JPH0339074B2 - - Google Patents

Info

Publication number: JPH0339074B2
Authority: JP; Japan
Prior art keywords: ammonia; phosphoric acid; maap; acetylation; daap
Prior art date: 1983-01-28
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP1227583A

Other languages

English (en)

Japanese (ja)

Other versions

JPS59139391A (ja

Inventor

Yoichiro Ueda

Tatsuo Goto

Mitsuru Murai

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Daicel Corp

Original Assignee

Daicel Chemical Industries Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-01-28

Filing date

1983-01-28

Publication date

1991-06-12

1983-01-28 Application filed by Daicel Chemical Industries Ltd filed Critical Daicel Chemical Industries Ltd

1983-01-28 Priority to JP1227583A priority Critical patent/JPS59139391A/ja

1984-08-10 Publication of JPS59139391A publication Critical patent/JPS59139391A/ja

1991-06-12 Publication of JPH0339074B2 publication Critical patent/JPH0339074B2/ja

Status Granted legal-status Critical Current

Links

QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 120
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 110
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 87
WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical group CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims description 66
229910021529 ammonia Inorganic materials 0.000 claims description 60
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 55
238000006640 acetylation reaction Methods 0.000 claims description 37
230000021736 acetylation Effects 0.000 claims description 28
239000002904 solvent Substances 0.000 claims description 28
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
LIPOUNRJVLNBCD-UHFFFAOYSA-N acetyl dihydrogen phosphate Chemical compound CC(=O)OP(O)(O)=O LIPOUNRJVLNBCD-UHFFFAOYSA-N 0.000 claims description 19
238000000034 method Methods 0.000 claims description 17
150000003839 salts Chemical class 0.000 claims description 13
239000012345 acetylating agent Substances 0.000 claims description 10
230000000397 acetylating effect Effects 0.000 claims description 9
239000011541 reaction mixture Substances 0.000 claims description 9
-1 acetate ester Chemical class 0.000 claims description 5
239000012452 mother liquor Substances 0.000 claims description 5
238000004519 manufacturing process Methods 0.000 claims description 3
239000003795 chemical substances by application Substances 0.000 claims 1
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 78
235000011007 phosphoric acid Nutrition 0.000 description 54
IZASLLIUFQPKOG-UHFFFAOYSA-N diazanium;acetyl phosphate Chemical compound [NH4+].[NH4+].CC(=O)OP([O-])([O-])=O IZASLLIUFQPKOG-UHFFFAOYSA-N 0.000 description 39
239000000243 solution Substances 0.000 description 23
239000013078 crystal Substances 0.000 description 20
238000006243 chemical reaction Methods 0.000 description 19
239000002244 precipitate Substances 0.000 description 18
239000000047 product Substances 0.000 description 18
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 17
238000001556 precipitation Methods 0.000 description 15
238000000926 separation method Methods 0.000 description 13
DLFVBJFMPXGRIB-UHFFFAOYSA-N Acetamide Chemical compound CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 description 10
238000010521 absorption reaction Methods 0.000 description 8
239000012535 impurity Substances 0.000 description 8
239000000203 mixture Substances 0.000 description 8
230000000052 comparative effect Effects 0.000 description 7
239000007788 liquid Substances 0.000 description 6
USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 5
239000005695 Ammonium acetate Substances 0.000 description 5
229940043376 ammonium acetate Drugs 0.000 description 5
235000019257 ammonium acetate Nutrition 0.000 description 5
150000003863 ammonium salts Chemical class 0.000 description 5
230000001376 precipitating effect Effects 0.000 description 5
239000007787 solid Substances 0.000 description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 4
229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 description 4
239000007864 aqueous solution Substances 0.000 description 4
150000001875 compounds Chemical class 0.000 description 4
238000006911 enzymatic reaction Methods 0.000 description 4
235000019837 monoammonium phosphate Nutrition 0.000 description 4
229910052757 nitrogen Inorganic materials 0.000 description 4
239000004254 Ammonium phosphate Substances 0.000 description 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
229910000148 ammonium phosphate Inorganic materials 0.000 description 3
235000019289 ammonium phosphates Nutrition 0.000 description 3
239000007795 chemical reaction product Substances 0.000 description 3
MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 3
CCGKOQOJPYTBIH-UHFFFAOYSA-N ethenone Chemical compound C=C=O CCGKOQOJPYTBIH-UHFFFAOYSA-N 0.000 description 3
239000007789 gas Substances 0.000 description 3
239000012456 homogeneous solution Substances 0.000 description 3
239000002994 raw material Substances 0.000 description 3
238000003756 stirring Methods 0.000 description 3
238000003860 storage Methods 0.000 description 3
ZKHQWZAMYRWXGA-KQYNXXCUSA-J ATP(4-) Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](COP([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O)[C@@H](O)[C@H]1O ZKHQWZAMYRWXGA-KQYNXXCUSA-J 0.000 description 2
ZKHQWZAMYRWXGA-UHFFFAOYSA-N Adenosine triphosphate Natural products C1=NC=2C(N)=NC=NC=2N1C1OC(COP(O)(=O)OP(O)(=O)OP(O)(O)=O)C(O)C1O ZKHQWZAMYRWXGA-UHFFFAOYSA-N 0.000 description 2
ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 2
XLYOFNOQVPJJNP-ZSJDYOACSA-N Heavy water Chemical compound [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 description 2
BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 description 2
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 2
125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 2
KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 2
150000001298 alcohols Chemical class 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
239000012295 chemical reaction liquid Substances 0.000 description 2
238000001816 cooling Methods 0.000 description 2
238000001035 drying Methods 0.000 description 2
238000000921 elemental analysis Methods 0.000 description 2
238000001914 filtration Methods 0.000 description 2
JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropanol acetate Natural products CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 description 2
229940011051 isopropyl acetate Drugs 0.000 description 2
GWYFCOCPABKNJV-UHFFFAOYSA-N isovaleric acid Chemical compound CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 description 2
229910052698 phosphorus Inorganic materials 0.000 description 2
239000011574 phosphorus Substances 0.000 description 2
230000000704 physical effect Effects 0.000 description 2
230000035484 reaction time Effects 0.000 description 2
239000000126 substance Substances 0.000 description 2
238000005406 washing Methods 0.000 description 2
RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
SVONRAPFKPVNKG-UHFFFAOYSA-N 2-ethoxyethyl acetate Chemical compound CCOCCOC(C)=O SVONRAPFKPVNKG-UHFFFAOYSA-N 0.000 description 1
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 description 1
UUIQMZJEGPQKFD-UHFFFAOYSA-N Methyl butyrate Chemical compound CCCC(=O)OC UUIQMZJEGPQKFD-UHFFFAOYSA-N 0.000 description 1
XLLNINGEDIOQGQ-UHFFFAOYSA-N [acetyloxy(hydroxy)phosphoryl] acetate Chemical class CC(=O)OP(O)(=O)OC(C)=O XLLNINGEDIOQGQ-UHFFFAOYSA-N 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
150000001242 acetic acid derivatives Chemical class 0.000 description 1
150000001408 amides Chemical class 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
OZMZHCTWGFIXGY-UHFFFAOYSA-N azane;phosphono acetate Chemical compound N.CC(=O)OP(O)(O)=O OZMZHCTWGFIXGY-UHFFFAOYSA-N 0.000 description 1
QAENJDPUIACIKD-UHFFFAOYSA-N azanium;diacetyl phosphate Chemical compound [NH4+].CC(=O)OP([O-])(=O)OC(C)=O QAENJDPUIACIKD-UHFFFAOYSA-N 0.000 description 1
238000007664 blowing Methods 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
239000007810 chemical reaction solvent Substances 0.000 description 1
230000008878 coupling Effects 0.000 description 1
238000010168 coupling process Methods 0.000 description 1
238000005859 coupling reaction Methods 0.000 description 1
238000005520 cutting process Methods 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
JBIJMTLVUKEXJO-UHFFFAOYSA-N diacetyloxyphosphoryl acetate Chemical class CC(=O)OP(=O)(OC(C)=O)OC(C)=O JBIJMTLVUKEXJO-UHFFFAOYSA-N 0.000 description 1
238000007865 diluting Methods 0.000 description 1
YWEUIGNSBFLMFL-UHFFFAOYSA-N diphosphonate Chemical compound O=P(=O)OP(=O)=O YWEUIGNSBFLMFL-UHFFFAOYSA-N 0.000 description 1
XPPKVPWEQAFLFU-UHFFFAOYSA-N diphosphoric acid Chemical class OP(O)(=O)OP(O)(O)=O XPPKVPWEQAFLFU-UHFFFAOYSA-N 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000001952 enzyme assay Methods 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
238000000227 grinding Methods 0.000 description 1
230000020169 heat generation Effects 0.000 description 1
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
238000009776 industrial production Methods 0.000 description 1
238000011081 inoculation Methods 0.000 description 1
229910052744 lithium Inorganic materials 0.000 description 1
230000007774 longterm Effects 0.000 description 1
229910001425 magnesium ion Inorganic materials 0.000 description 1
239000012457 nonaqueous media Substances 0.000 description 1
DLYUQMMRRRQYAE-UHFFFAOYSA-N phosphorus pentoxide Inorganic materials O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 1
239000000843 powder Substances 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
238000005809 transesterification reaction Methods 0.000 description 1

JP1227583A 1983-01-28 1983-01-28 アセチルリン酸塩の製法 Granted JPS59139391A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP1227583A JPS59139391A (ja)	1983-01-28	1983-01-28	アセチルリン酸塩の製法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP1227583A JPS59139391A (ja)	1983-01-28	1983-01-28	アセチルリン酸塩の製法

Publications (2)

Publication Number	Publication Date
JPS59139391A JPS59139391A (ja)	1984-08-10
JPH0339074B2 true JPH0339074B2 (cs)	1991-06-12

Family

ID=11800811

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP1227583A Granted JPS59139391A (ja)	1983-01-28	1983-01-28	アセチルリン酸塩の製法

Country Status (1)

Country	Link
JP (1)	JPS59139391A (cs)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO2000056693A1 (en) *	1999-03-22	2000-09-28	Purac Biochem B.V.	Method of industrial-scale purification of lactic acid
PL364886A1 (en)	1999-07-28	2004-12-27	Monsanto Technology Llc	Process for making a downstream processable ammonium glyphosate paste

1983
- 1983-01-28 JP JP1227583A patent/JPS59139391A/ja active Granted

Also Published As

Publication number	Publication date
JPS59139391A (ja)	1984-08-10

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