JPH02209500A - NiまたはNi合金めっき廃液の再生方法 - Google Patents
NiまたはNi合金めっき廃液の再生方法Info
- Publication number
- JPH02209500A JPH02209500A JP2917789A JP2917789A JPH02209500A JP H02209500 A JPH02209500 A JP H02209500A JP 2917789 A JP2917789 A JP 2917789A JP 2917789 A JP2917789 A JP 2917789A JP H02209500 A JPH02209500 A JP H02209500A
- Authority
- JP
- Japan
- Prior art keywords
- plating
- rare earth
- earth metal
- solution
- plating soln
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000007747 plating Methods 0.000 title claims abstract description 68
- 229910000990 Ni alloy Inorganic materials 0.000 title claims abstract description 7
- 238000000034 method Methods 0.000 title claims description 12
- 230000001172 regenerating effect Effects 0.000 title claims description 7
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 27
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 26
- -1 rare earth metal ions Chemical class 0.000 claims abstract description 26
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 9
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 claims abstract description 8
- 229910000287 alkaline earth metal oxide Inorganic materials 0.000 claims abstract description 8
- 239000002699 waste material Substances 0.000 claims description 22
- 239000002253 acid Substances 0.000 claims description 6
- 229910045601 alloy Inorganic materials 0.000 claims description 6
- 239000000956 alloy Substances 0.000 claims description 6
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract description 4
- 150000001342 alkaline earth metals Chemical class 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract description 4
- RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 abstract description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract description 2
- 229910001863 barium hydroxide Inorganic materials 0.000 abstract description 2
- 150000002500 ions Chemical class 0.000 abstract description 2
- 230000001376 precipitating effect Effects 0.000 abstract 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 33
- 239000000243 solution Substances 0.000 description 32
- 239000007788 liquid Substances 0.000 description 12
- 239000000654 additive Substances 0.000 description 7
- 230000002378 acidificating effect Effects 0.000 description 5
- 229910001172 neodymium magnet Inorganic materials 0.000 description 5
- 239000002244 precipitate Substances 0.000 description 5
- 230000000996 additive effect Effects 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 150000004679 hydroxides Chemical class 0.000 description 2
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 2
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 2
- 150000002910 rare earth metals Chemical class 0.000 description 2
- 238000011282 treatment Methods 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- 229910000521 B alloy Inorganic materials 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- NINOVVRCHXVOKB-UHFFFAOYSA-N dialuminum;dioxido(dioxo)chromium Chemical compound [Al+3].[Al+3].[O-][Cr]([O-])(=O)=O.[O-][Cr]([O-])(=O)=O.[O-][Cr]([O-])(=O)=O NINOVVRCHXVOKB-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 150000004687 hexahydrates Chemical class 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- LAIZPRYFQUWUBN-UHFFFAOYSA-L nickel chloride hexahydrate Chemical compound O.O.O.O.O.O.[Cl-].[Cl-].[Ni+2] LAIZPRYFQUWUBN-UHFFFAOYSA-L 0.000 description 1
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
Landscapes
- Manufacture And Refinement Of Metals (AREA)
- Removal Of Specific Substances (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2917789A JPH02209500A (ja) | 1989-02-08 | 1989-02-08 | NiまたはNi合金めっき廃液の再生方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2917789A JPH02209500A (ja) | 1989-02-08 | 1989-02-08 | NiまたはNi合金めっき廃液の再生方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH02209500A true JPH02209500A (ja) | 1990-08-20 |
| JPH0469240B2 JPH0469240B2 (2) | 1992-11-05 |
Family
ID=12268947
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2917789A Granted JPH02209500A (ja) | 1989-02-08 | 1989-02-08 | NiまたはNi合金めっき廃液の再生方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH02209500A (2) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013047340A1 (ja) * | 2011-09-28 | 2013-04-04 | 日立金属株式会社 | 電気ニッケルめっき液中の希土類不純物の除去方法 |
| JP2013173993A (ja) * | 2012-02-27 | 2013-09-05 | Hitachi Metals Ltd | 電気ニッケルめっき液中の希土類不純物の除去方法 |
| JP2014185373A (ja) * | 2013-03-25 | 2014-10-02 | Hitachi Metals Ltd | 電気ニッケルめっき液中の希土類不純物の除去装置 |
| WO2014156767A1 (ja) * | 2013-03-25 | 2014-10-02 | 日立金属株式会社 | 電気ニッケルめっき液中の希土類不純物の除去方法 |
| WO2014156761A1 (ja) * | 2013-03-25 | 2014-10-02 | 日立金属株式会社 | 電気ニッケルめっき液中の希土類不純物の除去方法 |
-
1989
- 1989-02-08 JP JP2917789A patent/JPH02209500A/ja active Granted
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPWO2013047340A1 (ja) * | 2011-09-28 | 2015-03-26 | 日立金属株式会社 | 電気ニッケルめっき液中の希土類不純物の除去方法 |
| CN103842561A (zh) * | 2011-09-28 | 2014-06-04 | 日立金属株式会社 | 镍电镀液中的稀土杂质的除去方法 |
| WO2013047340A1 (ja) * | 2011-09-28 | 2013-04-04 | 日立金属株式会社 | 電気ニッケルめっき液中の希土類不純物の除去方法 |
| US9695524B2 (en) | 2011-09-28 | 2017-07-04 | Hitachi Metals, Ltd. | Method for removing rare earth impurities from nickel-electroplating solution |
| EP2749674A4 (en) * | 2011-09-28 | 2015-08-19 | Hitachi Metals Ltd | METHOD FOR REMOVING RARE DEHUMIDIFICATION IN A SOLUTION FOR ELECTROLYTIC NICKELING |
| JP2013173993A (ja) * | 2012-02-27 | 2013-09-05 | Hitachi Metals Ltd | 電気ニッケルめっき液中の希土類不純物の除去方法 |
| JP2014185373A (ja) * | 2013-03-25 | 2014-10-02 | Hitachi Metals Ltd | 電気ニッケルめっき液中の希土類不純物の除去装置 |
| WO2014156761A1 (ja) * | 2013-03-25 | 2014-10-02 | 日立金属株式会社 | 電気ニッケルめっき液中の希土類不純物の除去方法 |
| CN105051263A (zh) * | 2013-03-25 | 2015-11-11 | 日立金属株式会社 | 镍电镀液中的稀土类杂质的除去方法 |
| CN105051264A (zh) * | 2013-03-25 | 2015-11-11 | 日立金属株式会社 | 镍电镀液中的稀土类杂质的除去方法 |
| WO2014156767A1 (ja) * | 2013-03-25 | 2014-10-02 | 日立金属株式会社 | 電気ニッケルめっき液中の希土類不純物の除去方法 |
| US9771664B2 (en) | 2013-03-25 | 2017-09-26 | Hitachi Metals, Ltd. | Method for removing rare earth impurities from nickel-electroplating solution |
| US9873953B2 (en) | 2013-03-25 | 2018-01-23 | Hitachi Metals, Ltd. | Method for removing rare earth impurities from nickel-electroplating solution |
| CN105051264B (zh) * | 2013-03-25 | 2018-05-29 | 日立金属株式会社 | 镍电镀液中的稀土类杂质的除去方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0469240B2 (2) | 1992-11-05 |
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