JPH0470587B2 - - Google Patents

Info

Publication number: JPH0470587B2
Authority: JP; Japan
Prior art keywords: coal; boiling point; temperature; oil; separation
Prior art date: 1987-08-24
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Lifetime

Application number

JP62209903A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6453153A (en

Inventor

Kazuo Makino

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Individual

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1987-08-24

Filing date

1987-08-24

Publication date

1992-11-11

1987-08-24 Application filed by Individual filed Critical Individual

1987-08-24 Priority to JP62209903A priority Critical patent/JPS6453153A/ja

1989-03-01 Publication of JPS6453153A publication Critical patent/JPS6453153A/ja

1992-11-11 Publication of JPH0470587B2 publication Critical patent/JPH0470587B2/ja

Status Granted legal-status Critical Current

Links

239000003245 coal Substances 0.000 claims description 37
238000003763 carbonization Methods 0.000 claims description 32
238000009835 boiling Methods 0.000 claims description 30
238000012856 packing Methods 0.000 claims description 13
239000000463 material Substances 0.000 claims description 12
238000004519 manufacturing process Methods 0.000 claims description 7
239000007788 liquid Substances 0.000 claims description 6
239000011261 inert gas Substances 0.000 claims description 5
239000007789 gas Substances 0.000 claims description 4
238000004517 catalytic hydrocracking Methods 0.000 claims description 3
238000000926 separation method Methods 0.000 description 22
239000003921 oil Substances 0.000 description 16
239000000126 substance Substances 0.000 description 13
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
239000000295 fuel oil Substances 0.000 description 10
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 8
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 8
238000002474 experimental method Methods 0.000 description 8
239000008103 glucose Substances 0.000 description 8
239000000203 mixture Substances 0.000 description 8
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 6
229930006000 Sucrose Natural products 0.000 description 6
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 6
WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 6
150000001720 carbohydrates Chemical class 0.000 description 6
239000005720 sucrose Substances 0.000 description 6
235000014633 carbohydrates Nutrition 0.000 description 5
238000006243 chemical reaction Methods 0.000 description 5
239000000945 filler Substances 0.000 description 5
230000014759 maintenance of location Effects 0.000 description 5
239000002994 raw material Substances 0.000 description 5
239000003610 charcoal Substances 0.000 description 4
238000005516 engineering process Methods 0.000 description 4
238000004811 liquid chromatography Methods 0.000 description 4
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical group N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
229930091371 Fructose Natural products 0.000 description 3
239000005715 Fructose Substances 0.000 description 3
RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 3
239000004305 biphenyl Substances 0.000 description 3
235000010290 biphenyl Nutrition 0.000 description 3
125000006267 biphenyl group Chemical group 0.000 description 3
239000003575 carbonaceous material Substances 0.000 description 3
238000004587 chromatography analysis Methods 0.000 description 3
238000011161 development Methods 0.000 description 3
238000004128 high performance liquid chromatography Methods 0.000 description 3
ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 3
239000007787 solid Substances 0.000 description 3
OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 2
GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 description 2
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 2
GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 2
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
125000003118 aryl group Chemical group 0.000 description 2
GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 2
229910052799 carbon Inorganic materials 0.000 description 2
238000010586 diagram Methods 0.000 description 2
229930195733 hydrocarbon Natural products 0.000 description 2
150000002430 hydrocarbons Chemical class 0.000 description 2
239000001257 hydrogen Substances 0.000 description 2
229910052739 hydrogen Inorganic materials 0.000 description 2
239000008101 lactose Substances 0.000 description 2
238000005259 measurement Methods 0.000 description 2
150000001247 metal acetylides Chemical class 0.000 description 2
238000000034 method Methods 0.000 description 2
150000002828 nitro derivatives Chemical class 0.000 description 2
239000010742 number 1 fuel oil Substances 0.000 description 2
239000011295 pitch Substances 0.000 description 2
238000012545 processing Methods 0.000 description 2
238000011160 research Methods 0.000 description 2
239000011343 solid material Substances 0.000 description 2
XRVUVXISPFFMCT-UHFFFAOYSA-N C1=CC=CC2=CC=CC=C12.C1(=CC=CC=C1)C1=CC=CC=C1.C1=CC=CC=C1 Chemical group C1=CC=CC2=CC=CC=C12.C1(=CC=CC=C1)C1=CC=CC=C1.C1=CC=CC=C1 XRVUVXISPFFMCT-UHFFFAOYSA-N 0.000 description 1
239000004215 Carbon black (E152) Substances 0.000 description 1
239000013543 active substance Substances 0.000 description 1
238000005054 agglomeration Methods 0.000 description 1
230000002776 aggregation Effects 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
150000001413 amino acids Chemical class 0.000 description 1
RCJBQOXVMVYQAU-UHFFFAOYSA-N aniline benzene-1,4-diamine Chemical compound NC1=CC=CC=C1.NC1=CC=C(N)C=C1 RCJBQOXVMVYQAU-UHFFFAOYSA-N 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
238000011021 bench scale process Methods 0.000 description 1
230000008859 change Effects 0.000 description 1
238000003889 chemical engineering Methods 0.000 description 1
239000000571 coke Substances 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
230000005494 condensation Effects 0.000 description 1
238000009833 condensation Methods 0.000 description 1
238000001514 detection method Methods 0.000 description 1
229910001873 dinitrogen Inorganic materials 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000000921 elemental analysis Methods 0.000 description 1
239000012847 fine chemical Substances 0.000 description 1
239000012530 fluid Substances 0.000 description 1
239000000446 fuel Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
229910001385 heavy metal Inorganic materials 0.000 description 1
238000005984 hydrogenation reaction Methods 0.000 description 1
239000012770 industrial material Substances 0.000 description 1
239000011344 liquid material Substances 0.000 description 1
239000011331 needle coke Substances 0.000 description 1
150000005181 nitrobenzenes Chemical class 0.000 description 1
229910052757 nitrogen Chemical group 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
230000008520 organization Effects 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000012188 paraffin wax Substances 0.000 description 1
239000003208 petroleum Substances 0.000 description 1
239000000843 powder Substances 0.000 description 1
230000008569 process Effects 0.000 description 1
238000005086 pumping Methods 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
238000000197 pyrolysis Methods 0.000 description 1
230000009467 reduction Effects 0.000 description 1
238000007670 refining Methods 0.000 description 1
230000004044 response Effects 0.000 description 1
238000001612 separation test Methods 0.000 description 1
235000000346 sugar Nutrition 0.000 description 1
150000008163 sugars Chemical class 0.000 description 1
238000004381 surface treatment Methods 0.000 description 1
238000012360 testing method Methods 0.000 description 1

Landscapes

Solid-Sorbent Or Filter-Aiding Compositions (AREA)

JP62209903A 1987-08-24 1987-08-24 Production of liquid chromatograph packing material from coal liquefied oil Granted JPS6453153A (en)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP62209903A JPS6453153A (en)	1987-08-24	1987-08-24	Production of liquid chromatograph packing material from coal liquefied oil

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP62209903A JPS6453153A (en)	1987-08-24	1987-08-24	Production of liquid chromatograph packing material from coal liquefied oil

Publications (2)

Publication Number	Publication Date
JPS6453153A JPS6453153A (en)	1989-03-01
JPH0470587B2 true JPH0470587B2 (de)	1992-11-11

Family

ID=16580557

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP62209903A Granted JPS6453153A (en)	1987-08-24	1987-08-24	Production of liquid chromatograph packing material from coal liquefied oil

Country Status (1)

Country	Link
JP (1)	JPS6453153A (de)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6787029B2 (en)	2001-08-31	2004-09-07	Cabot Corporation	Material for chromatography

1987
- 1987-08-24 JP JP62209903A patent/JPS6453153A/ja active Granted

Also Published As

Publication number	Publication date
JPS6453153A (en)	1989-03-01

Publication	Publication Date	Title
Bartle et al.	1987	The functionality of nitrogen in coal and derived liquids: An XPS study
Zander	1987	Recent advances in pitch characterization
Wiser et al.	1970	Catalytic hydrogenation of multiring aromatic coal tar constituents
US4081351A (en)	1978-03-28	Conversion of coal into motor fuel
Li et al.	2017	Co-pyrolysis performance of coal and its direct coal liquefaction residue with solid heat carrier
US5698174A (en)	1997-12-16	Process for separating fullerenes
Granda et al.	1990	Application of extrography for characterization of coal tar and petroleum pitches
Llano et al.	1994	Catalytic hydrogenation of anthracene oil with red mud
US4052291A (en)	1977-10-04	Production of asphalt cement
US4127475A (en)	1978-11-28	Process for the isolation of chemicals from processed coals
JPH0344117B2 (de)	1991-07-04
Sharkey Jr et al.	1966	Mass spectra of pyrolyzates of several aromatic structures identified in coal extracts
Petrakis et al.	1983	Catalytic hydroprocessing of SRC-II heavy distillate fractions. 1. Preparation of the fractions by liquid chromatography
GB1600428A (en)	1981-10-14	Process for the liquefaction of solid carbonaceous materials
US3755136A (en)	1973-08-28	System for removing solids from coal liquefaction reactor effluents
Moinelo et al.	1988	Fractionation of coal-derived liquids by extrography
CN117723683A (zh)	2024-03-19	一种分离石油类样品中烯烃化合物的方法
Goldstein	1976	Separation of polycyclic aromatic hydrocarbons by liquid chromatography on cross-linked polyvinylpyrrolidone
Palmer et al.	1972	The smaller molecules obtainable from coal and their significance: Part 3. Steaming/carbonization of a weakly-caking coal at temperatures up to 600° C
Wozniak et al.	1985	Analysis of hydroaromatics in coal-derived synthetic fuels: applications to pilot-plant samples
Teo et al.	1987	Characterization of pyrolysis tars from Canadian coals
Zhong et al.	2026	Biochar as a structure-tunable stationary phase for column chromatographic fractionation of bio-oil
CN112986455A (zh)	2021-06-18	一种煤液化油组分的分离方法
CN120761565A (zh)	2025-10-10	一种针状焦原料中详细烃含量的高效高精度分析方法
Lanças et al.	1994	Chromatographic Isolation of Nitrogen-Containing Compounds in Liquid Fuels 1 Ti (IV) Oxide Grafted onto Silica as Stationary Phase