JPH0116817B2 - - Google Patents

Info

Publication number: JPH0116817B2
Authority: JP; Japan
Prior art keywords: methacrylic acid; acid chloride; mol; main component; liquid
Prior art date: 1985-02-14
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP2524285A

Other languages

English (en)

Japanese (ja)

Other versions

JPS61186345A (ja

Inventor

Tatsuto Matsuda

Tadao Kondo

Hiroshi Sugisawa

Norio Takatani

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Nippon Shokubai Co Ltd

Original Assignee

Nippon Shokubai Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-02-14

Filing date

1985-02-14

Publication date

1989-03-27

1985-02-14 Application filed by Nippon Shokubai Co Ltd filed Critical Nippon Shokubai Co Ltd

1985-02-14 Priority to JP2524285A priority Critical patent/JPS61186345A/ja

1986-08-20 Publication of JPS61186345A publication Critical patent/JPS61186345A/ja

1989-03-27 Publication of JPH0116817B2 publication Critical patent/JPH0116817B2/ja

Status Granted legal-status Critical Current

Links

CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 54
VHRYZQNGTZXDNX-UHFFFAOYSA-N methacryloyl chloride Chemical compound CC(=C)C(Cl)=O VHRYZQNGTZXDNX-UHFFFAOYSA-N 0.000 claims description 34
239000007788 liquid Substances 0.000 claims description 28
FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 claims description 17
238000000034 method Methods 0.000 claims description 16
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
238000006243 chemical reaction Methods 0.000 claims description 12
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
239000011541 reaction mixture Substances 0.000 claims description 6
229910052698 phosphorus Inorganic materials 0.000 claims description 5
239000011574 phosphorus Substances 0.000 claims description 5
-1 phosphorus compound Chemical class 0.000 claims description 4
238000011084 recovery Methods 0.000 description 10
238000004821 distillation Methods 0.000 description 9
238000003756 stirring Methods 0.000 description 9
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
238000004519 manufacturing process Methods 0.000 description 6
238000001816 cooling Methods 0.000 description 5
238000004445 quantitative analysis Methods 0.000 description 4
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
230000000694 effects Effects 0.000 description 3
238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 3
WJFKNYWRSNBZNX-UHFFFAOYSA-N 10H-phenothiazine Chemical compound C1=CC=C2NC3=CC=CC=C3SC2=C1 WJFKNYWRSNBZNX-UHFFFAOYSA-N 0.000 description 2
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
229950000688 phenothiazine Drugs 0.000 description 2
238000010992 reflux Methods 0.000 description 2
238000005481 NMR spectroscopy Methods 0.000 description 1
GIGSZJOUTBMCNR-UHFFFAOYSA-N P(O)(O)O.C(C(=C)C)(=O)O Chemical compound P(O)(O)O.C(C(=C)C)(=O)O GIGSZJOUTBMCNR-UHFFFAOYSA-N 0.000 description 1
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
238000005917 acylation reaction Methods 0.000 description 1
239000003905 agrochemical Substances 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
230000018044 dehydration Effects 0.000 description 1
238000006297 dehydration reaction Methods 0.000 description 1
239000003814 drug Substances 0.000 description 1
229920001002 functional polymer Polymers 0.000 description 1
239000000417 fungicide Substances 0.000 description 1
238000009776 industrial production Methods 0.000 description 1
239000000543 intermediate Substances 0.000 description 1
239000000203 mixture Substances 0.000 description 1
150000003018 phosphorus compounds Chemical class 0.000 description 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
239000002994 raw material Substances 0.000 description 1
239000003507 refrigerant Substances 0.000 description 1
230000002194 synthesizing effect Effects 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

JP2524285A 1985-02-14 1985-02-14 メタクリル酸の回収方法 Granted JPS61186345A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP2524285A JPS61186345A (ja)	1985-02-14	1985-02-14	メタクリル酸の回収方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP2524285A JPS61186345A (ja)	1985-02-14	1985-02-14	メタクリル酸の回収方法

Publications (2)

Publication Number	Publication Date
JPS61186345A JPS61186345A (ja)	1986-08-20
JPH0116817B2 true JPH0116817B2 (fr)	1989-03-27

Family

ID=12160513

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP2524285A Granted JPS61186345A (ja)	1985-02-14	1985-02-14	メタクリル酸の回収方法

Country Status (1)

Country	Link
JP (1)	JPS61186345A (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2002047280A (ja) *	2000-08-02	2002-02-12	Mitsubishi Rayon Co Ltd	ラクトン（メタ）アクリレート類の製造方法

1985
- 1985-02-14 JP JP2524285A patent/JPS61186345A/ja active Granted

Also Published As

Publication number	Publication date
JPS61186345A (ja)	1986-08-20

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