect inspection, and to do so, it is necessary to improve the resolution using high-frequency ultrasonic waves with a frequency of 50 to 100 MHz. . Since the piezoelectric material that transmits and receives ultrasonic waves in this region has a thickness of 50 μm or less, a piezoelectric material formed as a thin film is used.

従来、この薄膜超音波変換器は、曝−の変換部として形
成され、機械的に平面内で走査して情報を得、画像を構
成する方法がとられている。この方法を利用した超音波
顕微鏡については「固体物J!]!J 17 (198
2年)第5工頁から第57頁において論じられている。
Conventionally, this thin film ultrasonic transducer is formed as an exposure converter, and a method has been adopted in which it mechanically scans within a plane to obtain information and construct an image. Regarding ultrasound microscopy using this method, see “Solid Objects J!]!J 17 (198
2) Discussed on pages 5 to 57.

0 〔発明が解決しようとする間層点〕 上記従来技術においては、超音波は圧電薄膜の形成され
ている基板をレンズとし、このレンズを介して放射され
ており、通常音lFl!整合層が設けられていない。こ
れに対してアレイ変換器の場合には、各素子間の電気的
1機械的分離を良くするためにアレイ状にした圧電薄膜
側から直接音を放出させる方式が有利と考えられる。そ
の場合、圧電薄膜と超音波の伝播媒体(例えば水)との
マツチングをとるための音響整合層を必要とする。
0 [Interlayer point to be solved by the invention] In the above-mentioned conventional technology, the ultrasonic wave is emitted through the lens using the substrate on which the piezoelectric thin film is formed, and the normal sound lFl! No matching layer is provided. On the other hand, in the case of an array transducer, it is considered advantageous to emit sound directly from the piezoelectric thin film side arranged in an array in order to improve electrical and mechanical separation between each element. In that case, an acoustic matching layer is required to match the piezoelectric thin film and the ultrasonic propagation medium (eg, water).

数MHz帯の超音波アレイ変換器では1通常セラミック
スを所望の厚み9幅に研磨、切断した後。
For ultrasonic array transducers in the several MHz band, 1. Normally, ceramics are polished and cut to the desired thickness and width.

上記音響整合層を形成している。この音響整合層は切断
せずに用いられる場合もあるが、素子間の分離を良くす
るためには分離した方が良い。しかも、数10MHz以
上の超音波を送受するプレイ変換器の場合には1つのエ
レメントの幅も小さくなり、整合層の分離は必須である
The above acoustic matching layer is formed. Although this acoustic matching layer may be used without being cut, it is better to separate it in order to improve separation between elements. Moreover, in the case of a play transducer that transmits and receives ultrasonic waves of several tens of MHz or more, the width of one element becomes small, and separation of matching layers is essential.

しかしながら、従来の方法に準じて、薄膜圧電体をエツ
チングにより分割した後、音響整合層を形成し、さらに
これをエツチングして分割する方法では、パターンの合
わせ精度も高く要求され、また工程も多くなる。これま
で、厚み縦振動を利用した薄膜アレイ変換器については
具体的な報告例がなく、音響整合層まで含めた変換器を
構成する上での問題点に配慮がなされていなかった。
However, according to the conventional method, a thin film piezoelectric material is divided by etching, an acoustic matching layer is formed, and this is further divided by etching. This method requires high pattern alignment accuracy and requires many steps. Become. Until now, there have been no specific reports on thin film array transducers that utilize thickness longitudinal vibration, and no consideration has been given to the problems involved in constructing a transducer that includes an acoustic matching layer.

本発明の目的は、少ない工程で形成可能な薄膜アレイ変
換器を提供することにある。
An object of the present invention is to provide a thin film array transducer that can be formed with fewer steps.

〔問題点を解決するための手段〕[Means for solving problems]

上記目的、基板上に形成された圧電薄膜、さらにその上
に形成された上部電極よりなる超音波変換塁上、先に音
響整合層を形成した後、音響整合層、上部電極、圧電薄
膜を順次エツチングすることにより達成される。
For the above purpose, on an ultrasonic conversion base consisting of a piezoelectric thin film formed on a substrate and an upper electrode formed on top of it, an acoustic matching layer is first formed, and then an acoustic matching layer, an upper electrode, and a piezoelectric thin film are sequentially formed. This is achieved by etching.

〔作用〕[Effect]

薄膜アレイ超音波変換器を作成するには、−様に形成さ
れた変換器を分割する必要がある。しかし、1つ1つの
変換器の大きさが10μmのオーダになるため1分割を
行うためにはフォトリソグラフィ技術及びエツチングの
技術を必要とする。
To create a thin film array ultrasound transducer, it is necessary to split the otherwise formed transducer. However, since the size of each converter is on the order of 10 μm, photolithography and etching techniques are required to perform one division.

超音波変換器を構成している圧電薄膜、電極、音響整合
層をエツチングする場合、各々適当なエツチング液を選
択する必要があり、それとともにエツチング液に対する
耐性の有る材料でマスクを形成する。
When etching the piezoelectric thin film, electrode, and acoustic matching layer constituting the ultrasonic transducer, it is necessary to select an appropriate etching solution for each, and at the same time, a mask is formed of a material that is resistant to the etching solution.

本発明になる薄膜アレイ超音波変換器では、音響整合層
まで先に形成した後、各々その上に設けられた層をマス
クとして順次エツチングすることを特徴としている。ま
ず、フォトリソグラフィーで形成されたレジストパター
ンをマスクとして音響整合層をエツチングし1次の電極
層及び圧電薄膜はバターニングされた音W整合層をマス
クとしてエツチングを行う。これにより、フォトリソグ
ラフィーによるパターニングは1回で済み、工程を少な
くすることが可能となる。
The thin film array ultrasonic transducer according to the present invention is characterized in that after forming up to the acoustic matching layer first, the layers provided thereon are sequentially etched using the layers provided thereon as masks. First, the acoustic matching layer is etched using a resist pattern formed by photolithography as a mask, and the primary electrode layer and piezoelectric thin film are etched using the patterned acoustic W matching layer as a mask. As a result, patterning by photolithography only needs to be performed once, making it possible to reduce the number of steps.

〔実施例〕〔Example〕

以下1本発明の一実施例を第1図により説明する。 An embodiment of the present invention will be described below with reference to FIG.

第1図は、本発明になる薄膜アレイ超音波変換器を示し
、aは平面図、bは断面図を示している。
FIG. 1 shows a thin film array ultrasonic transducer according to the present invention, in which a is a plan view and b is a cross-sectional view.

同図において1は石英ガラス基板、2はクロム(Cr)
・金(Au)ilを極、3及び3−1〜3−nは酸化亜
鉛(ZnO)*膜、4及び4−1〜4−nは、アル゛ミ
ニウム(AQ)電極、5及び5−1〜5−nは5i02
からなる音響整合層である。
In the same figure, 1 is a quartz glass substrate, 2 is chromium (Cr)
・Gold (Au) il electrodes, 3 and 3-1 to 3-n are zinc oxide (ZnO)* films, 4 and 4-1 to 4-n are aluminum (AQ) electrodes, 5 and 5- 1-5-n is 5i02
This is an acoustic matching layer consisting of.

第1図に示した超音波変換器の作成手順を第2図により
説明する。まず1石英ガラス基板ll上に220℃でク
ロミウム(Cr)及び金(A u )蒸着し、下部電極
12を形成する(同図a)。次に高周波マグネトロンス
パッタ法により、膜厚30μmの酸化亜鉛薄11113
を形成する(同図b)。
The procedure for creating the ultrasonic transducer shown in FIG. 1 will be explained with reference to FIG. 2. First, chromium (Cr) and gold (A u ) are vapor-deposited onto a quartz glass substrate 11 at 220° C. to form a lower electrode 12 (a in the same figure). Next, a thin film of zinc oxide 11113 with a thickness of 30 μm was formed by high-frequency magnetron sputtering.
(Figure b).

スパッタ条件は、パワー75Wで基板温度220℃、ア
ルゴン(Ar)−酸素(02)(50%−50%)導入
ガスのガス圧を3Pa (パスカル)とした。
The sputtering conditions were a power of 75 W, a substrate temperature of 220° C., and a gas pressure of argon (Ar)-oxygen (02) (50%-50%) introduced gas of 3 Pa (Pascal).

上記の薄膜13上に、室温でアルミニウム(AQ)を蒸
着し、上部電極14を形成する(同図c)、さらに、高
周波マグネトロンスパッタ法により膜厚約15μmの酸
化シリコン(SiO2)膜を音響整合M!j15として
形成する(同図d)。
Aluminum (AQ) is vapor-deposited on the thin film 13 at room temperature to form the upper electrode 14 (see figure c). Furthermore, a silicon oxide (SiO2) film with a thickness of approximately 15 μm is acoustically matched by high-frequency magnetron sputtering. M! j15 (d in the same figure).

スパッタ条件はパワー200Wで、基板温度200℃、
アルゴン(Ar)−酸素(90%−10%)導入ガスの
ガス圧を5Paとした。この条件でスパッタ時間は7時
間である。
The sputtering conditions were a power of 200W, a substrate temperature of 200℃,
The gas pressure of the argon (Ar)-oxygen (90%-10%) introduced gas was 5 Pa. Under these conditions, the sputtering time was 7 hours.

上記の一様な多層膜をアレイ変換器に加工するため、以
下のようにエツチングを行う。まず、フォトリソグラフ
ィ技術を用いて、ピッチ60μm、エレメント幅50μ
m、溝幅10μm、短軸方向の長さ1mmのレジストパ
ターン16−1〜16− nを形成する(同図8)、こ
のレジストパターンをマスクとして、フッ酸(HF)及
びフッ化アンモニウム(’N H3F )の混合液(混
合比l:6)中で1時間エツチングを行い、酸化シリコ
ン膜15をパターニングする(同図f)、レジストを除
去した後、パターニングされた酸化シリコン膜15をマ
スクとしてアルミニウムのエツチング液(リン酸、硝酸
、氷酢酸、水=75:5:15:5の混合液)中で2分
間エツチングを行い、アルミニウム膜14をパターニン
グする(同図g)。
In order to process the above uniform multilayer film into an array transducer, etching is performed as follows. First, using photolithography technology, the pitch was 60 μm and the element width was 50 μm.
Resist patterns 16-1 to 16-n with a groove width of 10 μm and a length of 1 mm in the minor axis direction are formed (FIG. 8). Using this resist pattern as a mask, hydrofluoric acid (HF) and ammonium fluoride (' The silicon oxide film 15 is patterned by etching for 1 hour in a mixed solution of N H3F (mixing ratio 1:6) (f in the same figure). After removing the resist, the patterned silicon oxide film 15 is used as a mask. Etching is performed for 2 minutes in an aluminum etching solution (a mixture of phosphoric acid, nitric acid, glacial acetic acid, and water = 75:5:15:5) to pattern the aluminum film 14 (see g in the figure).

さらに、2%の塩酸水溶液中で5分間エツチングを行い
酸化亜鉛薄膜13をパターニングする(同(i21h)
 、最後に、各素子からのリード線引出し部となる上部
電極14−1.2.・・・、nの一部を露出させるため
、その上の整合層を除去する。
Furthermore, the zinc oxide thin film 13 is patterned by etching in a 2% hydrochloric acid aqueous solution for 5 minutes (same (i21h)).
, and finally, upper electrodes 14-1.2, which serve as lead wire extraction parts from each element. . . ., the matching layer thereon is removed to expose a portion of n.

以上のようにして、第1図に示した薄膜アレイ変換器が
構成される。この方法では、微細パターンの形成が1回
で済むため、マスク合わせの精度も必要としない、この
変換器の下部電極及び上部電極4−1〜4−nよりワイ
ヤボンディングによりリード線を引出す。
In the manner described above, the thin film array transducer shown in FIG. 1 is constructed. In this method, since the fine pattern is formed only once, precision in mask alignment is not required.Lead wires are drawn out from the lower electrodes and upper electrodes 4-1 to 4-n of this converter by wire bonding.

この状態において、下部電極、酸化亜鉛薄膜3−1〜3
− n 、上部電極4−1〜4− n 、音響整合層5
−1〜5−nより成るn個のエレメントを複数個ずつま
とめ、各々に中心部はど遅れた位相差を与えて駆動して
音波を放射させ、そのビームの測定を行ったところ、ア
レイの配列方向に鋭いビーム形状となった。さらに複数
ごとに順次切換えて駆動することによりビームを走査で
きることが確認できた。これはエツチングにより各エレ
メントが分離され、独立に動作できるためである。
In this state, the lower electrode, zinc oxide thin film 3-1 to 3
-n, upper electrodes 4-1 to 4-n, acoustic matching layer 5
When a plurality of n elements consisting of -1 to 5-n were grouped together, each was driven with a delayed phase difference at the center to emit a sound wave, and the beam was measured. The beam has a sharp shape in the array direction. Furthermore, it was confirmed that the beam could be scanned by sequentially switching and driving multiple units. This is because each element is separated by etching and can operate independently.

第3図は1本発明の第2実施例である薄膜アレイ変換器
の平面および断面を示す図である。第3図において、2
1は基板、22−1〜22−nは下部電極23−1〜2
3− nは酸化亜鉛(ZnO)薄膜、24−1〜24−
nはアルミニウム(AQ)膜、25は金膜、26−1〜
26−nは溶融石英(SiOs+)膜である。
FIG. 3 is a plan view and a cross-sectional view of a thin film array transducer according to a second embodiment of the present invention. In Figure 3, 2
1 is a substrate, 22-1 to 22-n are lower electrodes 23-1 to 2
3-n is a zinc oxide (ZnO) thin film, 24-1 to 24-
n is aluminum (AQ) film, 25 is gold film, 26-1~
26-n is a fused silica (SiOs+) film.

このアレイ変換器の製作は、前述の第1の実施例とほぼ
同様にして行う。但し、この第2の実施例においては下
部電極が各素子を分離している電極であり、上部電極が
共通電極となっている点が異なる。まず石英ガラス基板
1上にクロム(Cr)及び金(A u )よりなる電極
を形成し、素子幅と同じかそれより広い幅を有する部分
22−1〜22−nに分割する。この上に酸化亜鉛(Z
nO)薄11123.アルミニウム(AQ)電極24を
形成する。さらにその一部を金(Au)膜25で覆う。
This array transducer is manufactured in substantially the same manner as in the first embodiment described above. However, this second embodiment differs in that the lower electrode is an electrode that separates each element, and the upper electrode is a common electrode. First, an electrode made of chromium (Cr) and gold (Au) is formed on a quartz glass substrate 1, and is divided into portions 22-1 to 22-n each having a width equal to or wider than the device width. On top of this, zinc oxide (Z
nO) Thin 11123. An aluminum (AQ) electrode 24 is formed. Furthermore, a part of it is covered with a gold (Au) film 25.

この金膜はアルミニウムをエツチングする際のマスクの
役割を果たす。さらにアルミニウム膜上に溶融石英(S
iOz)膜26を形成し、下部電極22−1〜22−n
と位置合わせをして、ピッチ60μm2幅50μm、長
さ1mmのライン状レジストパターンを形成し、以下第
1の実施例と同様に順次エツチングを行えば良い。この
方法では溶融石英膜26を2度に分けてエツチングする
必要がない。また、基板上に形成された下部電極がリー
ド線引出しの際のポンディングパッドとなり、充分な強
度が得られるという利点がある。
This gold film serves as a mask when etching aluminum. Furthermore, fused silica (S) is placed on the aluminum film.
iOz) film 26 is formed, and the lower electrodes 22-1 to 22-n
A line-shaped resist pattern having a pitch of 60 μm, a width of 50 μm, and a length of 1 mm is formed by aligning the pattern with the resist pattern, and then etching is performed sequentially in the same manner as in the first embodiment. This method eliminates the need to etch the fused silica film 26 twice. Further, the lower electrode formed on the substrate serves as a bonding pad when drawing out lead wires, and there is an advantage that sufficient strength can be obtained.

〔発明の効果〕〔Effect of the invention〕

以上説明したように、本発明によれば、音?[金層まで
一様に形成した後、順次エツチングを行っているので、
フォトリソグラフィーによる微細パターンの形成が1回
で済み、アレイ変換器の作成工程を少なくすることが可
能である。
As explained above, according to the present invention, sound? [After uniformly forming the gold layer, etching is performed sequentially, so
Formation of a fine pattern by photolithography only needs to be done once, and it is possible to reduce the number of steps for creating an array converter.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は本発明の実施例である超音波薄膜アレイ変換器
の平面図(a)及び断面図(b)、第2図は本発明の超
音波変換器の作成手順を示す加工工程断面図、第3図は
本発明の他の実施例である超音波薄膜アレイ変換器の平
面図(a)及び断面図(b)である。 1.11.’21・・・基板、2,12,22・・・下
部電極、3,13.23・・・酸化亜鉛薄膜、4.14
・・・上部電極、5,15.26・・・音響整合層、2
4・・・アルミニウム膜、25・・・金膜。 肯 11!1 汁 2 図
FIG. 1 is a plan view (a) and a cross-sectional view (b) of an ultrasonic thin film array transducer according to an embodiment of the present invention, and FIG. 2 is a cross-sectional view of the processing steps showing the steps for manufacturing the ultrasonic transducer of the present invention. , FIG. 3 is a plan view (a) and a cross-sectional view (b) of an ultrasonic thin film array transducer according to another embodiment of the present invention. 1.11. '21...Substrate, 2,12,22...Lower electrode, 3,13.23...Zinc oxide thin film, 4.14
... Upper electrode, 5, 15.26 ... Acoustic matching layer, 2
4... Aluminum film, 25... Gold film. Confirmation 11!1 Juice 2 Diagram

Claims (5)

【特許請求の範囲】[Claims] 1.下部電極の形成された基板上に、圧電体からなる薄
膜、該薄膜上に形成された上部電極、および該上部電極
上に形成された音響整合層より成る素子を多数配列した
薄膜アレイ超音波変換器において、音響整合層まで含め
た上記素子を基板上に一様に形成した後、順次アレイ状
にエッチングしたことを特徴とする薄膜アレイ超音波変
換器。
1. A thin film array ultrasonic transducer in which a large number of elements each consisting of a thin film made of a piezoelectric material, an upper electrode formed on the thin film, and an acoustic matching layer formed on the upper electrode are arranged on a substrate on which a lower electrode is formed. 1. A thin film array ultrasonic transducer characterized in that the above elements including an acoustic matching layer are uniformly formed on a substrate and then sequentially etched in an array shape.
2.前記圧電体に、酸化亜鉛(ZnO)を用いることを
特徴とする特許請求の範囲第1項記載の薄膜アレイ超音
波変換器。
2. 2. The thin film array ultrasonic transducer according to claim 1, wherein zinc oxide (ZnO) is used for the piezoelectric material.
3.前記音響整合層に、溶融石英(SiO_2)を用い
ることを特徴とする特許請求の範囲第1項記載の薄膜ア
レイ超音波変換器。
3. 2. The thin film array ultrasonic transducer according to claim 1, wherein fused silica (SiO_2) is used for the acoustic matching layer.
4.前記基板に溶融石英(SiO_2)を用いることを
特徴とする特許請求の範囲第2項記載の薄膜アレイ超音
波変換器。
4. 3. The thin film array ultrasonic transducer according to claim 2, wherein fused silica (SiO_2) is used for the substrate.
5.前記基板にAl_2O_3を用いることを特徴とす
る特許請求の範囲第2項記載の薄膜アレイ超音波変換器
5. 3. The thin film array ultrasonic transducer according to claim 2, wherein Al_2O_3 is used for the substrate.
JP62257223A 1987-10-14 1987-10-14 Manufacturing method of thin film array ultrasonic transducer Expired - Lifetime JP2620945B2 (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5038068A (en) * 1988-12-09 1991-08-06 Hitachi Construction Machinery Co., Ltd. Thin film pattern and method of forming the same
US7726192B2 (en) 2006-10-04 2010-06-01 Denso Corporation Ultrasonic sensor
CN111559734A (en) * 2020-05-20 2020-08-21 内江师范学院 Manufacturing method of multi-frequency CMUT device and multi-frequency CMUT device

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60128769A (en) * 1983-12-16 1985-07-09 Nippon Telegr & Teleph Corp <Ntt> Communication conference device
JPS6115500A (en) * 1984-07-02 1986-01-23 Tdk Corp Manufacture of ultrasonic probe

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60128769A (en) * 1983-12-16 1985-07-09 Nippon Telegr & Teleph Corp <Ntt> Communication conference device
JPS6115500A (en) * 1984-07-02 1986-01-23 Tdk Corp Manufacture of ultrasonic probe

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5038068A (en) * 1988-12-09 1991-08-06 Hitachi Construction Machinery Co., Ltd. Thin film pattern and method of forming the same
US7726192B2 (en) 2006-10-04 2010-06-01 Denso Corporation Ultrasonic sensor
CN111559734A (en) * 2020-05-20 2020-08-21 内江师范学院 Manufacturing method of multi-frequency CMUT device and multi-frequency CMUT device

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