JPH0566101B2 - - Google Patents

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Publication number
JPH0566101B2
JPH0566101B2 JP60069087A JP6908785A JPH0566101B2 JP H0566101 B2 JPH0566101 B2 JP H0566101B2 JP 60069087 A JP60069087 A JP 60069087A JP 6908785 A JP6908785 A JP 6908785A JP H0566101 B2 JPH0566101 B2 JP H0566101B2
Authority
JP
Japan
Prior art keywords
vinegar
acetic acid
raw materials
fermentation
acid fermentation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP60069087A
Other languages
Japanese (ja)
Other versions
JPS61227776A (en
Inventor
Tomohiko Fukuda
Sumio Akita
Naotake Ooyama
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NAKANO SUTEN KK
Original Assignee
NAKANO SUTEN KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NAKANO SUTEN KK filed Critical NAKANO SUTEN KK
Priority to JP60069087A priority Critical patent/JPS61227776A/en
Publication of JPS61227776A publication Critical patent/JPS61227776A/en
Publication of JPH0566101B2 publication Critical patent/JPH0566101B2/ja
Granted legal-status Critical Current

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  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Description

【発明の詳細な説明】[Detailed description of the invention]

〔産業上の利用分野〕 本発明は食酢の製造方法、詳しくは優れた香味
を有する食酢の製造方法に関する。 〔従来の技術〕 常法の食酢製造法においては、種々の穀物、果
実等を用いた酢酸発酵調製醪または酢酸発酵調製
液を酢酸発酵させ発酵終了後常温で熟成させるこ
とが知られている。しかし、これら従来の方法に
より作られる米酢、粕酢、ぶどう酢等の食酢は酸
味、酸臭が強く感じられ、一般に酢が好まれない
原因の1つとなつている。 〔発明が解決しようとする問題点〕 上述の様に、従来法で製造される食酢には特有
の酸味、酸臭があり、これが一般に酢が好まれな
い原因の1つであり、食酢の需要拡大を妨げる大
きな要因となつている。 本発明は、この問題を解決したもので、優れた
香味を有し、酸味、酸臭を感じさせない食酢を製
造する方法を提供することを目的とするものであ
る。 〔問題点を解決するための手段〕 上記問題を解決するための手段である本発明
は、澱粉質原料または澱粉質原料と蛋白質原料を
酵素による分解と酵母による発酵を行つて得た酒
精発酵醪を圧搾および/または過して得られた
酒精含有液もしくはこれに必要に応じて酒精を加
えた酒精含有液に種酢と水を加え混合した酢酸発
酵調製液に、〓を20%(W/V)以下の範囲で添
加して酢酸発酵を行い、発酵終了後、この醪を70
〜80℃で熟成させることを特徴とする食酢の製造
方法である。 本発明において澱粉質原料としては、たとえば
米、小麦、大麦、コーン、高梁、粟などの穀類や
これらの副産物(例えばふすま)等様々のものを
単独でまたは組合せて用いることができる。 また、蛋白質原料としては、各種のものが用い
られ、たとえば大豆、豌豆などの豆類、その副産
物、小麦グルテン、コーングルテンなどを単独で
または組合せて使用することができる。 上記原料については、常法による処理、たとえ
ば原料組織の軟化、澱粉のα化、殺菌、磨砕等が
適宜行われる。 また、本発明に使用される酵素としては、各種
起源のものが使用でき、微生物由来のものが好適
で、具体的には澱粉質原料または澱粉質原料と蛋
白質原料とを分解する酵素を生産する微生物、た
とえば黄麹菌、黒麹菌、リゾプス属およびバチル
ス属の微生物の固体培養物(すなわち麹)または
液体培養物もしくはこれら培養物から常法によつ
て得た粗酵素や精製酵素が挙げられ、これらは単
独で、あるいは適宜組合せて用いることができ
る。 また、酵母は澱粉質原料または澱粉質原料と蛋
白質原料を上記の酵素により分解したものを酒精
発酵させる場合に用いられ、この酵母としては、
醸造食品等の食品の製造に使用されているものを
任意に使用でき、その具体例としてたとえば清酒
酵母、ビール酵母、ワイン酵母、パン酵母などが
挙げられる。 本発明では、澱粉質原料または澱粉質原料と蛋
白質原料を酵素による分解と酵母による発酵を行
なつて得た酒精発酵醪を圧搾および/または過
して得られた酒精含有液もしくはこれに必要に応
じて酒精を加えた酒精含有液に種酢と水を加えて
調製した酢酸発酵調製液に、〓を20%(W/V)
以下の範囲、好ましくは5〜15%(W/V)の範
囲で添加して酢酸発酵を行う。 これに使用する〓は、小麦粉を製造する際に生
じる副産物であり、通常市販されているものを用
いても何らさしつかえはなく、また使用時に蒸
煮、殺菌を行うことは必ずしも必要ではない。 また酢酸発酵調製液に〓を添加する場合、同時
に他の穀類の副産物、例えばそばがら、粟がら、
もみがらなどを〓と併用しても何らさしつかえは
ない。 酢酸発酵の条件は常法の酢酸発酵の条件と同様
でよく、〓を加えたことにより、特別な条件を設
定する必要はない。 また酢酸発酵終了後、再度〓を添加することも
可能であり、その添加量には特に限定はないが、
酢酸発酵調製液に添加した〓量との合計が35%
(W/V)以下となる様に添加することが適当で
ある。 発酵終了後の醪の熟成は、好しくは密ぺい槽内
で、70〜80℃で行い、必要に応じて撹拌する。熟
成の期間には特に限定はないが、通常は1〜10日
間、好ましくは4〜6日間であり、熟成終了後は
圧搾もしくは過を行い、以下常法にしたがつて
処理して食酢を得る。 本発明によつて得られる食酢は、〓を添加して
酢酸発酵を行い、更に70〜80℃で熟成させている
ため、特有の酸味、酸臭が感じられず、まろやか
で優れた香味を有する食酢である。 〔発明の効果〕 本発明によれば、下記試験例から認められるよ
うに、従来の食酢に特有の酸味、酸臭が感じられ
ない、まろやかな食酢が得られ、したがつて嗜好
上の制約が解消し、食酢の需要拡大が期待され
る。 試験例 後記する実施例1により得られた本発明製品で
ある食酢(酢酸濃度4.5%、以下試料Aという)、
常法により得られた醸造粕酢(酢酸濃度4.5%、
以下試料Bという)について習熟したパネル20名
により官能評価を行つた。官能評価は2点識別試
験法(「食品の品質測定」−食品工学シリーズ、第
15巻、40〜42頁、1961年光琳書院発行)を用いて
行い、酸味、酸臭について弱いと思う方を選択
し、有意差検定を行つた。その結果を第1表に示
す。
[Industrial Application Field] The present invention relates to a method for producing vinegar, and more particularly, to a method for producing vinegar having excellent flavor. [Prior Art] In the conventional vinegar production method, it is known that an acetic acid fermentation prepared mash or an acetic acid fermentation prepared liquid using various grains, fruits, etc. is subjected to acetic acid fermentation, and after completion of fermentation, it is aged at room temperature. However, the vinegars produced by these conventional methods, such as rice vinegar, lees vinegar, and grape vinegar, have a strong sour taste and odor, which is one of the reasons why vinegar is not generally liked. [Problems to be solved by the invention] As mentioned above, vinegar produced by conventional methods has a unique sour taste and odor, and this is one of the reasons why vinegar is not generally liked, and the demand for vinegar has increased. This is a major factor hindering expansion. The present invention solves this problem and aims to provide a method for producing vinegar that has excellent flavor and does not give a sour taste or odor. [Means for Solving the Problems] The present invention, which is a means for solving the above-mentioned problems, provides a fermented sake mash obtained by decomposing starchy raw materials or starchy raw materials and protein raw materials with enzymes and fermenting with yeast. 20% (W/ V) Perform acetic acid fermentation by adding in the following range, and after fermentation, this moromi
This method of producing vinegar is characterized by aging at ~80°C. In the present invention, various starchy raw materials can be used singly or in combination, such as grains such as rice, wheat, barley, corn, takahashi, and millet, and their byproducts (eg, bran). In addition, various types of protein raw materials can be used, such as legumes such as soybeans and potato beans, by-products thereof, wheat gluten, corn gluten, etc., alone or in combination. The above-mentioned raw materials are appropriately subjected to conventional treatments such as softening of the raw material structure, gelatinization of starch, sterilization, and grinding. In addition, the enzymes used in the present invention can be of various origins, and those derived from microorganisms are preferred. Specifically, enzymes used to produce enzymes that decompose starchy raw materials or starchy raw materials and protein raw materials are used. Examples include solid cultures (i.e., koji) or liquid cultures of microorganisms of the genus Aspergillus yellow, Aspergillus aspergillus, Rhizopus, and Bacillus, as well as crude enzymes and purified enzymes obtained from these cultures by conventional methods. can be used alone or in appropriate combination. Yeast is also used for alcoholic fermentation of starchy raw materials or starchy raw materials and protein raw materials decomposed by the enzymes mentioned above.
Any yeast used in the production of foods such as brewed foods can be used, and specific examples thereof include sake yeast, beer yeast, wine yeast, and baker's yeast. In the present invention, an alcohol-containing liquid obtained by squeezing and/or filtering an alcoholic fermented mash obtained by decomposing a starchy raw material or a starchy raw material and a protein raw material by enzymatic decomposition and fermentation by yeast, or an alcoholic liquor necessary for this, is used. Add 20% (W/V) of 〓 to the acetic acid fermentation preparation liquid prepared by adding seed vinegar and water to the alcoholic liquid containing alcoholic spirit.
Acetic acid fermentation is performed by adding in the following range, preferably in the range of 5 to 15% (W/V). The 〓 used for this is a by-product produced during the production of wheat flour, and there is no problem in using the one that is normally commercially available, and it is not necessarily necessary to steam or sterilize it before use. In addition, when adding 〓 to the acetic acid fermentation preparation, other grain by-products such as buckwheat hulls, millet hulls, etc.
There is nothing wrong with using rice husk etc. in combination with 〓. The conditions for acetic acid fermentation may be the same as those for conventional acetic acid fermentation, and by adding 〓, there is no need to set any special conditions. It is also possible to add 〓 again after the completion of acetic acid fermentation, and there is no particular limitation on the amount added, but
The total amount with the amount added to the acetic acid fermentation preparation solution is 35%.
(W/V) or less is appropriate. Aging of the moromi after fermentation is preferably carried out at 70 to 80°C in a tightly sealed tank, with stirring as necessary. There is no particular limitation on the period of aging, but it is usually 1 to 10 days, preferably 4 to 6 days, and after the aging is finished, it is squeezed or filtered, and then processed according to the conventional method to obtain vinegar. . The vinegar obtained by the present invention undergoes acetic acid fermentation by adding 〓 and is further aged at 70 to 80°C, so it has no characteristic sour taste or odor and has a mellow and excellent flavor. It's vinegar. [Effects of the Invention] According to the present invention, as can be seen from the test examples below, it is possible to obtain mild vinegar that does not have the sour taste and sour odor characteristic of conventional vinegar, and therefore has no restrictions on taste. The situation is expected to be resolved, and demand for vinegar is expected to increase. Test Example Vinegar, which is a product of the present invention obtained in Example 1 described later (acetic acid concentration 4.5%, hereinafter referred to as sample A),
Brewing lees vinegar (acetic acid concentration 4.5%,
A sensory evaluation was conducted by 20 experienced panelists regarding Sample B). Sensory evaluation is based on the two-point discrimination test method ("Food quality measurement" - Food engineering series, Vol.
Volume 15, pages 40-42, published by Korin Shoin in 1961), and we selected those that were considered to be weak in sour taste and sour odor, and conducted a significant difference test. The results are shown in Table 1.

〔実施例〕〔Example〕

次に本発明の実施例を示すが、本発明はこれに
より制限されるものではない。 実施例 1 大麦1400Kgと豌豆600Kgを混合し、常法通り120
℃で45分間蒸煮した。これにアスペルギルス・オ
リゼーIAM2616を接種し、30℃で45時間培養し
て麹1440Kgを得た。 また、マイロ1500Kgを750の冷水に12時間浸
漬後、100℃で90分間蒸煮し、これに70℃の温水
3375を加えて充分混和した。これを25℃まで冷
却した後、上記の麹937.5Kgと水975を加え、酒
母100を添加混合して25〜30℃で5日間平行複
発酵を行つた。得られた酒精発酵醪を圧搾して、
エタノール濃度10.5%の酒精液3000を得た。 この酒精液2850と種酢5400に水を加えて
10000とした後、〓を1000Kg添加し、充分撹拌
したのち30℃で30日間酢酸発酵を行つた。 酢酸発酵終了後、醪に更に〓1500Kgを添加し充
分撹拌したのち、密ぺい槽内で75℃で4日間熟成
させた。この間、1回/日の割合で醪を撹拌し
た。その後、この醪を過し、更に1ケ月間常温
で熟成させたのち、ケイソウ土過、殺菌、びん
詰をして酢酸濃度4.5%の、酸味、酸臭の感じら
れないきわめて濃厚な食酢を得た。 実施例 2 脱脂大豆200Kgに100%撤水し、これに小麦粉
140Kgを混合し常法通り120℃で45分間蒸煮した。
これにアスペルギルス・ソーヤIFO4239を接種
し、30℃で43時間培養した。この様にして得られ
た麹250Kgに、玄米180Kgを冷水に20〜24時間浸漬
後、100℃で60分間蒸煮したものを混合した後、
水を加えて1000としたものに、酒母10を添加
混合し、25〜30℃で5日間平行複発酵を行なつ
た。得られた酒精発酵醪を圧搾してエタノール濃
度9%の酒精液850を得た。 この酒精液300と、種酢540に水を加えて
1000とした後、〓50Kgともみがら50Kgを添加
し、充分撹拌したのち、30℃で30日間酢酸発酵を
行つた。 酢酸発酵終了後、醪を密ぺい槽内で80℃で5日
間熟成させた。この間、1回/日の割合で醪を撹
拌した。その後、この醪を過し、更に1ケ月間
常温で熟成させた後、ケイソウ土過、殺菌、び
ん詰をして酢酸濃度5.0%の、酸味、酸臭の感じ
られないきわめて醇厚な食酢を得た。 実施例 3 米360Kgを一夜水に浸漬し水切し、ついで120℃
で45分間蒸煮した後、水を加えて1000とし、こ
れに市販のアミラーゼ酵素剤0.4Kgを添加して充
分混合し、55℃で70時間糖化した。これに、あら
かじめ前培養しておいた酒母10を加え、30℃で
5日間酒精発酵を行い、発酵終了後、この醪を圧
搾してエタノール濃度12%の米酒液700を得た。 この米酒液250に種酢540と水を加えて1000
とし後、〓75Kgを添加して充分撹拌し、30℃で
30日間酢酸発酵を行つた。 酢酸発酵終了後、更にもみがら70Kgを添加し、
充分撹拌した後、密ぺい槽内で75℃で5日間熟成
させた。この間、1回/日の割合で醪を撹拌し
た。その後、この醪を過し、更に1ケ月間常温
で熟成させた後、ケイソウ土過、殺菌、びん詰
をして、酢酸濃度4.5%の酸味、酸臭の感じられ
ない食酢を得た。
Next, examples of the present invention will be shown, but the present invention is not limited thereto. Example 1 1400Kg of barley and 600Kg of potato beans were mixed, and 120Kg of barley was mixed as usual.
Steamed at ℃ for 45 minutes. This was inoculated with Aspergillus oryzae IAM2616 and cultured at 30°C for 45 hours to obtain 1440 kg of koji. In addition, 1,500 kg of Milo was soaked in 750°C cold water for 12 hours, then steamed at 100°C for 90 minutes, and then heated with 70°C water.
3375 was added and mixed thoroughly. After cooling this to 25°C, 937.5 kg of the above-mentioned koji and 975 kg of water were added, and 100 ml of yeast mash was added and mixed, and parallel multiple fermentation was carried out at 25 to 30° C. for 5 days. The obtained alcoholic fermented moromi is pressed,
3000 pieces of sake semen with an ethanol concentration of 10.5% were obtained. Add water to this sake semen 2850 and seed vinegar 5400.
After adjusting the concentration to 10,000, 1,000 kg of 〓 was added, and after thorough stirring, acetic acid fermentation was carried out at 30°C for 30 days. After the acetic acid fermentation was completed, an additional 1,500 kg was added to the moromi, thoroughly stirred, and then aged at 75°C for 4 days in a tightly sealed tank. During this time, the moromi was stirred once a day. After that, this moromi is filtered and further aged at room temperature for one month, then filtered with diatomaceous earth, sterilized, and bottled to obtain extremely rich vinegar with an acetic acid concentration of 4.5% and no sour taste or odor. Ta. Example 2 100% water was removed from 200 kg of defatted soybeans, and flour was added to this.
140 kg were mixed and steamed at 120°C for 45 minutes as usual.
This was inoculated with Aspergillus sojae IFO4239 and cultured at 30°C for 43 hours. After mixing 250 kg of koji obtained in this way with 180 kg of brown rice soaked in cold water for 20 to 24 hours and then steamed at 100℃ for 60 minutes,
Water was added to bring the concentration to 1000, and 10 mash of yeast was added and mixed, and parallel multiple fermentation was carried out at 25 to 30°C for 5 days. The obtained alcoholic fermented mash was pressed to obtain 850 sake semen with an ethanol concentration of 9%. Add water to 300% of this sake semen and 540% of seed vinegar.
After adjusting the temperature to 1000, 50 kg and 50 kg of rice hulls were added, and after thorough stirring, acetic acid fermentation was carried out at 30°C for 30 days. After the acetic acid fermentation was completed, the moromi was aged in a tightly sealed tank at 80°C for 5 days. During this time, the moromi was stirred once a day. After that, this moromi is filtered and further aged at room temperature for one month, then filtered with diatomaceous earth, sterilized, and bottled to obtain extremely rich vinegar with an acetic acid concentration of 5.0% and no sour taste or odor. Ta. Example 3 360 kg of rice was soaked in water overnight, drained, and then heated to 120°C.
After steaming for 45 minutes, water was added to bring the concentration to 1000, and 0.4 kg of a commercially available amylase enzyme was added thereto, thoroughly mixed, and saccharified at 55°C for 70 hours. Sake mash 10, which had been precultured in advance, was added to this, and alcoholic fermentation was carried out at 30°C for 5 days. After fermentation, this moromi was pressed to obtain rice liquor liquid 700 with an ethanol concentration of 12%. Add 540% of seed vinegar and water to 250% of this rice wine liquid to make 1000%
After cooling, add 75 kg, stir thoroughly, and heat at 30℃.
Acetic acid fermentation was carried out for 30 days. After the acetic acid fermentation was completed, 70 kg of rice husks were added,
After thorough stirring, the mixture was aged at 75°C for 5 days in a tightly sealed tank. During this time, the moromi was stirred once a day. After that, this moromi was filtered and further aged at room temperature for one month, then filtered with diatomaceous earth, sterilized, and bottled to obtain vinegar with an acetic acid concentration of 4.5% and no sour taste or odor.

Claims (1)

【特許請求の範囲】[Claims] 1 澱粉質原料または澱粉質原料と蛋白質原料を
酵素による分解と酵母による発酵を行つて得た酒
精発酵醪を圧搾および/または過し得られた酒
精含有液もしくはこれに必要に応じて酒精を加え
た酒精含有液に種酢と水を加え混合した酢酸発酵
調製液に、〓を20%(W/V)以下の範囲で添加
して酢酸発酵を行い、発酵終了後、この醪を70〜
80℃で熟成させることを特徴とする食酢の製造方
法。
1. Alcohol-containing liquid obtained by squeezing and/or filtering the fermented alcoholic moromi obtained by decomposing starchy raw materials or starchy raw materials and protein raw materials with enzymes and fermenting with yeast, or adding alcoholic spirit to this as necessary. Acetic acid fermentation is carried out by adding 〓 in a range of 20% (W/V) or less to an acetic acid fermentation preparation liquid made by adding and mixing seed vinegar and water to an alcohol-containing liquid. After fermentation, this mash is
A method for producing vinegar, which is characterized by aging at 80℃.
JP60069087A 1985-04-03 1985-04-03 Production of edible vinegar Granted JPS61227776A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP60069087A JPS61227776A (en) 1985-04-03 1985-04-03 Production of edible vinegar

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP60069087A JPS61227776A (en) 1985-04-03 1985-04-03 Production of edible vinegar

Publications (2)

Publication Number Publication Date
JPS61227776A JPS61227776A (en) 1986-10-09
JPH0566101B2 true JPH0566101B2 (en) 1993-09-21

Family

ID=13392452

Family Applications (1)

Application Number Title Priority Date Filing Date
JP60069087A Granted JPS61227776A (en) 1985-04-03 1985-04-03 Production of edible vinegar

Country Status (1)

Country Link
JP (1) JPS61227776A (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2000035A1 (en) * 2007-06-07 2008-12-10 PURAC Biochem BV Method for removing odor from vinegar
JP6024942B2 (en) * 2012-02-29 2016-11-16 株式会社福山こめ酢 Testosterone secretion promoter, anti-fatigue agent, and production method and use thereof

Also Published As

Publication number Publication date
JPS61227776A (en) 1986-10-09

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