JPH0566387B2 - - Google Patents

Info

Publication number: JPH0566387B2
Authority: JP; Japan
Prior art keywords: reactor; mineral oil; reaction; starting materials; boiling point
Prior art date: 1982-12-07
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Lifetime

Application number

JP58229971A

Other languages

English (en)

Japanese (ja)

Other versions

JPS59116268A (ja

Inventor

Dotsukunaa Tooni

Kuruuku Heruberuto

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

BASF SE

Original Assignee

BASF SE

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-12-07

Filing date

1983-12-07

Publication date

1993-09-21

Family has litigation

First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=6179935&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JPH0566387(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.

1983-12-07 Application filed by BASF SE filed Critical BASF SE

1984-07-05 Publication of JPS59116268A publication Critical patent/JPS59116268A/ja

1993-09-21 Publication of JPH0566387B2 publication Critical patent/JPH0566387B2/ja

Status Granted legal-status Critical Current

Links

239000002480 mineral oil Substances 0.000 claims abstract description 34
235000010446 mineral oil Nutrition 0.000 claims abstract description 33
238000000034 method Methods 0.000 claims abstract description 24
239000007858 starting material Substances 0.000 claims abstract description 24
238000009835 boiling Methods 0.000 claims abstract description 21
239000007788 liquid Substances 0.000 claims abstract description 15
238000006482 condensation reaction Methods 0.000 claims abstract description 14
239000003054 catalyst Substances 0.000 claims description 23
239000007795 chemical reaction product Substances 0.000 claims description 13
238000006243 chemical reaction Methods 0.000 claims description 12
239000003921 oil Substances 0.000 claims description 12
229930195733 hydrocarbon Natural products 0.000 claims description 3
150000002430 hydrocarbons Chemical class 0.000 claims description 3
239000004215 Carbon black (E152) Substances 0.000 claims description 2
229910052799 carbon Inorganic materials 0.000 claims description 2
238000004821 distillation Methods 0.000 claims description 2
239000006227 byproduct Substances 0.000 claims 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 14
239000007789 gas Substances 0.000 description 12
229910052757 nitrogen Inorganic materials 0.000 description 7
239000000047 product Substances 0.000 description 7
HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 6
238000000354 decomposition reaction Methods 0.000 description 5
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 4
-1 aromatic sulfonic acids Chemical class 0.000 description 4
239000010453 quartz Substances 0.000 description 4
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
WBIQQQGBSDOWNP-UHFFFAOYSA-N 2-dodecylbenzenesulfonic acid Chemical compound CCCCCCCCCCCCC1=CC=CC=C1S(O)(=O)=O WBIQQQGBSDOWNP-UHFFFAOYSA-N 0.000 description 3
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
238000009833 condensation Methods 0.000 description 3
230000005494 condensation Effects 0.000 description 3
229940060296 dodecylbenzenesulfonic acid Drugs 0.000 description 3
MTNDZQHUAFNZQY-UHFFFAOYSA-N imidazoline Chemical compound C1CN=CN1 MTNDZQHUAFNZQY-UHFFFAOYSA-N 0.000 description 3
239000006200 vaporizer Substances 0.000 description 3
OTPDWCMLUKMQNO-UHFFFAOYSA-N 1,2,3,4-tetrahydropyrimidine Chemical compound C1NCC=CN1 OTPDWCMLUKMQNO-UHFFFAOYSA-N 0.000 description 2
ITQTTZVARXURQS-UHFFFAOYSA-N 3-methylpyridine Chemical compound CC1=CC=CN=C1 ITQTTZVARXURQS-UHFFFAOYSA-N 0.000 description 2
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
230000002378 acidificating effect Effects 0.000 description 2
229910021529 ammonia Inorganic materials 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
239000000295 fuel oil Substances 0.000 description 2
238000010574 gas phase reaction Methods 0.000 description 2
239000008246 gaseous mixture Substances 0.000 description 2
239000011521 glass Substances 0.000 description 2
239000011261 inert gas Substances 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
ABVVEAHYODGCLZ-UHFFFAOYSA-N tridecan-1-amine Chemical compound CCCCCCCCCCCCCN ABVVEAHYODGCLZ-UHFFFAOYSA-N 0.000 description 2
NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 description 1
LBLYYCQCTBFVLH-UHFFFAOYSA-N 2-Methylbenzenesulfonic acid Chemical compound CC1=CC=CC=C1S(O)(=O)=O LBLYYCQCTBFVLH-UHFFFAOYSA-N 0.000 description 1
MCGBIXXDQFWVDW-UHFFFAOYSA-N 4,5-dihydro-1h-pyrazole Chemical compound C1CC=NN1 MCGBIXXDQFWVDW-UHFFFAOYSA-N 0.000 description 1
150000000565 5-membered heterocyclic compounds Chemical class 0.000 description 1
150000000644 6-membered heterocyclic compounds Chemical class 0.000 description 1
PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
CKUAXEQHGKSLHN-UHFFFAOYSA-N [C].[N] Chemical group [C].[N] CKUAXEQHGKSLHN-UHFFFAOYSA-N 0.000 description 1
239000002253 acid Substances 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
238000007259 addition reaction Methods 0.000 description 1
150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 description 1
229940092714 benzenesulfonic acid Drugs 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000011203 carbon fibre reinforced carbon Chemical group 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
230000009849 deactivation Effects 0.000 description 1
238000010586 diagram Methods 0.000 description 1
238000005194 fractionation Methods 0.000 description 1
150000002391 heterocyclic compounds Chemical class 0.000 description 1
IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 description 1
238000007654 immersion Methods 0.000 description 1
PRSKAITVGVQSEU-UHFFFAOYSA-N n-(2-aminoethyl)-n-formylformamide Chemical compound NCCN(C=O)C=O PRSKAITVGVQSEU-UHFFFAOYSA-N 0.000 description 1
NBNDPGGJEJRDBJ-UHFFFAOYSA-N n-(2-formamidoethyl)formamide Chemical compound O=CNCCNC=O NBNDPGGJEJRDBJ-UHFFFAOYSA-N 0.000 description 1
GQDCNSNHIMZCMH-UHFFFAOYSA-N n-(2-formamidopropyl)formamide Chemical compound O=CNC(C)CNC=O GQDCNSNHIMZCMH-UHFFFAOYSA-N 0.000 description 1
BVGACDWWDWVMME-UHFFFAOYSA-N n-(3-formamidopropyl)formamide Chemical compound O=CNCCCNC=O BVGACDWWDWVMME-UHFFFAOYSA-N 0.000 description 1
238000011017 operating method Methods 0.000 description 1
239000012188 paraffin wax Substances 0.000 description 1
150000002989 phenols Chemical class 0.000 description 1
OXNIZHLAWKMVMX-UHFFFAOYSA-N picric acid Chemical compound OC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O OXNIZHLAWKMVMX-UHFFFAOYSA-N 0.000 description 1
150000003141 primary amines Chemical class 0.000 description 1
238000000746 purification Methods 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
230000008929 regeneration Effects 0.000 description 1
238000011069 regeneration method Methods 0.000 description 1
150000003335 secondary amines Chemical class 0.000 description 1
150000003512 tertiary amines Chemical class 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
238000010626 work up procedure Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/06—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
- B01J12/005—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor carried out at high temperatures, e.g. by pyrolysis
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
- C07D213/08—Preparation by ring-closure
- C07D213/09—Preparation by ring-closure involving the use of ammonia, amines, amine salts, or nitriles
- C07D213/12—Preparation by ring-closure involving the use of ammonia, amines, amine salts, or nitriles from unsaturated compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/04—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
- C07D233/06—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
- C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
- C07D239/06—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Pyridine Compounds (AREA)
Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

JP58229971A 1982-12-07 1983-12-07 有機縮合反応を実施する方法 Granted JPS59116268A (ja)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE19823245109 DE3245109A1 (de)	1982-12-07	1982-12-07	Verfahren zur durchfuehrung von organischen kondensationsreaktionen
DE3245109.1		1982-12-07

Publications (2)

Publication Number	Publication Date
JPS59116268A JPS59116268A (ja)	1984-07-05
JPH0566387B2 true JPH0566387B2 (de)	1993-09-21

Family

ID=6179935

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP58229971A Granted JPS59116268A (ja)	1982-12-07	1983-12-07	有機縮合反応を実施する方法

Country Status (6)

Country	Link
US (1)	US4551528A (de)
EP (1)	EP0110411B1 (de)
JP (1)	JPS59116268A (de)
AT (1)	ATE19053T1 (de)
CA (1)	CA1253496A (de)
DE (2)	DE3245109A1 (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE3643011A1 (de) *	1986-12-17	1988-06-30	Basf Ag	Verfahren zur herstellung von caprolactam aus 6-aminocapronsaeure, deren estern und amiden
US7003215B2 (en) *	2002-01-21	2006-02-21	Air Products And Chemicals, Inc.	Vapor flow controller

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR847617A (fr) *	1937-12-18	1939-10-12		Procédé pour la fabrication de produits synthétiques liquiques ou gazeux à partir de constituants gazeux
CH214894A (de) *	1938-08-31	1941-05-31	Degussa	Verfahren zur Durchführung chemischer Reaktionen in Schmelzen.
GB1298687A (en) *	1970-04-13	1972-12-06	Montedison Spa	The catalytic preparation of alpha-picoline and gamma-picoline
US4231757A (en) *	1978-06-02	1980-11-04	The Lubrizol Corporation	Nitro phenol-amine condensates, methods of making same, fuels and additive concentrates containing them
US4284555A (en) *	1979-04-27	1981-08-18	Schering Corporation	7-Chloro-8(substituted amino carbonyloxy)-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepines
US4444956A (en) *	1982-11-08	1984-04-24	Standard Oil Company (Indiana)	Process for preparation of Mannich condensation product

1982
- 1982-12-07 DE DE19823245109 patent/DE3245109A1/de not_active Withdrawn
1983
- 1983-12-01 EP EP83112078A patent/EP0110411B1/de not_active Expired
- 1983-12-01 AT AT83112078T patent/ATE19053T1/de not_active IP Right Cessation
- 1983-12-01 DE DE8383112078T patent/DE3362956D1/de not_active Expired
- 1983-12-06 CA CA000442682A patent/CA1253496A/en not_active Expired
- 1983-12-06 US US06/558,442 patent/US4551528A/en not_active Expired - Lifetime
- 1983-12-07 JP JP58229971A patent/JPS59116268A/ja active Granted

Also Published As

Publication number	Publication date
DE3362956D1 (en)	1986-05-15
US4551528A (en)	1985-11-05
EP0110411B1 (de)	1986-04-09
EP0110411A1 (de)	1984-06-13
ATE19053T1 (de)	1986-04-15
DE3245109A1 (de)	1984-06-07
JPS59116268A (ja)	1984-07-05
CA1253496A (en)	1989-05-02

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