JPH0499843A - Case hardening steel - Google Patents

Case hardening steel

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Publication number
JPH0499843A
JPH0499843A JP21712590A JP21712590A JPH0499843A JP H0499843 A JPH0499843 A JP H0499843A JP 21712590 A JP21712590 A JP 21712590A JP 21712590 A JP21712590 A JP 21712590A JP H0499843 A JPH0499843 A JP H0499843A
Authority
JP
Japan
Prior art keywords
machinability
less
carburizing
hardness
hardenability
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP21712590A
Other languages
Japanese (ja)
Other versions
JP2546045B2 (en
Inventor
Tetsuo Shiragami
哲夫 白神
Tetsuya Sanpei
哲也 三瓶
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JFE Engineering Corp
Original Assignee
NKK Corp
Nippon Kokan Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NKK Corp, Nippon Kokan Ltd filed Critical NKK Corp
Priority to JP2217125A priority Critical patent/JP2546045B2/en
Publication of JPH0499843A publication Critical patent/JPH0499843A/en
Application granted granted Critical
Publication of JP2546045B2 publication Critical patent/JP2546045B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Heat Treatment Of Steel (AREA)
  • Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)

Abstract

(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。
(57) [Summary] This bulletin contains application data before electronic filing, so abstract data is not recorded.

Description

【発明の詳細な説明】 「発明の目的」 (産業上の利用分野) 本発明は肌焼鋼に係り、省エネルギー、省工程的で浸炭
時の歪も小さい肌焼鋼を提供しようとするものである。
[Detailed Description of the Invention] "Objective of the Invention" (Industrial Application Field) The present invention relates to case hardening steel, and aims to provide a case hardening steel that is energy saving, process saving, and has less distortion during carburizing. be.

(従来の技術) 肌焼鋼を用いた部品の加工工程として、熱間鍛造−焼な
らし一切削仕上一浸炭処理がある。即ち熱間鍛造による
成形時には加熱温度が1200°C程度になり、結晶粒
度が大きく、鍛造後の硬度が高いため被削性が悪い。そ
こで一般的には熱間鍛造後に焼ならしを行って組織を微
細化し、硬さを低減させて切削を行うものである しかしこのような熱処理(焼ならし)を行うことば製造
工程が煩雑で熱エネルギーを増大し、コスト高を招くこ
とから特公昭61−54844でばTi、 Zr、11
fの1種以上を含有させて結晶粒の微細化を図っている
(Prior Art) Processing processes for parts using case hardened steel include hot forging, normalizing, cutting and carburizing. That is, when forming by hot forging, the heating temperature is about 1200°C, the crystal grain size is large, and the hardness after forging is high, resulting in poor machinability. Therefore, generally, after hot forging, normalization is performed to refine the structure and reduce hardness before cutting. Because it increases thermal energy and increases costs, the use of Ti, Zr, and 11 in Japanese Patent Publication No. 61-54844
The crystal grains are made finer by containing one or more types of f.

また肌焼鋼は最終形状に加工された後、920°C程度
で数時間加熱し浸炭されるため結晶粒度が大きくなり易
い。これについては多くの研究がなされており、Aj!
、Nb、Ti等の析出物を用いて結晶粒粗大化防止を図
っており、特公昭61−54844ではTiなどによっ
て対処している。
Furthermore, after case hardened steel is processed into its final shape, it is heated at about 920° C. for several hours and carburized, so the grain size tends to increase. A lot of research has been done on this, and Aj!
Precipitates such as , Nb, and Ti are used to prevent coarsening of crystal grains, and in Japanese Patent Publication No. 61-54844, Ti is used as a countermeasure.

(発明が解決しようとする課題) 上記したような析出物を用いた結晶粒粗大化防止技術に
よるものは熱間鍛造時と浸炭時の加熱温度差が大きいた
め同じ析出物で結晶粒粗大化防止を図ることは困難であ
る。
(Problem to be Solved by the Invention) The technique using precipitates as described above to prevent crystal grain coarsening has a large difference in heating temperature between hot forging and carburizing, so it is difficult to prevent crystal grain coarsening using the same precipitates. It is difficult to achieve this goal.

又特公昭61−54844によるものでは焼ならし本来
の目的である硬さの低減ないし被削性の向上が必ずしも
有効に得られていない。
Furthermore, the method disclosed in Japanese Patent Publication No. 61-54844 does not necessarily effectively achieve the original purpose of normalizing, which is to reduce hardness or improve machinability.

従って製造工程の煩雑且つ高コスト化を避け、しかも被
削性が良好で、浸炭処理時に結晶粒粗大化を生じないよ
うな肌焼鋼は未だ得られるに到っていない。
Therefore, it has not yet been possible to obtain a case-hardening steel that avoids complicated and high-cost manufacturing processes, has good machinability, and does not cause grain coarsening during carburization.

「発明の構成」 (課題を解決するための手段) 本発明は上記したような従来技術における課題を解消す
るように鋭意研究した結果、Tiの微量添加、Sの添加
、焼入性指数制御により焼ならしを行うことなしに被削
性を向上させ、且つAAとNのバランス制御を行うこと
により浸炭時の結晶粒粗大化防止を図ることに成功した
ものであって、以下の如くである。
"Structure of the Invention" (Means for Solving the Problems) As a result of intensive research to solve the problems in the prior art as described above, the present invention has been developed by adding a small amount of Ti, adding S, and controlling the hardenability index. This method succeeded in improving machinability without normalizing and preventing grain coarsening during carburizing by controlling the balance between AA and N, and is as follows. .

C: 0.15〜0.35wt%、Si:0.5wt%
以下、Mn:1.5wt%以下、   Cr:1.5w
t%以下、Mo : 0.25wt%以下、 s:o、03〜o、oswt%、 Ti:0.005〜0.015wt%、All/N” 
 : 1.5〜2.8 T層 D+:85〜901m 〔イ旦しD+=7.95、ハゴ−(1十〇、64Si)
(1+4.IMn)(1+2.33Cr) (1+3.
14Mo)  )を含有し、残部がFeおよび不可避的
不純物から成ることを特徴とした肌焼鋼。
C: 0.15-0.35wt%, Si: 0.5wt%
Below, Mn: 1.5wt% or less, Cr: 1.5w
t% or less, Mo: 0.25wt% or less, s: o, 03~o, oswt%, Ti: 0.005~0.015wt%, All/N"
: 1.5~2.8 T layer D+: 85~901m [Itanshi D+=7.95, Hago (100, 64Si)
(1+4.IMn) (1+2.33Cr) (1+3.
14Mo) ), with the remainder consisting of Fe and inevitable impurities.

(作用) 上記したような本発明における成分組成範囲をwt%(
以下単に「%」という)によって説明すると、以下の如
くである。
(Function) The component composition range in the present invention as described above is changed by wt% (
(hereinafter simply referred to as "%") is as follows.

C: 0.15〜0.35%。C: 0.15-0.35%.

Cは、強度確保のため0.15%以上を必要とするが、
0.35%を超えると心部の靭性が低下するので、0.
15〜0.35%とする。
C requires 0.15% or more to ensure strength, but
If it exceeds 0.35%, the toughness of the core will decrease;
15 to 0.35%.

Si : 0.5%以下。Si: 0.5% or less.

脱酸に必要な元素であるが、0.5%を超えると靭性が
劣化するので0.5%以下とする。
It is an element necessary for deoxidation, but if it exceeds 0.5%, toughness will deteriorate, so it should be kept at 0.5% or less.

Mn:1.5%以下。Mn: 1.5% or less.

焼入性確保のため必要であるが、1.5%を超えると焼
入性が大きくなり過ぎるので1.5%以下とした。
Although it is necessary to ensure hardenability, if it exceeds 1.5%, the hardenability becomes too large, so it is set to 1.5% or less.

Cr:1.5%以下。Cr: 1.5% or less.

Crも、焼入性確保のため必要であるが、1.5%を超
えることにより焼入性が大きくなり過ぎるので1.5%
を上限とする。
Cr is also necessary to ensure hardenability, but if it exceeds 1.5%, the hardenability becomes too large, so Cr is added at 1.5%.
is the upper limit.

Mo:0.25%以下。Mo: 0.25% or less.

M6も、Mn、 Crと同じに焼入性を得るために必要
であるけれども、このMOは0.25%を超えることに
よって焼入性が大きくなり過ぎるから0.25%以下と
することが必要である。
Like Mn and Cr, M6 is also necessary to obtain hardenability, but if this MO exceeds 0.25%, the hardenability becomes too large, so it is necessary to keep it below 0.25%. It is.

S:0.03〜0.05%。S: 0.03-0.05%.

Sは、被削性を向上させる元素であり、0.03%以上
を必要とする。然し0.05%を超えると疲労特性、靭
性などに悪影響を及ぼすのでこれを上限とし、0.03
〜0.05%の範囲内とする。
S is an element that improves machinability and requires 0.03% or more. However, if it exceeds 0.05%, it will have a negative effect on fatigue properties, toughness, etc., so this is the upper limit, and 0.03
-0.05%.

Ti:0.005〜0.015%。Ti: 0.005-0.015%.

Tiは、Nと結合してTiNとなり、熱間鍛造のような
高温に加熱したときにオーステナイト結晶粒の粗大化を
防止する作用があるので0.005%以上を必要とする
が、一方TiN粒子は硬質なためその量が増すと被削性
などに悪影響を及ぼすので0.015%以下とする。
Ti combines with N to form TiN, which has the effect of preventing coarsening of austenite crystal grains when heated to high temperatures such as in hot forging, and therefore requires a content of 0.005% or more, but on the other hand, TiN particles Since C is hard, an increase in its amount will have a negative effect on machinability, so it should be kept at 0.015% or less.

Nは、Tiと結合してTiNとなる以外に多量に添加し
AAとも結合し、浸炭時におけるオーステナイト結晶粒
の粗大化を防止する作用があるので(Ti/3.42 
+0.01)%以上を必要とするが、一方0.02%を
超えると靭性が劣化するので0.02%以下とする。
In addition to combining with Ti to form TiN, N is added in large amounts and also combines with AA, which has the effect of preventing coarsening of austenite crystal grains during carburizing (Ti/3.42
+0.01% or more is required, but on the other hand, if it exceeds 0.02%, the toughness deteriorates, so the content should be 0.02% or less.

八β/N“ :1.5〜2.8 Nと結合してAANとなり、浸炭時のオーステナイト結
晶粒粗大化防止を図るが、Tiと結合した残りのN (
N”  :有効窒素)との比率が1.5〜2.8のとき
に効果があり、この範囲外では結晶粒が粗大化するので
上記範囲内とする。
8β/N": 1.5 to 2.8 It combines with N to form AAN and prevents coarsening of austenite crystal grains during carburizing, but the remaining N combined with Ti (
It is effective when the ratio to N'' (available nitrogen) is 1.5 to 2.8. Outside this range, the crystal grains become coarse, so it is set within the above range.

D、15〜9Qmm 焼入指数D1を規定するのは8511以下では焼入性が
低過ぎて不完全焼入を生じ易く、一方90鶴以上では熱
間鍛造後の硬さが高(なり過ぎて被削性に悪影響を及ぼ
す。従って85n以上9011以下とする。
D, 15~9Qmm The hardening index D1 is defined as below 8511, the hardenability is too low and incomplete quenching tends to occur, while above 90 Tsuru, the hardness after hot forging is high (too much). It has an adverse effect on machinability.Therefore, it should be 85n or more and 9011 or less.

(実施例) 本発明者等は本発明の成分範囲内で、D1値の異る鋼を
溶製し、これを60mφに圧延し、1200℃加熱によ
る熱間鍛造にて30龍φにした場合の硬さ、工具寿命の
関係を要約したのが第1図である。
(Example) The present inventors melted steels with different D1 values within the composition range of the present invention, rolled them to 60 mφ, and hot-forged them to 30 mmφ by heating at 1200°C. Figure 1 summarizes the relationship between hardness and tool life.

即ち第1図に示すようにD1値が90mを超えると硬さ
が高くなり、被削性が劣化する。Tiの如何によるミク
ロ組織を第2図に示した。即ちTiの有無でD1値のほ
ぼ同等の2鋼種を30鶴φに熱間鍛造後のミクロ組織を
第2図に示すが、Ti添加鋼の組織はフェライト・パー
ライト、Ti無添加鋼の組織は、フェライト・ベイナイ
トでTi添加により細粒化し焼入性が低下しベイナイト
が出にくくなっていることが知られる。
That is, as shown in FIG. 1, when the D1 value exceeds 90 m, the hardness increases and the machinability deteriorates. Figure 2 shows the microstructure depending on the Ti content. In other words, Figure 2 shows the microstructures of two steel types with almost the same D1 value in the presence and absence of Ti, after hot forging into 30 mm diameter. It is known that the addition of Ti to ferrite and bainite makes the grains finer, lowers the hardenability, and makes it difficult for bainite to form.

更にiとNの添加量を種々変えた鋼を溶製し、1200
 ’cに加熱し、3Qmi+φに鍛伸し、その後、92
0℃で5時間の浸炭を行い、旧オーステナイト粒を観察
した。第3図には粗大粒(粒度隘5以下)発生の有無を
示すが、この第3図より、粗大化防止に、N*は0,0
1%以上必要であり、またA6/N”=1.5〜2.8
となる必要があることが知られる。
Furthermore, steels with various addition amounts of i and N were produced, and 1200
'c, forge-stretched to 3Qmi+φ, then 92
Carburizing was performed at 0° C. for 5 hours, and prior austenite grains were observed. Figure 3 shows the presence or absence of coarse particles (particle size of 5 or less).
1% or more is required, and A6/N”=1.5 to 2.8
It is known that it is necessary to

本発明によるものの具体的な製造例について説明すると
以下の如くである。
A specific manufacturing example of the product according to the present invention will be described below.

本発明者等は次の第1表に示すような化学成分を有する
鋼を溶製し、1200℃に加熱し、30璽■φに鍛伸し
た。
The present inventors melted steel having the chemical composition shown in Table 1 below, heated it to 1200°C, and forged it to a diameter of 30 mm.

上記のようにして得られたものは、その後硬さ、被削性
、浸炭粒度、ジョミニー焼入性試験を行った。即ち硬さ
は、ブリネル硬度計を用い測定し、被削性は、ハイス(
SKH51)チップラ用い、切削速度120 m/mi
n 、切込み21′11送り0.1vs / r6シで
旋削にて工具寿命を測定した。又浸炭粒度は、850〜
1100℃の間を25℃間隔で5時間保持後、焼入れで
、旧オーステナイト粒を測定し、粒度漱5以下の粗大粒
が発生する温度を粗大化温度とした。更にジョミニー焼
入性試験は、JIS  GO561に基づいて行った。
The specimens obtained as described above were then tested for hardness, machinability, carburized grain size, and Jominy hardenability. That is, hardness is measured using a Brinell hardness tester, and machinability is measured using a Brinell hardness tester.
SKH51) Using tipper, cutting speed 120 m/mi
The tool life was measured in turning with a depth of cut of 21'11 and a feed of 0.1 vs/r6. Also, the carburized particle size is 850~
After holding the temperature between 1100°C at 25°C intervals for 5 hours, the prior austenite grains were measured by quenching, and the temperature at which coarse grains with a grain size of 5 or less were generated was defined as the coarsening temperature. Furthermore, the Jominy hardenability test was conducted based on JIS GO561.

このような試験測定の結果は次の第2表の如くである。The results of these test measurements are shown in Table 2 below.

第2表 即ち、このような第2表の結果によるならば、本発明に
従った本発明鋼1〜3は、熱間鍛造ままで、被削性が良
好であるとともに、浸炭時の結晶粒粗大化温度も高い。
According to Table 2, that is, the results of Table 2, inventive steels 1 to 3 according to the present invention have good machinability as hot-forged, and the grain size during carburization is The coarsening temperature is also high.

これに対し比較鋼1は、Ti無添加でり、値が高いこと
もあり、鍛造後の硬さが高く、被削性が悪い。比較鋼2
は鍛造後の被削性は良いものの、DI値が低く、浸炭後
の強度が得られない。又比較鋼3は、Tiの添加量が多
過ぎることと、AA/N’″が2.8以上のため、被削
性が劣り、浸炭後の結晶粒粗大化温度が低い。然して比
較鋼4は、八β/N”が1.6以下のため、浸炭後の結
晶粒粗大化温度が低い。更に比較鋼5はS量が低いため
、被削性が劣る。比較鋼6は、通常のSCM420で焼
ならしを行ったものであり、これは被削性が良好である
が、鍛造ままでは、硬さが高くなり過ぎて、被削性が劣
る。
On the other hand, Comparative Steel 1 does not contain Ti and has a high Ti value, so it has high hardness after forging and poor machinability. Comparison steel 2
Although the machinability after forging is good, the DI value is low and the strength after carburizing cannot be obtained. In addition, Comparative Steel 3 has poor machinability and low grain coarsening temperature after carburizing because the amount of Ti added is too large and AA/N''' is 2.8 or more. Since 8β/N” is 1.6 or less, the crystal grain coarsening temperature after carburizing is low. Furthermore, Comparative Steel 5 has a low S content, so its machinability is poor. Comparative steel 6 was normalized with ordinary SCM420 and has good machinability, but if as-forged, the hardness becomes too high and the machinability is poor.

「発明の効果」 以上説明したような本発明によるときは熱間鍛造後に焼
ならしを行わなくても被削性を劣化することがなく、又
浸炭後も結晶粒粗大化を生じ難いので製造上における省
工程、省エネルギーを充分にもたらし、更に浸炭時の歪
みも小さくなり、低コストに好ましい肌焼鋼を提供し得
るものであるから工業的にその効果の大きい発明である
"Effects of the Invention" According to the present invention as explained above, machinability does not deteriorate even if normalizing is not performed after hot forging, and crystal grain coarsening does not easily occur even after carburizing. This invention is industrially very effective because it sufficiently saves the process and energy mentioned above, and also reduces distortion during carburizing, and provides a case-hardening steel that is preferred at low cost.

【図面の簡単な説明】[Brief explanation of drawings]

図面は本発明の技術的内容を示すものであって、第1図
はり、値と硬さ及び工具寿命の関係を示した図表、第2
図はTiの有無による顕微鏡金属組織を比較して示した
写真で(A)はTi添加なし、(B)は添加ありの場合
を示し、第3図は有効窒素およびsoβ、Aβと粗大粒
の発生状態を要約して示した図表である。 第 岡 (mm) 第 舊 5oLAL (%) 第 賜 (A) (B)
The drawings show the technical content of the present invention;
The figure shows photographs comparing microscopic metal structures with and without Ti. (A) shows the case without the addition of Ti, (B) shows the case with the addition. Figure 3 shows the difference between available nitrogen, soβ, Aβ, and coarse grains. This is a chart summarizing the state of occurrence. No. oka (mm) No. 5 o LAL (%) No. 5 (A) (B)

Claims (1)

【特許請求の範囲】 C:0.15〜0.35wt%、Si:0.5wt%以
下、Mn:1.5wt%以下、Cr:1.5wt%以下
、Mo:0.25wt%以下、 S:0.03〜0.05wt%、 Ti:0.005〜0.015Wt%、 N:(Ti/3.42)+0.01〜0.02wt%、
Al/N^*:1.5〜2.8 (但し、N^*=N−(Ti/3.42))D_I:8
5〜90mm 〔但しD_I=7.95√C(1+0.64Si)(1
+4.1Mn)(1+2.33Cr)(1+3.14M
o)〕を含有し、残部がFeおよび不可避的不純物から
成ることを特徴とした肌焼綱。
[Claims] C: 0.15 to 0.35 wt%, Si: 0.5 wt% or less, Mn: 1.5 wt% or less, Cr: 1.5 wt% or less, Mo: 0.25 wt% or less, S :0.03~0.05wt%, Ti:0.005~0.015wt%, N:(Ti/3.42)+0.01~0.02wt%,
Al/N^*: 1.5 to 2.8 (However, N^* = N-(Ti/3.42)) D_I: 8
5~90mm [However, D_I=7.95√C(1+0.64Si)(1
+4.1Mn) (1+2.33Cr) (1+3.14M
o)] with the remainder consisting of Fe and inevitable impurities.
JP2217125A 1990-08-20 1990-08-20 Case hardening steel Expired - Fee Related JP2546045B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2217125A JP2546045B2 (en) 1990-08-20 1990-08-20 Case hardening steel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2217125A JP2546045B2 (en) 1990-08-20 1990-08-20 Case hardening steel

Publications (2)

Publication Number Publication Date
JPH0499843A true JPH0499843A (en) 1992-03-31
JP2546045B2 JP2546045B2 (en) 1996-10-23

Family

ID=16699246

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2217125A Expired - Fee Related JP2546045B2 (en) 1990-08-20 1990-08-20 Case hardening steel

Country Status (1)

Country Link
JP (1) JP2546045B2 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101967606A (en) * 2010-11-02 2011-02-09 武汉钢铁(集团)公司 Hot rolled steel strip for straight slit electric resistance welding petroleum casing pipe and production method thereof
CN104789878A (en) * 2015-05-05 2015-07-22 内蒙古包钢钢联股份有限公司 Seamless steel tube for high-hardenability oil casing coupling material and preparation method

Citations (4)

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JPS5719324A (en) * 1980-05-30 1982-02-01 Nippon Steel Corp Production of steel for machine structural use for forging having fine structure at high temperature
JPS6247425A (en) * 1985-08-23 1987-03-02 Sumitomo Metal Ind Ltd Manufacture of face hardened steel
JPS634042A (en) * 1986-06-24 1988-01-09 Daido Steel Co Ltd Case hardening steel for cold and warm forging
JPH01191764A (en) * 1988-01-26 1989-08-01 Daido Steel Co Ltd Free cutting steel for carburization quenching

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Publication number Priority date Publication date Assignee Title
JPS5719324A (en) * 1980-05-30 1982-02-01 Nippon Steel Corp Production of steel for machine structural use for forging having fine structure at high temperature
JPS6247425A (en) * 1985-08-23 1987-03-02 Sumitomo Metal Ind Ltd Manufacture of face hardened steel
JPS634042A (en) * 1986-06-24 1988-01-09 Daido Steel Co Ltd Case hardening steel for cold and warm forging
JPH01191764A (en) * 1988-01-26 1989-08-01 Daido Steel Co Ltd Free cutting steel for carburization quenching

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101967606A (en) * 2010-11-02 2011-02-09 武汉钢铁(集团)公司 Hot rolled steel strip for straight slit electric resistance welding petroleum casing pipe and production method thereof
CN104789878A (en) * 2015-05-05 2015-07-22 内蒙古包钢钢联股份有限公司 Seamless steel tube for high-hardenability oil casing coupling material and preparation method

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