JPH0522857Y2 - - Google Patents
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- Publication number
- JPH0522857Y2 JPH0522857Y2 JP1986173730U JP17373086U JPH0522857Y2 JP H0522857 Y2 JPH0522857 Y2 JP H0522857Y2 JP 1986173730 U JP1986173730 U JP 1986173730U JP 17373086 U JP17373086 U JP 17373086U JP H0522857 Y2 JPH0522857 Y2 JP H0522857Y2
- Authority
- JP
- Japan
- Prior art keywords
- aroma
- measurement
- measurement chamber
- chamber
- inert gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- Investigating Or Analyzing Materials By The Use Of Fluid Adsorption Or Reactions (AREA)
- Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)
Description
【考案の詳細な説明】 [産業上の利用分野] 本考案は香気測定装置に関するものである。[Detailed explanation of the idea] [Industrial application field] The present invention relates to an aroma measuring device.
[従来の技術とその問題点]
生鮮食品の出荷時の鮮度評価や食品製造分野、
特に醗酵技術を用いるところでの香気測定による
醗酵度の制御、更には海草、コーヒー、酒類など
にみられるように香気濃度による等級決めを必要
とする分野での品質検査には、香気が重要な役割
を占めている。この品質検査を行なう場合、香気
を構成している各成分に対する測定はさほど必要
がなく、香気のトータル量を即時的に捕らえるこ
とが要求されている。[Conventional technology and its problems] Freshness evaluation during shipping of fresh foods, food manufacturing field,
In particular, aroma plays an important role in controlling the degree of fermentation by measuring aroma when fermentation technology is used, and in quality inspection in fields that require grading based on aroma concentration, such as in seaweed, coffee, and alcoholic beverages. occupies . When performing this quality inspection, it is not so necessary to measure each component that makes up the aroma, and it is required to immediately determine the total amount of aroma.
この品質検査においては、従来人間の嗅覚によ
る官能検査が行なわれている。この検査は味覚や
嗅覚に優れた者を選別して訓練を施こした熟練者
によつて行なうものであり、誰でもができるもの
ではない。また熟練者の養成は時間を要する。更
には、検査の際の検査官の体調によつては検査結
果が異なることもある。 In this quality inspection, a sensory test using the human sense of smell has conventionally been performed. This test is carried out by trained and selected people with excellent sense of taste and smell, and cannot be performed by just anyone. Also, training experts takes time. Furthermore, test results may vary depending on the physical condition of the examiner at the time of the test.
このように香気は、客観性がないだけにその計
測方法や自動監視の技術の確立はむずかしいこと
とされていた。 Because aroma is not objective, it has been thought that it is difficult to establish methods for measuring it or automatic monitoring technology.
また、化粧品或いは酒類等の製造分野では香気
の成分が品質の重要な役割を占めており、このた
め香気成分の分析測定による品質検査が必要であ
る。従来、香気成分の分析には、主にガスクロマ
トグラフが多く用いられ、香気の成分の分離測定
に利用されている。しかし、これには、サンプ
リングの方法による測定結果のバラツキ。分析
にはある程度熟練した者を必要とすること。装
置自体が高価であること。更に重要なことは分
析結果がでるまでにかなりの時間を要する点であ
り、この点で香気濃度のリアルタイムでの測定を
必要とする現場向きではない。 Further, in the field of manufacturing cosmetics or alcoholic beverages, aroma components play an important role in quality, and therefore quality inspection by analysis and measurement of aroma components is necessary. Conventionally, gas chromatographs have been mainly used to analyze aroma components, and are used to separate and measure aroma components. However, this includes variations in measurement results due to the sampling method. Analysis requires a person with some level of skill. The equipment itself is expensive. What is more important is that it takes a considerable amount of time to obtain analysis results, and in this respect, it is not suitable for use in the field where real-time measurement of aroma concentration is required.
特開昭60−194344号公報には、このような問題
を解決する香り濃度測定法及び装置が提案されて
いるが、実用上十分ではなかつた。 JP-A-60-194344 proposes a method and device for measuring fragrance concentration that solves these problems, but it is not sufficient for practical use.
[問題点を解決するための手段] 本考案は上記問題点を解決するものである。[Means for solving problems] The present invention solves the above problems.
即ち本考案は、
収容扉が設けてあり、内部に測定室を備えた測
定ボツクス本体と、
上記測定室の側壁下部に設けられている、不活
性ガスを導入する導入口と、
上記測定室の上部に備えられ、測定室の香気を
測定する香気測定センサと、
測定室内に収容されている被測定物を入れた試
料容器の開口部に蓋をして試料容器内部を密閉す
る密閉装置と、
を備え、
上記測定ボツクス本体の上部には、上記測定室
と連通した香気排出部が設けてあり、
この香気排出部には、香気排出孔を設けた封鎖
体が設けてあり、
この封鎖体には、通常状態では自重によつて上
記香気排出孔を封鎖し、測定の際の不活性ガス導
入時に測定室の内圧が高まると浮上がつて上記香
気排出孔を開放する感圧封鎖板が載置されてい
る、
香気測定装置である。 That is, the present invention comprises: a measurement box body provided with an accommodation door and a measurement chamber inside; an inlet for introducing inert gas provided at the lower side wall of the measurement chamber; and an inlet for introducing an inert gas into the measurement chamber. an aroma measurement sensor provided in the upper part to measure the aroma in the measurement chamber; a sealing device for sealing the inside of the sample container by covering the opening of the sample container containing the object to be measured housed in the measurement chamber; An aroma discharge part communicating with the measurement chamber is provided in the upper part of the measurement box main body, and a sealing body provided with an aroma discharge hole is provided in the aroma discharge part, and the sealing body has is equipped with a pressure-sensitive sealing plate that closes the aroma exhaust hole under its own weight under normal conditions, and floats up to open the aroma exhaust hole when the internal pressure of the measurement chamber increases when inert gas is introduced during measurement. This is an aroma measuring device.
本考案で使用される香気測定センサとしては、
複数個のガスセンサを組合わせたもの或いは単一
のセンサからなるものを挙げることができる。単
一のセンサとしては、酸化錫(SnO2)、酸化亜鉛
(ZnO)等のn形半導体を感応部とし、これを加
熱するヒータを備え半導体の電気抵抗が気体分子
の吸脱着において変化するものであつて感応部酸
化錫(SnO2)、酸化亜鉛(ZnO)等のn形半導体
の単体よりなるものを挙げることができる。これ
らの香気測定センサに、測定に必要な性格をもた
せることによつて、同一試料でその香気濃度の強
弱を検出することができるし、香気の分離分析も
できるようにすることもできる。 The aroma measurement sensor used in this invention is:
Examples include a combination of a plurality of gas sensors or a single sensor. A single sensor uses an n-type semiconductor such as tin oxide (SnO 2 ) or zinc oxide (ZnO) as a sensitive part, and is equipped with a heater to heat it, so that the electrical resistance of the semiconductor changes as gas molecules are adsorbed and desorbed. Among them, the sensitive part may be made of a simple n-type semiconductor such as tin oxide (SnO 2 ) or zinc oxide (ZnO). By providing these aroma measurement sensors with the characteristics necessary for measurement, it is possible to detect the strength or weakness of the aroma concentration in the same sample, and it is also possible to separate and analyze aromas.
密閉装置の構造は特に限定するものではない
が、例えばギヤモータで密閉板を昇降させて試料
容器の開口部を密閉する構造のもの、或は手動レ
バーで密閉板を昇降させる構造のもの等が挙げら
れる。 The structure of the sealing device is not particularly limited, but examples include one that uses a gear motor to raise and lower the sealing plate to seal the opening of the sample container, or one that uses a manual lever to raise and lower the sealing plate. It will be done.
[実施例]
本考案を図面に示した実施例により更に詳細に
説明する。[Example] The present invention will be explained in more detail with reference to an example shown in the drawings.
第1図は本考案の一実施例を示す一部切欠斜視
図、第2図は概略断面図、第3図は内部構造を示
す要部斜視図である。 FIG. 1 is a partially cutaway perspective view showing an embodiment of the present invention, FIG. 2 is a schematic sectional view, and FIG. 3 is a perspective view of essential parts showing the internal structure.
符号1は測定ボツクス本体で、側部には収容扉
2が設けられており、内部には測定室3が形成さ
れ、上部には測定室3と連通した香気排出部4が
形成されている。 Reference numeral 1 denotes a measurement box main body, which is provided with an accommodation door 2 on its side, a measurement chamber 3 formed inside, and an aroma discharge section 4 communicating with the measurement chamber 3 formed in its upper part.
測定室3の上部には香気測定センサ5が備えら
れ、香気測定センサ5の上方の香気排出部4には
香気排出孔7を設けた、封鎖体である封鎖台板6
が形成されており、封鎖台板6には香気排出孔7
を封鎖するように感圧封鎖板8が載置されてい
る。 The upper part of the measurement chamber 3 is equipped with an aroma measurement sensor 5, and the aroma discharge part 4 above the aroma measurement sensor 5 is provided with an aroma discharge hole 7, and a sealing base plate 6 is a sealing body.
is formed, and the sealing base plate 6 has an aroma discharge hole 7.
A pressure-sensitive sealing plate 8 is placed to seal the area.
感圧封鎖板8の封鎖台板6の上面と接触する部
分には通気孔9が設けられており、載置状態では
香気排出孔7は封鎖されている。 A ventilation hole 9 is provided in a portion of the pressure-sensitive sealing plate 8 that contacts the upper surface of the sealing base plate 6, and the aroma discharge hole 7 is sealed in the mounted state.
後述するように測定の際の不活性ガス導入時に
測定室3の内圧が高まると感圧封鎖板8が浮上が
り、測定室3内の不要のガス、香気等は香気排出
孔7から通気孔9を通り、天井部に形成された排
出口10から外部へ排出される。 As will be described later, when the internal pressure of the measurement chamber 3 increases when inert gas is introduced during measurement, the pressure-sensitive sealing plate 8 rises, and unnecessary gases, aromas, etc. in the measurement chamber 3 are discharged from the aroma exhaust hole 7 to the ventilation hole 9. and is discharged to the outside from an outlet 10 formed in the ceiling.
測定室3下部の側壁11,11aには不活性ガ
スを導入する導入口30,30aが設けられてい
る。 The side walls 11, 11a at the bottom of the measurement chamber 3 are provided with inlet ports 30, 30a for introducing inert gas.
また側壁11,11aの導入口30,30aよ
りやや上方には支持梁12が架設されており、そ
のほぼ中心部には昇降ギヤボツクス13を備えて
いる。側壁11aにはギヤモータ14が設けら
れ、回転軸15は昇降ギヤボツクス13を貫通し
て側壁11に設けられた軸受16で支持され、更
に先端部は側壁11を貫通しており制御円盤17
が取付けられている。制御円盤17には突起18
が設けられており、回転軸15の回転によつて上
下に設けられたリミツトスイツチ19,19aの
切入操作をするようにしている。 A support beam 12 is installed slightly above the inlets 30, 30a of the side walls 11, 11a, and a lift gear box 13 is provided at the approximate center of the support beam 12. A gear motor 14 is provided on the side wall 11a, and a rotating shaft 15 passes through the lift gear box 13 and is supported by a bearing 16 provided on the side wall 11. The tip of the rotating shaft 15 passes through the side wall 11 and is connected to a control disk 17.
The control disk 17 has a projection 18.
By the rotation of the rotary shaft 15, limit switches 19, 19a provided above and below are turned on and off.
回転軸15の昇降ギヤボツクス13部分にはピ
ニオンギヤ20が取着されており、ピニオンギヤ
20と噛み合うようにラツクギヤ21が昇降可能
に取着されている。そしてラツクギヤ21下部に
は密閉板22が取着されており、密閉板22の底
面にはゴム板23が設けられている。また密閉板
22はスプリング24によつて下方に付勢されて
おり、試料容器25の開口部に十分に密着し、試
料容器25内を密閉できるようにしている。 A pinion gear 20 is attached to the elevating gear box 13 portion of the rotating shaft 15, and a rack gear 21 is attached so as to be movable up and down so as to mesh with the pinion gear 20. A sealing plate 22 is attached to the lower part of the rack gear 21, and a rubber plate 23 is provided on the bottom surface of the sealing plate 22. Further, the sealing plate 22 is urged downward by a spring 24, and is brought into close contact with the opening of the sample container 25, so that the inside of the sample container 25 can be sealed.
作 用
被測定物を入れた試料容器25を測定室3の
所定の位置に収容する。Operation The sample container 25 containing the object to be measured is accommodated at a predetermined position in the measurement chamber 3.
ギヤモータ14を作動させ、密閉板22を下
降させて試料容器25内部を密閉する。 The gear motor 14 is operated and the sealing plate 22 is lowered to seal the inside of the sample container 25.
導入口30,30aから不活性ガスである窒
素ガスを導入し、これによつて測定室3内の不
要ガスやノイズガスを排出口10から排出す
る。 Nitrogen gas, which is an inert gas, is introduced through the inlet ports 30 and 30a, and thereby unnecessary gas and noise gas in the measurement chamber 3 are discharged through the exhaust port 10.
測定室3内に窒素ガスが充満しきつたところ
で窒素ガスの導入を止め、密閉板22を上昇さ
せて試料容器25の密閉を解除する。 When the measurement chamber 3 is completely filled with nitrogen gas, the introduction of nitrogen gas is stopped, and the sealing plate 22 is raised to release the sealing of the sample container 25.
なお密閉板22の上下の停止位置は回転軸1
5に設けられた制御円盤17の突起18とリミ
ツトスイツチ19,19aにより制御される。 Note that the upper and lower stopping positions of the sealing plate 22 are at the rotation axis 1.
It is controlled by a protrusion 18 of a control disk 17 provided at 5 and limit switches 19, 19a.
測定室3内に試料容器25内の被測定物の香
気が充満し、香気測定センサ5により香気が感
知され、その信号は図示を省略した香気測定装
置に送られ測定装置に設けられたデジタルまた
はアナログメーターによつて定量的に表わされ
る。 The measurement chamber 3 is filled with the aroma of the object to be measured in the sample container 25, the aroma is detected by the aroma measurement sensor 5, and the signal is sent to an aroma measurement device (not shown), which is connected to a digital or It is expressed quantitatively by an analog meter.
なお、本考案は図示の実施例に限定されるも
のではなく、実用新案登録請求の範囲内におい
て数々の変形が可能である。 It should be noted that the present invention is not limited to the illustrated embodiment, and many modifications can be made within the scope of the utility model registration claims.
[考案の効果] 本考案は上記構成を備え、次の効果を奏する。[Effect of the idea] The present invention has the above configuration and has the following effects.
(a) 香気濃度が測定対象物を損ねることなく無傷
のまま、非接触的に及びリアルタイムで測定で
きる。したがつて、鮮度、熟成度といつたこれ
までどちらかというと官能に依存していたとこ
ろを定量的に評価できる。(a) Aroma concentration can be measured non-contact and in real time without damaging the object to be measured. Therefore, it is now possible to quantitatively evaluate aspects such as freshness and ripeness, which until now have been rather dependent on sensory perception.
(b) 測定対象物の香気成分を即時に分析測定し、
予め測定しておいたデータと比較することによ
つて測定試料物の識別あるいは一定の品質を有
する製品かどうかの識別が、測定対象物を損ね
ることなく、無傷のまま、非接触的に、かつリ
アルタイムで可能である。したがつて、分析に
時間がかからず現場での使用ができる。(b) Instantly analyze and measure the aroma components of the object to be measured;
By comparing with previously measured data, it is possible to identify the sample to be measured or to identify whether it is a product of a certain quality without damaging the sample, without damaging it, without contacting it, and Possible in real time. Therefore, analysis does not take much time and can be used in the field.
(c) 装置自体も安価で単純であり、特にリアルタ
イムでの測定ができるので生鮮食品一般につい
て簡便な鮮度測定に適用できると同時に食品製
造工程での品質監視にも広く活用できるばかり
か、食品の出荷時の規準を香気濃度で評価する
出荷規準として、醗酵技術の研究等にも、広い
適用が可能である。(c) The device itself is inexpensive and simple, and in particular can perform measurements in real time, so it can be applied to simple freshness measurements of fresh foods in general, and can also be widely used for quality monitoring in food manufacturing processes. As a shipping standard that evaluates shipping standards based on aroma concentration, it can be widely applied to research on fermentation technology.
(d) 測定前に測定室内や実験室に充満している、
測定に不要なガスは無臭の不活性ガスに置換さ
れるのでセンサが被測定物の香気や他の香気な
どノイズとなるものを感知せず、実験室等様々
な香気のある部屋でも容易に香気測定ができ
る。(d) the measurement room or laboratory is full before the measurement;
Gases unnecessary for measurement are replaced with odorless inert gas, so the sensor does not detect noise such as the scent of the object to be measured or other scents, and can easily detect scents even in rooms with various scents such as laboratories. Can be measured.
(e) 香気の濃度や成分の測定だけでなく拡散速度
の測定もできる。(e) It is possible to measure not only the concentration and components of aromas but also the diffusion rate.
(f) 不活性ガスを導入する導入口は測定室の側壁
下部に設けられており、香気測定センサは測定
室の上部に備えられ、測定室と連通した香気排
出部はボツクス本体の上部に設けてある。(f) An inlet for introducing inert gas is provided at the bottom of the side wall of the measurement chamber, an aroma measurement sensor is provided at the top of the measurement chamber, and an aroma discharge section communicating with the measurement chamber is provided at the top of the box body. There is.
このため不活性ガスは測定室全体を通つて排
出され、測定室内の不要のガス、香気等の排出
効率がよい。 Therefore, the inert gas is discharged through the entire measurement chamber, and unnecessary gases, fragrances, etc. in the measurement chamber are efficiently discharged.
(g) 香気排出部には、香気排出孔を設けた封鎖体
が設けてあり、この封鎖体には、通常状態では
自重によつて香気排出孔を封鎖し、測定の際の
不活性ガス導入時に測定室の内圧が高まると浮
上がつて香気排出孔を開放する感圧封鎖板が載
置されている。(g) The aroma exhaust section is equipped with a sealing body with an aroma exhaust hole, and this sealing body closes the aroma exhaust hole with its own weight under normal conditions and prevents inert gas from being introduced during measurement. A pressure-sensitive sealing plate is mounted that floats up and opens the aroma exhaust hole when the internal pressure of the measurement chamber increases.
このため、簡単な構造で香気排出孔の開閉が
できる。 Therefore, the fragrance exhaust hole can be opened and closed with a simple structure.
第1図は本考案の一実施例を示す一部切欠斜視
図、第2図は概略断面図、第3図は内部構造を示
す要部斜視図である。
1……測定ボツクス本体、3……測定室、3
0,30a……導入口、5……香気測定センサ、
14……ギヤモータ、22……密閉板。
FIG. 1 is a partially cutaway perspective view showing an embodiment of the present invention, FIG. 2 is a schematic sectional view, and FIG. 3 is a perspective view of essential parts showing the internal structure. 1...Measurement box body, 3...Measurement chamber, 3
0,30a...Inlet, 5...Fragrance measurement sensor,
14... Gear motor, 22... Sealing plate.
Claims (1)
定ボツクス本体と、 上記測定室の側壁下部に設けられている、不活
性ガスを導入する導入口と、 上記測定室の上部に備えられ、測定室の香気を
測定する香気測定センサと、 測定室内に収容されている被測定物を入れた試
料容器の開口部に蓋をして試料容器内部を密閉す
る密閉装置と、 を備え、 上記測定ボツクス本体の上部には、上記測定室
と連通した香気排出部が設けてあり、 この香気排出部には、香気排出孔を設けた封鎖
体が設けてあり、 この封鎖体には、通常状態では自重によつて上
記香気排出孔を封鎖し、測定の際の不活性ガス導
入時に測定室の内圧が高まると浮上がつて上記香
気排出孔を開放する感圧封鎖板が載置されてい
る、 香気測定装置。[Scope of Claim for Utility Model Registration] A measuring box body with a housing door and a measuring chamber inside; An inlet for introducing inert gas provided at the lower part of the side wall of the measuring chamber; and the above. An aroma measurement sensor that is installed at the top of the measurement chamber and measures the aroma in the measurement chamber, and a seal that seals the inside of the sample container by covering the opening of the sample container containing the object to be measured housed in the measurement chamber. An aroma discharge part communicating with the measurement chamber is provided in the upper part of the measurement box main body, and a sealing body provided with an aroma discharge hole is provided in this aroma discharge part, and this The sealing body includes a pressure-sensitive sealing plate that seals the aroma exhaust hole under its own weight under normal conditions, and floats up to open the aroma exhaust hole when the internal pressure of the measurement chamber increases when inert gas is introduced during measurement. An aroma measuring device on which is installed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1986173730U JPH0522857Y2 (en) | 1986-11-11 | 1986-11-11 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1986173730U JPH0522857Y2 (en) | 1986-11-11 | 1986-11-11 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6378260U JPS6378260U (en) | 1988-05-24 |
| JPH0522857Y2 true JPH0522857Y2 (en) | 1993-06-11 |
Family
ID=31111465
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1986173730U Expired - Lifetime JPH0522857Y2 (en) | 1986-11-11 | 1986-11-11 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH0522857Y2 (en) |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60194344A (en) * | 1984-03-16 | 1985-10-02 | Katsuo Ebara | Method and apparatus for measuring concentration of aroma |
| JPS60173730A (en) * | 1985-01-25 | 1985-09-07 | Hitachi Ltd | optical head device |
-
1986
- 1986-11-11 JP JP1986173730U patent/JPH0522857Y2/ja not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6378260U (en) | 1988-05-24 |
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