JPH042703A - Manufacture of al-base composite material - Google Patents
Manufacture of al-base composite materialInfo
- Publication number
- JPH042703A JPH042703A JP10431390A JP10431390A JPH042703A JP H042703 A JPH042703 A JP H042703A JP 10431390 A JP10431390 A JP 10431390A JP 10431390 A JP10431390 A JP 10431390A JP H042703 A JPH042703 A JP H042703A
- Authority
- JP
- Japan
- Prior art keywords
- capsule
- composite material
- alloy
- powder
- aluminum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002131 composite material Substances 0.000 title claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 9
- 239000002775 capsule Substances 0.000 claims abstract description 55
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 21
- 239000011812 mixed powder Substances 0.000 claims abstract description 19
- 239000000843 powder Substances 0.000 claims abstract description 17
- 229910000838 Al alloy Inorganic materials 0.000 claims abstract description 15
- 239000012779 reinforcing material Substances 0.000 claims abstract description 10
- 238000001513 hot isostatic pressing Methods 0.000 claims abstract description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 9
- 239000000463 material Substances 0.000 abstract description 14
- 239000011159 matrix material Substances 0.000 abstract description 9
- 238000007872 degassing Methods 0.000 abstract description 7
- 239000000919 ceramic Substances 0.000 abstract description 5
- 239000002245 particle Substances 0.000 abstract description 5
- 238000007789 sealing Methods 0.000 abstract 2
- 238000012856 packing Methods 0.000 abstract 1
- 230000003014 reinforcing effect Effects 0.000 abstract 1
- -1 whisker Substances 0.000 abstract 1
- 229910045601 alloy Inorganic materials 0.000 description 14
- 239000000956 alloy Substances 0.000 description 14
- 238000000465 moulding Methods 0.000 description 7
- 229910001209 Low-carbon steel Inorganic materials 0.000 description 6
- 238000003466 welding Methods 0.000 description 4
- 238000001125 extrusion Methods 0.000 description 3
- 238000005520 cutting process Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229910052581 Si3N4 Inorganic materials 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000011268 mixed slurry Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000013585 weight reducing agent Substances 0.000 description 1
Landscapes
- Powder Metallurgy (AREA)
Abstract
Description
【発明の詳細な説明】
（産業上の利用分野）
本発明は熱間等方圧加圧（以下、ＨＩＰという。）によ
り固化成形されるＡｌ基複合材料の製造方法に関する。DETAILED DESCRIPTION OF THE INVENTION (Industrial Application Field) The present invention relates to a method for producing an Al-based composite material that is solidified and molded by hot isostatic pressing (hereinafter referred to as HIP).
（従来の技術）
軽量金属であるＡＩ又はＭ合金と、セラミクスのウィス
カや短繊維、セラミクス粒子等の強化材とを複合化した
Ａｌ基複合材料は、高比強度、高比弾性率、高疲労強度
、高耐摩耗性等の優れた機械的性質を有する。このため
、軽量化高性能化が強く指向されている宇宙航空機、自
動車、ＯＡ機器などの部品や構造部材の材料として、ま
たスポーツ用品材料として注目を集めている。(Conventional technology) Al-based composite materials, which are made by combining AI or M alloy, which is a lightweight metal, with reinforcing materials such as ceramic whiskers, short fibers, and ceramic particles, have high specific strength, high specific modulus, and high fatigue. It has excellent mechanical properties such as strength and high wear resistance. For this reason, it is attracting attention as a material for parts and structural members of spacecraft, automobiles, office automation equipment, etc., where weight reduction and high performance are strongly desired, as well as as a material for sporting goods.
前記Ａ１基複合材料の成形方法として、Ｍ又はＡ１合金
（以下、単にＭ合金という。）の粉末と強化材との混合
粉末をＨＩＰ成形用カプセルに充填し、脱気し、密封し
た後、ＨＩＰにより一体成形する方法がある。この方法
によれば、複合材料にボイド等の欠陥が生じず、又所期
の特性を具備したものが容易に得られる。As a method for forming the A1-based composite material, a mixed powder of M or A1 alloy (hereinafter simply referred to as M alloy) and a reinforcing material is filled into a capsule for HIP molding, degassed, sealed, and then HIP There is a method of integral molding. According to this method, a composite material that does not have defects such as voids and has desired characteristics can be easily obtained.
この際、前記カプセルとしては、軟鋼製継目無管で形成
された胴部に軟綱型の底板と蓋板とを溶接して作製され
たものが使用されている。In this case, the capsule used is one made by welding a soft-rope bottom plate and a cover plate to a body made of a seamless pipe made of mild steel.
ＨＩＰ成形後の複合材料は、カプセルを除去した後、固
化成形されたまま、あるいは押出し加工等の塑性加工を
施して各種形状に仕上げられる。After HIP molding, the composite material is finished into various shapes after removing the capsules, either as solidified or molded, or by being subjected to plastic processing such as extrusion.
（発明が解決しようとする課題）
しかし、アルミニウム合金基複合材料の固化成形温度は
比較的低いので、軟鋼製カプセルでは成形時に十分軟化
しないため、不均一な収縮を起こす。その結果、例えば
押出素材等として利用度の高い円柱形状の製品を削り出
す場合、有効径が小さくなり歩留りが極めて低くなると
いう問題がある。(Problem to be Solved by the Invention) However, since the solidification and forming temperature of the aluminum alloy matrix composite material is relatively low, the capsule made of mild steel does not soften sufficiently during forming, causing non-uniform shrinkage. As a result, when cutting a cylindrical product, which is often used as an extrusion material, for example, there is a problem that the effective diameter becomes small and the yield becomes extremely low.
この場合、歩留りを上げようと思うと、不均一収縮を防
止すればよく、カプセル内の粉末充填率を上げればよい
。このため、プレスにより加圧充填し、充填率の向上が
図られている。しかし、充填率を上げると脱ガスが困難
になるという問題が生ずる。従って、充填率をあまり大
きくすることができず、充填率は６０〜７０％程度に止
められている。それ故、加圧充填した場合でも、カプセ
ルの不均一収縮は避けられず、歩留りは６５％程度の低
い値になっているのが現状である。第４図および第５図
は、加圧充填した軟鋼製円筒状カプセルのＨＩＰ後の形
状を模式的に示しており、加圧充填しても、同図のよう
にかなりの不均一収縮が発生する。In this case, in order to increase the yield, it is sufficient to prevent uneven shrinkage and increase the powder filling rate in the capsule. For this reason, filling is performed under pressure using a press to improve the filling rate. However, increasing the filling rate causes the problem that degassing becomes difficult. Therefore, the filling rate cannot be increased very much, and the filling rate is limited to about 60 to 70%. Therefore, even when pressure-filled, uneven shrinkage of the capsules is unavoidable, and the current yield is as low as about 65%. Figures 4 and 5 schematically show the shape of a pressurized cylindrical capsule made of mild steel after HIP, and as shown in the figure, considerable uneven shrinkage occurs even when pressurized. do.
本発明はかかる問題点に鑑みなされたもので、ＨＩＰに
よりアルミニウム基複合材料を製造するに際し、歩留り
の向上を図ることを目的とする。The present invention was made in view of such problems, and an object of the present invention is to improve the yield when manufacturing an aluminum matrix composite material by HIP.
（課題を解決するための手段）
上記目的を達成するためになされた本発明の製造方法は
、アルミニウム又はアルミニウム合金粉末と強化材との
混合粉末をカプセルに充填し脱気し密封した後、ＨＩＰ
により固化成形するＡ１基複合材料の製造方法において
、前記カプセルとしてアルミニウム又はアルミニウム合
金で形成されたカプセルを用いることを発明の構成とす
るものである。(Means for Solving the Problems) The manufacturing method of the present invention, which has been made to achieve the above object, is to fill a capsule with a mixed powder of aluminum or aluminum alloy powder and a reinforcing material, deaerate it, seal it, and then HIP it.
In the method for manufacturing an A1-based composite material which is solidified and formed by a method, the invention is characterized in that a capsule made of aluminum or an aluminum alloy is used as the capsule.
（作 用）
本発明は、粉末冶金法にてＨＩＰを用いてアルミニウム
基複合材料を製造する際に、従来用いられている軟鋼製
カプセルに代わり、アルミニウムもしくはアルミニウム
合金製カプセル（以下アルミニウムカプセルと略す）を
用いるものである。(Function) The present invention provides an aluminum or aluminum alloy capsule (hereinafter abbreviated as aluminum capsule) in place of the conventionally used mild steel capsule when manufacturing an aluminum matrix composite material using HIP using a powder metallurgy method. ) is used.
アルミニウム基複合材料を固化成形する場合、通常、熱
間で行われるが、この際、軟鋼製カプセルに比ベアルミ
ニウムカプセルは十分に軟化しており、延性も十分大き
いために均一変形する。また、カプセル内材料もマトリ
ックスがアルミニウムもしくはアルミニウム合金である
ため軟化しており、このため従来の軟鋼製カプセルを用
いた場合、高温下でのカプセル内部材料の変形抵抗とカ
プセルのそれとでは大きく開きがあるので不均一な収縮
を起こしていたが、アルミニウムカプセルを用いること
で高温下での変形抵抗がカプセル内部の材料と近い値に
なるために均一な収縮をする。When solidifying and molding an aluminum matrix composite material, it is usually hot-formed, and at this time, the aluminum capsule is sufficiently softened compared to the mild steel capsule and has sufficiently high ductility, so that it is uniformly deformed. In addition, the material inside the capsule is also softened because the matrix is aluminum or aluminum alloy, so when conventional mild steel capsules are used, there is a large difference between the deformation resistance of the inside material of the capsule at high temperatures and that of the capsule. However, by using an aluminum capsule, the deformation resistance at high temperatures is close to that of the material inside the capsule, so it shrinks uniformly.
（実施例）
第１図は本発明に使用するＨＩＰ成形用カプセルの一例
を示したもので、円筒状の胴部１の上。(Example) FIG. 1 shows an example of a capsule for HIP molding used in the present invention.
下端開口に蓋板２．底板３が溶接されている。蓋板２に
は脱気管４が設けられている。５は成形対象の混合粉末
である。かかるカプセルの基本構造は従来と同様である
が、本発明においてはその材質に特徴があり、これらは
アルミニウム又はアルミニウム合金により形成されてい
る。Lid plate 2 at the bottom opening. The bottom plate 3 is welded. A degassing pipe 4 is provided on the cover plate 2. 5 is a mixed powder to be molded. The basic structure of such a capsule is the same as the conventional one, but the present invention is characterized by its material, which is made of aluminum or aluminum alloy.
カプセルに用いるアルミニウム合金には、複合材料のマ
トリックスであるアルミニウム合金よりも高い固相線温
度を有したものの方が、高温下での強度面より望ましい
。ＨＩＰ温度よりも固相線温度の方が高いアルミニウム
合金を用いることは言うまでもない。また、カプセルの
胴部は、押し出し、引抜き、あるいは深絞りによる継目
無管を用いるのが望ましいが、溶接により製管したもの
でも使用できる。It is preferable that the aluminum alloy used for the capsule has a higher solidus temperature than the aluminum alloy that is the matrix of the composite material in terms of strength at high temperatures. Needless to say, an aluminum alloy whose solidus temperature is higher than the HIP temperature is used. Further, for the body of the capsule, it is preferable to use a seamless pipe made by extrusion, drawing, or deep drawing, but a pipe made by welding can also be used.
前記混合粉末５は、Ｍ合金粉末と強化材とを均一に混合
したものであるが、Ａ１合金としては、６０６１材、７
０７５材等種々のものを利用することができ、−力強化
材としては、ＳｉＣ，Ｓｉ３Ｎ４． ＋ＡＬｚＯ＋＋Ａ
ｌｚ０３＋５１０ｚ等のセラミクスのウィスカや粒子、
その他各種金属短繊維やウィスカを利用することができ
る。The mixed powder 5 is a uniform mixture of M alloy powder and reinforcing material, but as A1 alloy, 6061 material, 7
Various materials such as 075 materials can be used, and as force reinforcing materials, SiC, Si3N4. +ALzO++A
Whiskers and particles of ceramics such as lz03+510z,
Other various short metal fibers and whiskers can be used.
尚、Ｍ合金粉末とセラミクスウィスカの強化材とを均一
に混合する好適な方法として、特開昭６０−２５１９２
２号において開示されている通り、有機溶媒中で強化材
に超音波振動を与えて絡まりを解きほぐし、この中にＭ
合金粉末を加えて撹拌し、得られた混合スラリーを吸引
濾過し、ケーキを真空乾燥する方法がある。A suitable method for uniformly mixing M alloy powder and ceramic whisker reinforcing material is disclosed in Japanese Patent Application Laid-Open No. 60-25192.
As disclosed in No. 2, the reinforcing material was subjected to ultrasonic vibration in an organic solvent to disentangle it, and M
There is a method in which alloy powder is added and stirred, the resulting mixed slurry is suction-filtered, and the cake is vacuum-dried.
前記混合粉末５をカプセルに充填するには、底板３が溶
接された胴部１に混合粉末５を装入した後、脱気管４付
の蓋板２をその上端開口部に溶接することによって行う
。尚、混合粉末の充填に当っては、プレス等による加圧
は不要であり、棒材により粉末を締める様にするだけで
十分である。The mixed powder 5 is filled into a capsule by charging the mixed powder 5 into the body 1 to which the bottom plate 3 is welded, and then welding the lid plate 2 with the degassing pipe 4 to its upper opening. . Note that when filling the mixed powder, it is not necessary to apply pressure using a press or the like, and it is sufficient to tighten the powder with a rod.
前記混合粉末をカプセルに充填後、蓋板２の脱気管４よ
りカプセル内部の空気を脱気する。この際、カブセール
を加熱しながら脱気するとよい。脱気後、脱気管４を圧
着して密封した後、ＨＩＰ処理を行う。After filling the capsule with the mixed powder, the air inside the capsule is evacuated through the deaeration pipe 4 of the lid plate 2. At this time, it is recommended to degas the cabsail while heating it. After degassing, the degassing tube 4 is crimped and sealed, and then HIP treatment is performed.
第２図および第３図はＨＩＰ処理後のカプセルの外形図
（脱気管図示省略）および第２図Ａ−Ａ線断面図を模式
的に示したものであり、カプセルの収縮は軸方向、径方
向ともほぼ均等に収縮しており、特に径方向の不均一収
縮は生していない。Figures 2 and 3 schematically show the external dimensions of the capsule after HIP treatment (deaeration tube not shown) and the cross-sectional view taken along the line A-A in Figure 2. The shrinkage was almost uniform in both directions, and there was no uneven shrinkage in the radial direction.
カプセル中の混合粉末は４００〜６６０°Ｃの固相域あ
るいは固液共存域の温度でＨＩＰ処理を行うことにより
加圧焼結され、所期の複合材料となっている。適宜の切
削機械によりカプセルを除去し、複合材料を円柱状に精
整加工することにより製品が得られる。The mixed powder in the capsule is pressure sintered by HIP treatment at a temperature in the solid phase region or solid-liquid coexistence region of 400 to 660° C. to form the desired composite material. A product is obtained by removing the capsule using an appropriate cutting machine and finely processing the composite material into a cylindrical shape.
次に具体的実施例を掲げる。Next, specific examples are listed.
（１）第１表に示すように、種々の寸法の円筒状カプセ
ルを準備した。Ｎｏ、 １〜３は実施例であり、カプセ
ル材質は工業用純アルミニウムである。(1) As shown in Table 1, cylindrical capsules of various sizes were prepared. Nos. 1 to 3 are examples, and the capsule material is industrial pure aluminum.
Ｎｏ、 ４〜６は従来例であり、カプセル材質は軟調で
ある。Nos. 4 to 6 are conventional examples, and the capsule material is soft.
（２） Ａ７合金粉末とＳｉＣウィスカを均一に混合
して混合粉末を調製した。Ｍ合金粉末は２０２４．６０
６１７０７５４７合金のアトマイズ粉末であり、粒径４
４μｍ以下に分級したものを用いた。ＳｉＣウィスカの
体積分率は２０％とした。(2) A mixed powder was prepared by uniformly mixing A7 alloy powder and SiC whiskers. M alloy powder is 2024.60
Atomized powder of 61707547 alloy, particle size 4
The particles classified to 4 μm or less were used. The volume fraction of SiC whiskers was 20%.
（３）カプセルに混合粉末を充填し、加熱下において脱
気密封した。混合粉末の充填に当っては、蓋板の溶接し
ていないものを使用した。Ｎｏ、 １〜３（実施例）の
場合、混合粉末を加圧することなく、棒材によりしめる
程度に止めた。一方、Ｎｏ、 ４〜６（従来例）の場合
、プレスにより加圧して充填率を高めた。(3) The mixed powder was filled into capsules, and the capsules were degassed and sealed under heating. When filling the mixed powder, a lid plate without welding was used. In the case of Nos. 1 to 3 (Examples), the mixed powder was not pressurized, but was only compressed by the rod. On the other hand, in the case of Nos. 4 to 6 (conventional examples), the filling rate was increased by applying pressure with a press.
第１表
注１．Ｎｏ、１〜３・・・実施例、Ｎｏ、 ４〜６・・
・従来個性２．混合粉末の種類
Ａ・・・２０２４Ｍ合金粉末、ＳｉＣウィスカＢ・・・
６０６１Ａ１合金粉末、ＳｉＣウィスカＣ・・・７０７
５Ｍ合金粉末、ＳｉＣウィスカ（４）実施例、従来例と
も同条件でＨＩＰ処理した。Table 1 Note 1. No. 1 to 3...Example, No. 4 to 6...
・Conventional individuality 2. Mixed powder type A...2024M alloy powder, SiC whisker B...
6061A1 alloy powder, SiC whisker C...707
5M alloy powder, SiC whisker (4) Example and conventional example were both subjected to HIP treatment under the same conditions.
処理条件は、４８０°Ｃ１１Ｃ１１５Ｏ０／ｃｌ” ア
ル。（−（７）結果、カプセルは実施例が第２図および
第３図、従来例が第４図および第５図のようであった。The treatment conditions were 480 DEG C. 11C115O0/cl'' Al.
因みに、試料Ｎｏ、 １とＮｏ、 ４のカプセル外観写
真を参考写真１（試料Ｎｏ、 １ ）および２（試料Ｎ
ｏ、 ４ ）に示す。Incidentally, the capsule exterior photos of samples No. 1 and No. 4 are used as reference photos 1 (sample No. 1) and 2 (sample N.
o, 4).
（５）ＨＩＰ処理後のカプセルから、可能な限り大きい
直径を有する円柱形ビレットを削り出した。(5) A cylindrical billet having the largest possible diameter was milled from the HIP-treated capsule.
その結果を第１表に併せて示す。同表より、実施例のＮ
ｏ、 １〜３は、従来例のＮｏ、 ４〜６に比べて粉末
充填率が１０％程度低いにも拘らず、歩留りが３０％程
度飛躍的に向上した。The results are also shown in Table 1. From the same table, N of the example
Nos. 1 to 3 had a powder filling rate about 10% lower than conventional examples Nos. 4 to 6, but the yields were dramatically improved by about 30%.
（発明の効果）
本発明によれば、カプセルの材質をアルミニウム又はそ
の合金で形成したので、アルミニウム合金基複合材料の
ような比較的低いＨＩＰ成形温度においてもカプセルは
十分に軟化し、混合粉末と同程度の強度となるので、径
方向及び軸方向の収縮を均一にすることができ、従って
円柱形状の製品を削り出した場合の歩留りは、約９５％
にまで高めることができ、製品であるアルミニウム基複
合材料のコストが低減できる。また、カプセルが均一に
収縮することから、要求される固化成形体の大きさ及び
形状に合わせたカプセル形状設計が可能となり、製造さ
れる固化成形体の自由度が高くなる。(Effects of the Invention) According to the present invention, since the material of the capsule is made of aluminum or its alloy, the capsule can be sufficiently softened even at a relatively low HIP molding temperature such as with an aluminum alloy matrix composite material, and can be used as a mixed powder. Since the strength is about the same, shrinkage in the radial and axial directions can be made uniform, and the yield when machining cylindrical products is approximately 95%.
The cost of the product, the aluminum matrix composite material, can be reduced. Furthermore, since the capsule contracts uniformly, it becomes possible to design the capsule shape in accordance with the required size and shape of the solidified molded product, increasing the degree of freedom of the manufactured solidified molded product.
更に、従来、不均一収縮を防止するため、混合粉末の充
填率を６５％以上にする必要があったが、本発明を用い
ることによって充填率を５０％〜６０％に下げてＨＩＰ
することが可能になったことから、カプセル内の脱ガス
が容易になった。Furthermore, conventionally, in order to prevent uneven shrinkage, it was necessary to increase the filling rate of the mixed powder to 65% or more, but by using the present invention, the filling rate can be lowered to 50% to 60% and HIP can be performed.
This made it easier to degas the capsule.
第１図はＨＩＰ成形用カプセルの構造を示す断面図、第
２図は本発明のカプセルのＨＩＰ処理後の外形正面図、
第３図は第２図のＡ−Ａ線断面図、第４図は従来のカプ
セルのＨＩＰ処理後の外形正面図、第５図は第４図のＡ
−Ａ線断面図である。
第４図FIG. 1 is a sectional view showing the structure of a capsule for HIP molding, FIG. 2 is a front view of the outer appearance of the capsule of the present invention after HIP processing,
Figure 3 is a sectional view taken along the line A-A in Figure 2, Figure 4 is a front view of the conventional capsule after HIP treatment, and Figure 5 is A in Figure 4.
-A cross-sectional view. Figure 4
Claims (1)
との混合粉末をカプセルに充填し脱気し密封した後、熱
間等方圧加圧により固化成形するＡｌ基複合材料の製造
方法において、 前記カプセルとしてアルミニウム又はアルミニウム合金
で形成されたカプセルを用いることを特徴とするＡｌ基
複合材料の製造方法。(1) In a method for producing an Al-based composite material, in which a mixed powder of aluminum or aluminum alloy powder and a reinforcing material is filled into a capsule, deaerated and sealed, and then solidified and molded by hot isostatic pressing, the capsule is A method for producing an Al-based composite material, the method comprising using a capsule made of aluminum or an aluminum alloy.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10431390A JPH042703A (en) | 1990-04-18 | 1990-04-18 | Manufacture of al-base composite material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10431390A JPH042703A (en) | 1990-04-18 | 1990-04-18 | Manufacture of al-base composite material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH042703A true JPH042703A (en) | 1992-01-07 |
Family
ID=14377444
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10431390A Pending JPH042703A (en) | 1990-04-18 | 1990-04-18 | Manufacture of al-base composite material |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH042703A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103194632A (en) * | 2013-05-02 | 2013-07-10 | 西安卓曦新材料科技有限公司 | Preparation method of high-volume fraction micrometer alumina ceramic enhanced composite material |
| CN103194631A (en) * | 2013-05-02 | 2013-07-10 | 西安卓曦新材料科技有限公司 | Preparation method of high-volume fraction alumina ceramic particle enhanced composite material |
| CN103882350A (en) * | 2014-04-10 | 2014-06-25 | 哈尔滨工业大学 | Method for severe plastic deformation of metal-based composite material reinforced by using granules with high volume fraction |
| CN104611597A (en) * | 2013-11-01 | 2015-05-13 | 北京有色金属研究总院 | Particle reinforced aluminum-based billet moulding and degassing method |
| CN105154705A (en) * | 2015-09-08 | 2015-12-16 | 中国科学院上海硅酸盐研究所 | SPS (spark plasma sintering) silicon-carbide-particle-reinforced aluminum-based composite and preparing method thereof |
| CN105728718A (en) * | 2016-03-08 | 2016-07-06 | 苏州珍展科技材料有限公司 | Preparing method for weldable layered Fe/Al base composite board |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60121241A (en) * | 1983-11-30 | 1985-06-28 | Showa Alum Corp | Manufacture of fiber reinforced aluminum material |
| JPS62199703A (en) * | 1986-02-26 | 1987-09-03 | Sumitomo Light Metal Ind Ltd | Hot hydrostatic compression molding method for al-si powder alloy |
| JPS644418A (en) * | 1987-06-26 | 1989-01-09 | Tokai Carbon Kk | Production of whisker reinforced metal composite material |
-
1990
- 1990-04-18 JP JP10431390A patent/JPH042703A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60121241A (en) * | 1983-11-30 | 1985-06-28 | Showa Alum Corp | Manufacture of fiber reinforced aluminum material |
| JPS62199703A (en) * | 1986-02-26 | 1987-09-03 | Sumitomo Light Metal Ind Ltd | Hot hydrostatic compression molding method for al-si powder alloy |
| JPS644418A (en) * | 1987-06-26 | 1989-01-09 | Tokai Carbon Kk | Production of whisker reinforced metal composite material |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103194632A (en) * | 2013-05-02 | 2013-07-10 | 西安卓曦新材料科技有限公司 | Preparation method of high-volume fraction micrometer alumina ceramic enhanced composite material |
| CN103194631A (en) * | 2013-05-02 | 2013-07-10 | 西安卓曦新材料科技有限公司 | Preparation method of high-volume fraction alumina ceramic particle enhanced composite material |
| CN104611597A (en) * | 2013-11-01 | 2015-05-13 | 北京有色金属研究总院 | Particle reinforced aluminum-based billet moulding and degassing method |
| CN103882350A (en) * | 2014-04-10 | 2014-06-25 | 哈尔滨工业大学 | Method for severe plastic deformation of metal-based composite material reinforced by using granules with high volume fraction |
| CN105154705A (en) * | 2015-09-08 | 2015-12-16 | 中国科学院上海硅酸盐研究所 | SPS (spark plasma sintering) silicon-carbide-particle-reinforced aluminum-based composite and preparing method thereof |
| CN105728718A (en) * | 2016-03-08 | 2016-07-06 | 苏州珍展科技材料有限公司 | Preparing method for weldable layered Fe/Al base composite board |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4673549A (en) | Method for preparing fully dense, near-net-shaped objects by powder metallurgy | |
| US4032335A (en) | Process for making metallic, molded composite bodies | |
| US4526747A (en) | Process for fabricating parts such as gas turbine compressors | |
| US5130084A (en) | Powder forging of hollow articles | |
| JPS61246303A (en) | Production of composiite powder metallurgical billet | |
| EP0466401B1 (en) | Gear | |
| US3824097A (en) | Process for compacting metal powder | |
| JPH01268802A (en) | Method for molding metal product | |
| JPH0130898B2 (en) | ||
| JPS5842703A (en) | Manufacture of preform of one body powder alloy part from more than two kinds of powder alloy | |
| JPH042703A (en) | Manufacture of al-base composite material | |
| US4410488A (en) | Powder metallurgical process for producing a copper-based shape-memory alloy | |
| JPS6021306A (en) | Manufacturing method of composite reinforced member | |
| JP3199809B2 (en) | Manufacturing method of composite extruded member | |
| JPS62109903A (en) | Method for pressing and packing powder | |
| EP3646970B1 (en) | Method for fabricating components using hybrid additive manufacturing and consolidation process | |
| JPS63255331A (en) | Formation of ti-al intermetallic-compound member | |
| JPH0625363B2 (en) | Extruded A-1 group composite vitret and method for producing the same | |
| JP2752858B2 (en) | Manufacturing method of powder alloy billet | |
| JPH02217404A (en) | Method for forming al-base composite material | |
| JPS63247321A (en) | Formation of ti-al intermetallic compound member | |
| JPH04131307A (en) | Manufacture of metallic pipe and its metallic pipe | |
| JPS63282201A (en) | Method for forging powder metallurgical material | |
| JPS63247322A (en) | Formation of ti-al intermetallic compound member | |
| JPH05287315A (en) | Powder molding method by hydrostatic molding using a mold |