JPH0363801B2 - - Google Patents
Info
- Publication number
- JPH0363801B2 JPH0363801B2 JP7536384A JP7536384A JPH0363801B2 JP H0363801 B2 JPH0363801 B2 JP H0363801B2 JP 7536384 A JP7536384 A JP 7536384A JP 7536384 A JP7536384 A JP 7536384A JP H0363801 B2 JPH0363801 B2 JP H0363801B2
- Authority
- JP
- Japan
- Prior art keywords
- laser
- magnetic
- magnetizing
- recording medium
- magnetic recording
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 230000005415 magnetization Effects 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- 230000005405 multipole Effects 0.000 claims description 5
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 4
- 229910016036 BaF 2 Inorganic materials 0.000 claims description 3
- 229910004261 CaF 2 Inorganic materials 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- SBIBMFFZSBJNJF-UHFFFAOYSA-N selenium;zinc Chemical compound [Se]=[Zn] SBIBMFFZSBJNJF-UHFFFAOYSA-N 0.000 claims description 3
- 229910017768 LaF 3 Inorganic materials 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- 238000010521 absorption reaction Methods 0.000 claims 3
- 239000000126 substance Substances 0.000 claims 2
- 239000011248 coating agent Substances 0.000 claims 1
- 238000000576 coating method Methods 0.000 claims 1
- PQXKHYXIUOZZFA-UHFFFAOYSA-M lithium fluoride Inorganic materials [Li+].[F-] PQXKHYXIUOZZFA-UHFFFAOYSA-M 0.000 claims 1
- 229910052950 sphalerite Inorganic materials 0.000 claims 1
- 229910052984 zinc sulfide Inorganic materials 0.000 claims 1
- 230000005347 demagnetization Effects 0.000 description 5
- 239000010949 copper Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000696 magnetic material Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 238000004544 sputter deposition Methods 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- PSNPEOOEWZZFPJ-UHFFFAOYSA-N alumane;yttrium Chemical compound [AlH3].[Y] PSNPEOOEWZZFPJ-UHFFFAOYSA-N 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000002223 garnet Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000005381 magnetic domain Effects 0.000 description 1
- 239000011553 magnetic fluid Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229910000938 samarium–cobalt magnet Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F13/00—Apparatus or processes for magnetising or demagnetising
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Recording Or Reproducing By Magnetic Means (AREA)
Description
〔産業上の利用分野〕
本発明は、磁気記録媒体に多極の着磁を行う方
法に関するものである。
〔従来技術とその問題点〕
近年、希土類元素を含む硬質磁性材料が発見さ
れ、高保持力、高エネルギー積を有するため厚膜
化することにより磁気エンコーダやパルスモータ
に適用して高性能化を図る研究が行われている。
このような用途における硬質磁性膜は、多極着
磁して使われ、高性能化に伴いその極幅も小さく
なつている。ところが、この材料はあまりにも保
持力が大きいため、一般に行われている多極着磁
方法では極幅も3mm位が限度である。これを解決
する方法としてレーザによる局部消磁が考えられ
る。
このレーザによる方法は、基体上に形成した希
土類元素を含む磁気記録媒体(硬質磁性膜)をキ
ユーリ温度Tcの0.1〜0.95倍の温度に予熱したあ
と着磁し、その部分を再び着磁することにより多
極着磁を行うものである。しかしながら、希土類
元素を含む磁性材料は非常に酸化されやすいため
加熱すると酸化に基づく特性の低下が生じる。従
つて空気中で処理できないので、高真空装置また
は水素雰囲気装置が必要となり、装置が大がかり
になる。この欠点を解消するため、酸化防止皮膜
として銅メツキをしているが、この膜を付着した
場合、レーザの熱が保護膜に吸収されてしまうの
で消磁が有効に行なわれなかつた。
〔発明の目的〕
本発明は、このような問題点を解消するために
発明されたものであり、多極着磁を効率的に行わ
せる方法を提供することを目的とするものであ
る。
〔発明の構成〕
本発明は、着磁とレーザによる局部消磁を特定
の条件の下で組み合わせて多極着磁を行なうもの
であり、以下に実験例に基づいて説明する。
まずスパツタ法を使い、銅板上にSmCo5膜を
10μm付着したあと、さらに保護膜としてCuまた
はZnSe、LaF3、ZnS、MgF2、LiF、BaF2、
CaF2をそれぞれスパツタ法で3μmの厚さに付け
る。これら8種類の試料について膜の厚さ方向に
25KOeの外部磁界をかけて一方向に着磁した後、
図面に示した装置にセツトする。
試料1は加熱プレート6を設けたX−Y自動テ
ーブル2上にセツトしており、X−Y方向に移動
可能である。試料1の上方には光学系ユニツト3
があり、レーザ発振器本体4からのレーザビーム
の径をレンズ5により調整できるようにしてい
る。
実験は、シングルモードのCO2(炭酸ガス)気
体レーザとYAG(イツトリウム−アルミニウム−
ガーネツト)固体レーザを使用し、ビーム径は前
者で40μm、後者で5μmに調整し、パワー20W、
試料移動速度3mm/s、試料予熱温度300℃の条
件で行なつたあと、磁性流体を使つたビツター法
による磁区の観察を行なつた。熱消磁部は消磁し
なかつた部分の磁界により最初に着磁した方向と
反対向きに着磁されるため、熱消磁が完全かどう
かを調べるためには反対に磁化した部分の幅を調
べればよい。CO2レーザを使用し、ビーム径40μ
mとした場合の結果を第1表に示す。
[Industrial Application Field] The present invention relates to a method for multipolar magnetizing a magnetic recording medium. [Prior art and its problems] In recent years, hard magnetic materials containing rare earth elements have been discovered, and because they have high coercive force and high energy product, they can be applied to magnetic encoders and pulse motors to improve performance by making them thicker. Research is being conducted to Hard magnetic films for such applications are used with multipole magnetization, and the pole width is becoming smaller as performance improves. However, this material has such a large coercive force that the commonly used multi-pole magnetization method limits the pole width to about 3 mm. One possible solution to this problem is local demagnetization using a laser. This laser method involves preheating a magnetic recording medium (hard magnetic film) containing rare earth elements formed on a substrate to a temperature of 0.1 to 0.95 times the Curie temperature Tc, magnetizing it, and then magnetizing that part again. Multi-pole magnetization is performed by this method. However, since magnetic materials containing rare earth elements are highly susceptible to oxidation, when they are heated, their properties deteriorate due to oxidation. Therefore, since the process cannot be carried out in air, a high vacuum device or a hydrogen atmosphere device is required, resulting in a large-scale device. To overcome this drawback, copper plating is applied as an oxidation-preventing film, but when this film is attached, the heat of the laser is absorbed by the protective film, so demagnetization cannot be performed effectively. [Object of the Invention] The present invention was invented to solve these problems, and it is an object of the present invention to provide a method for efficiently performing multi-pole magnetization. [Structure of the Invention] The present invention performs multipolar magnetization by combining magnetization and local demagnetization using a laser under specific conditions, and will be described below based on experimental examples. First, we used the sputtering method to deposit an SmCo 5 film on a copper plate.
After 10μm of adhesion, a protective film of Cu or ZnSe, LaF 3 , ZnS, MgF 2 , LiF, BaF 2 ,
Apply CaF 2 to a thickness of 3 μm using a sputtering method. For these eight types of samples, in the thickness direction of the film
After applying an external magnetic field of 25KOe and magnetizing it in one direction,
Set it in the equipment shown in the drawing. The sample 1 is set on an X-Y automatic table 2 equipped with a heating plate 6, and is movable in the X-Y direction. Above sample 1 is optical system unit 3.
The diameter of the laser beam from the laser oscillator main body 4 can be adjusted by the lens 5. The experiment used a single-mode CO 2 (carbon dioxide) gas laser and YAG (yttrium-aluminum).
Garnet) solid-state laser was used, the beam diameter was adjusted to 40 μm for the former and 5 μm for the latter, the power was 20 W,
After conducting the test under the conditions of a sample moving speed of 3 mm/s and a sample preheating temperature of 300°C, magnetic domains were observed by the Bitter method using a magnetic fluid. The thermally demagnetized part is magnetized in the opposite direction to the initial magnetization direction by the magnetic field of the part that was not demagnetized, so to check whether the thermal demagnetization is complete, you can check the width of the part that is magnetized in the opposite direction. . Uses CO 2 laser, beam diameter 40μ
Table 1 shows the results when m is used.
【表】
また、YAGレーザを使用しビーム径5μmとし
た結果を第2表に示す。[Table] Table 2 also shows the results using a YAG laser with a beam diameter of 5 μm.
【表】【table】
上述したように本発明によれば、熱消磁が効率
的にしかも空気中で行なえるため、希土類元素を
含む磁気記録媒体の多極着磁が可能となるという
効果を奏するものである。
As described above, according to the present invention, thermal demagnetization can be carried out efficiently and in air, so that multipolar magnetization of a magnetic recording medium containing a rare earth element becomes possible.
図面は、本発明の実験に使用したレーザ熱消磁
装置の構成を示す概略図である。
1:試料、2:X−Y自動テーブル、3:光学
系ユニツト、4:レーザ発振器本体、5:レン
ズ、6:加熱プレート。
The drawing is a schematic diagram showing the configuration of a laser thermal demagnetizer used in experiments of the present invention. 1: sample, 2: X-Y automatic table, 3: optical system unit, 4: laser oscillator body, 5: lens, 6: heating plate.
Claims (1)
媒体にレーザ吸収率の小さい材料を被覆し、磁気
記録媒体をキユーリ点温度Tcの0.1倍〜0.95倍の
温度に加熱したあと着磁を行ない、ひきつづきレ
ーザを用いて前記着磁した部分の一部又は複数部
をTc以上に加熱して消磁後、消磁部を再び着磁
することを特徴とする多極着磁方法。 2 レーザ装置をYAGレーザとし、レーザ吸収
率の小さい材料をZnSe、LaF3、ZnS、MgF2、
LiF、BaF2、CaF2の群から選ばれた少なくとも
一種以上の物質とした特許請求の範囲第1項記載
の多極着磁方法。 3 レーザ装置をCO2レーザとし、レーザ吸収率
の小さい材料をZnSe、ZnS、BaF2、CaF2の群か
ら選ばれた少なくとも一種以上の物質とした特許
請求の範囲第2項記載の多極着磁方法。[Claims] 1. After coating a magnetic recording medium containing a rare earth element formed on a substrate with a material having a low laser absorption rate, and heating the magnetic recording medium to a temperature of 0.1 to 0.95 times the Curie point temperature Tc. 1. A multi-pole magnetization method, which comprises magnetizing, then demagnetizing a part or plurality of the magnetized parts using a laser to a temperature above Tc, and then magnetizing the demagnetized parts again. 2 The laser device is a YAG laser, and the materials with low laser absorption are ZnSe, LaF 3 , ZnS, MgF 2 ,
2. The multipolar magnetization method according to claim 1, wherein at least one substance selected from the group consisting of LiF, BaF 2 and CaF 2 is used. 3. The multi-electrode assembly according to claim 2, wherein the laser device is a CO 2 laser, and the material with low laser absorption is at least one substance selected from the group of ZnSe, ZnS, BaF 2 and CaF 2 . magnetic method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7536384A JPS60218809A (en) | 1984-04-14 | 1984-04-14 | Multi-pole magnetization method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7536384A JPS60218809A (en) | 1984-04-14 | 1984-04-14 | Multi-pole magnetization method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60218809A JPS60218809A (en) | 1985-11-01 |
| JPH0363801B2 true JPH0363801B2 (en) | 1991-10-02 |
Family
ID=13574059
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7536384A Granted JPS60218809A (en) | 1984-04-14 | 1984-04-14 | Multi-pole magnetization method |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60218809A (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100345300B1 (en) * | 1999-10-14 | 2002-07-25 | 한국과학기술연구원 | Fabrication Method of SmCo Hard Magnetic Film |
| KR100940721B1 (en) * | 2002-12-28 | 2010-02-08 | 주식회사 포스코 | Magnetic field heat treatment method of electrical steel |
-
1984
- 1984-04-14 JP JP7536384A patent/JPS60218809A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS60218809A (en) | 1985-11-01 |
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