JPH0574563B2 - - Google Patents
Info
- Publication number
- JPH0574563B2 JPH0574563B2 JP11187584A JP11187584A JPH0574563B2 JP H0574563 B2 JPH0574563 B2 JP H0574563B2 JP 11187584 A JP11187584 A JP 11187584A JP 11187584 A JP11187584 A JP 11187584A JP H0574563 B2 JPH0574563 B2 JP H0574563B2
- Authority
- JP
- Japan
- Prior art keywords
- powder
- particle size
- cosmetics
- powders
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000843 powder Substances 0.000 claims description 51
- 239000002245 particle Substances 0.000 claims description 35
- 239000002537 cosmetic Substances 0.000 claims description 26
- 239000010419 fine particle Substances 0.000 claims description 14
- 239000000203 mixture Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 5
- 238000002156 mixing Methods 0.000 description 4
- 230000001788 irregular Effects 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 238000010835 comparative analysis Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- -1 polyethylene Polymers 0.000 description 2
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- RJDOZRNNYVAULJ-UHFFFAOYSA-L [O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[F-].[F-].[Mg++].[Mg++].[Mg++].[Al+3].[Si+4].[Si+4].[Si+4].[K+] Chemical compound [O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[F-].[F-].[Mg++].[Mg++].[Mg++].[Al+3].[Si+4].[Si+4].[Si+4].[K+] RJDOZRNNYVAULJ-UHFFFAOYSA-L 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 239000000440 bentonite Substances 0.000 description 1
- 229910000278 bentonite Inorganic materials 0.000 description 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000000378 calcium silicate Substances 0.000 description 1
- 229910052918 calcium silicate Inorganic materials 0.000 description 1
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 description 1
- 229960000541 cetyl alcohol Drugs 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229940119170 jojoba wax Drugs 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000019792 magnesium silicate Nutrition 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000004005 microsphere Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Description
本発明は粒子径における均一性の高い不定形板
状または球状の微粒子粉体を配合することを特徴
とするもので、その目的とするところは化粧効果
において、肌への馴染み易さ、マイルドな使用
感、更には優れた密着感により均一性のあるマイ
ルドなつやや透明感のある皮膚感を感じさせ、厚
ぼつたさがなく、自然な仕上り感のある化粧料を
提供せんとするものである。
従来、化粧料に汎用されている粉体としては各
種のものが挙げられるが、その多くは天然鉱物由
来のものであり、その粒子の大きさは一般に不揃
いであつて実際の化粧料に使われているものは、
例えば粒子径で１〜40μ、また平均粒子径では５
〜20μと言う具合に粒子径の幅が広く、また平均
粒子径も比較的大きなものが多用されてきた。し
かしかかる粉体を用いた化粧料は、その含有割合
において、粒子径の大きな粉体が大である時、得
られた化粧料は皮膚への塗布時に弾力感を与える
反面重みや粒子感を感じさせ、またとまりも悪
く、且つ厚ぼつたいものとなる。一方、粒子径の
小さな粉体が大となると、得られた化粧料は皮膚
への塗布時に密着性は向上するものの、きしみを
感じさせすべりが悪化し、また白つぽさが強くな
り粉つぽく不自然な仕上りになるなどの欠点を有
していた。そして、従来の粉体は各種粒子径の幅
広い混合物であるが故に、前記の欠点を克服する
ことは困難であり、望ましい化粧料を得ることが
できなかつた。
そこで本発明者は、前記の欠点を解決し、特に
マイルドな使用感と自然な仕上り感を有する新規
な化粧料を得ようと種々実験研究を重ねた結果、
粒子径における均一性の高い特定形状の微粒子粉
体を配合することにより、この様な欠点がなく、
且つ所望の化粧効果を有する化粧料を見出すに致
つた。
本発明は、不定形板状粉体または球状粉体から
なり、前記粉体の粒子径が１〜10μで且つそのう
ち１〜5μのものの占める割合が50重量％以上で
あり、更に全平均粒子径が2.5〜5μである微粒子
粉体を１種以上配合することを特徴とする化粧料
に関するものである。
本発明に適用される微粒子粉体は不定形板状ま
たは球状の形状を有する粉体であり、無機粉体に
は、例えばタルク、絹雲母、合成雲母、カオリ
ン、ベントナイト等からなる不定形板状粉体、ま
た珪酸マグネシウム、珪酸カルシウム等の複合酸
化物、及び単体ではシリカからなる中空多孔性微
小球体が挙げられる。有機粉体には例えばナイロ
ンパウダー、ポリエチレンパウダー等からなる球
状粉体が挙げられる。
前記これらの粉体は皮膚に対する密着性に特に
優れていると共に、板状または球状という粉体の
形状に由来する流動性、伸びの滑らかさを備えて
いる。
また前記これらの微粒子粉体の粒子径はいづれ
も１〜10μであり、そのうちの50重量％以上を１
〜5μの粒子径のものが占め、また全平均粒子径
は2.5〜5μであり、好ましくは、2.5〜3μのものが
適用される。1μより小さな粒子径では、化粧料
として用いた時に、すべり感が感じられず、白つ
ぽく、粉浮きした化粧仕上りになり、透明感がな
く、皮膚感も感じられなくなる。また10μを越え
ると、使用感でざらつきが目立ち、肌への馴染み
が悪く、密着感に乏しくなり、厚ぼつたさのある
化粧仕上りになり好ましくない。
ここで、粉体の形状を特定すると同時に、粉体
の粒度を特定することが本発明の大きな特徴であ
り、粉体中の50重量％以上が１〜5μと言う狭い
分布の中に収束した、いわゆる粒の揃つた粉体を
用いることにより、前記の各種欠点を解決するば
かりでなく、使用時におけるマイルド感（均一な
当りの柔かさ）及び自然な仕上り感（その効果の
多くは均一な光の散乱に由来）を有する化粧料が
得られる。
そして、前記の各種微粒子粉体より１種以上が
選択され、化粧料に配合されるが、その配合割合
としては、化粧料の剤型に応じて0.5〜95重量％
の範囲で配合される。
尚、本発明においては、前述の微粒子粉体以外
の化粧品用原料、例えば通常の粒子径を有する粉
体や顔料類、スクワラン、ホホバ油、セタノール
等に代表される各種油分、界面活性剤、保湿剤、
香料などが製品目的に応じて適宜選択され、本発
明の効果を損なわない範囲で使用し得るものであ
る。
また、本発明に適用される化粧料剤型としては
幅広いものが挙げられ、粉体を中心に構成される
フエイスパウダーやプレストパウダーの如き粉末
化粧料、フアンデーシヨンの如き油性化粧料、更
にはクリームの如き乳化型化粧料などが例示され
る。
評価試験 １
本発明者は本発明に適用される特定形状及び特
定粒度をもつ微粒子粉体が化粧料に最適であるこ
とを確認するため、薄板状、球状、その他の形状
（多角結晶形、不定形、紡錘形等についてそれぞ
れ行つたがいずれも同様の結果であつた。）の各
形状の粉体に対し、それぞれ１〜10μ（平均粒径
3μ）、1μ未満、10μ超の粒径を有する粉体におい
て皮膚へ塗布し装用感のテストを実施し、比較評
価を行なつた。その結果を表−１に示す。
The present invention is characterized by blending irregularly shaped plate-like or spherical fine particle powder with high uniformity in particle size. The aim is to provide a cosmetic that gives a uniform, mild luster and translucent skin feel through use and excellent adhesion, and has a natural finish without leaving any thick spots. . Conventionally, there are various powders commonly used in cosmetics, but most of them are derived from natural minerals, and their particle sizes are generally irregular, making them difficult to use in actual cosmetics. What you have is
For example, the particle size is 1 to 40μ, and the average particle size is 5μ.
Particles with a wide range of particle diameters, such as ~20μ, and with a relatively large average particle diameter, have been frequently used. However, when cosmetics using such powders contain a large amount of powder with large particle diameters, the resulting cosmetics give a feeling of elasticity when applied to the skin, but feel heavy and grainy. It also has poor consistency and is thick. On the other hand, if the powder with a small particle size becomes large, the adhesion of the obtained cosmetic will improve when applied to the skin, but it will feel squeaky and slippery, and it will also become more whitish and powdery. It had drawbacks such as an unnatural finish. Since conventional powders are a mixture of a wide range of particle sizes, it has been difficult to overcome the above-mentioned drawbacks, and it has been impossible to obtain desirable cosmetics. Therefore, the inventor of the present invention has carried out various experimental studies in an attempt to solve the above-mentioned drawbacks and to obtain a new cosmetic that has a particularly mild feeling of use and a natural finish.
By blending fine particle powder with a specific shape with high uniformity in particle size, this drawback is eliminated.
In addition, we have found a cosmetic that has the desired cosmetic effect. The present invention is composed of an irregularly shaped plate-like powder or a spherical powder, and the powder has a particle size of 1 to 10μ, of which the ratio of 1 to 5μ is 50% by weight or more, and furthermore, the total average particle size is The present invention relates to a cosmetic composition characterized by containing one or more types of fine particle powder having a particle diameter of 2.5 to 5μ. The fine particle powder applied to the present invention is a powder having an irregular plate-like or spherical shape, and examples of inorganic powder include irregularly-shaped plate-like powders made of talc, sericite, synthetic mica, kaolin, bentonite, etc. Examples include powder, composite oxides such as magnesium silicate and calcium silicate, and hollow porous microspheres made of silica alone. Examples of the organic powder include spherical powder made of nylon powder, polyethylene powder, and the like. These powders have particularly excellent adhesion to the skin, and also have fluidity and smoothness of spread due to the shape of the powder, which is plate-like or spherical. In addition, the particle diameters of these fine particle powders are all 1 to 10μ, and 50% by weight or more of them are 1 to 10μ.
Particles with a particle size of ~5μ dominate, and the total average particle size is 2.5 to 5μ, preferably 2.5 to 3μ. If the particle size is smaller than 1μ, when used as a cosmetic, it will not feel slippery, and the makeup will have a white, powdery finish, lack transparency, and lose its skin feel. Moreover, if it exceeds 10μ, the roughness will be noticeable when used, it will not blend well with the skin, it will have poor adhesion, and the makeup will have a thick and flaky finish, which is undesirable. Here, a major feature of the present invention is to specify the particle size of the powder at the same time as specifying the shape of the powder. By using powder with so-called uniform grains, it not only solves the various drawbacks mentioned above, but also provides a mild feel (uniform softness to the touch) and a natural finish (many of its effects are due to the uniform softness of the touch). (originating from light scattering) can be obtained. Then, one or more types of fine particle powders are selected from the various types of fine particle powders mentioned above and blended into cosmetics, with a blending ratio of 0.5 to 95% by weight depending on the dosage form of the cosmetic.
It is blended within the range of. In addition, in the present invention, cosmetic raw materials other than the above-mentioned fine particle powders, such as powders and pigments having normal particle diameters, various oils represented by squalane, jojoba oil, cetanol, etc., surfactants, and moisturizers are used. agent,
Flavors and the like can be appropriately selected depending on the purpose of the product and can be used within a range that does not impair the effects of the present invention. In addition, there are a wide range of cosmetic formulations that can be applied to the present invention, including powder cosmetics such as face powder and pressed powder that are mainly composed of powder, oil-based cosmetics such as foundation, and even Examples include emulsified cosmetics such as creams. Evaluation Test 1 In order to confirm that the fine particle powder having a specific shape and specific particle size applied to the present invention is optimal for cosmetics, the present inventor has tested powders of thin plate shape, spherical shape, and other shapes (polygonal crystal shape, irregular shape, etc.). The results were the same for both regular and spindle-shaped powders.
3μ), less than 1μ, and more than 10μ in particle size were applied to the skin and tested for wearability, and a comparative evaluation was performed. The results are shown in Table-1.
【表】【table】
【表】
表−１の結果から明らかな様に薄板状または球
状をしている粉体はその形状に由来して伸びがよ
く、ざらつきや、厚ぼつたさを感じさせない。ま
た粒径が１〜10μである時に伸び、自然な仕上が
り感、皮膚感等全てにわたつて優れた化粧効果を
与える。
評価試験 ２
次に本発明者は、得られた本発明化粧料の効果
を確認する為、後記実施例１乃至４に示した各種
タイプの化粧料とこれに対応する市販品（粉体の
種類は各実施例と同様のものを用いているが、粒
度が幅広く、平均粒径が本発明の範囲よりより大
きいもの。）及び比較品（各実施例の微粒子粉体
を軽質炭酸カルシウムに置換したもの。但し、粒
度、平均粒径は引用例１に記載のものと同等であ
る。）とを用いて、100名の女性による３ケ月間の
長期連用テストを実施し、比較評価を行なつた。
その結果を表−２に示す。[Table] As is clear from the results in Table 1, powders that are plate-like or spherical have good spreadability due to their shape, and do not feel rough or thick. In addition, when the particle size is 1 to 10μ, it spreads and provides an excellent cosmetic effect over all aspects including a natural finish and skin feel. Evaluation Test 2 Next, in order to confirm the effects of the obtained cosmetics of the present invention, the inventors tested various types of cosmetics shown in Examples 1 to 4 below and the corresponding commercial products (types of powder). The same products as in each example were used, but the particle size was wide and the average particle size was larger than the range of the present invention.) and a comparative product (in which the fine particle powder of each example was replaced with light calcium carbonate). (However, the particle size and average particle diameter are the same as those described in Cited Example 1.) A long-term continuous use test for 3 months was conducted by 100 women and a comparative evaluation was conducted. .
The results are shown in Table-2.
【表】【table】
【表】
表−２の結果からも明らかな様に、本発明の微
粒子粉体を配合した化粧料は、市販品や比較品と
比較しても、粉体形状及び微粒子による密着感、
厚ぼつたさがない、肌への馴染み等が向上するば
かりでなく、その粒子径の均一性が高いことによ
るマイルドな使用感、自然な仕上がり感の評価が
格段に高い優れたものとなつている。
以上述べたように本願発明により特定形状及び
特定粒度を有する微粒子粉体を選択することで、
肌への馴染み易さ、マイルドな使用感、更には優
れた密着感により均一性のあるマイルドなつやや
透明感のある皮膚感を感じさせ、厚ぼつたさがな
く、自然な仕上がり感のある化粧料を入手するこ
とができる。
次に本発明化粧料の実施例を示す。配合割合は
重量部である。尚、実施例表示中、平均粒子径は
粉体中の主成分粒子径、含有率は全粉体中におい
て１〜5μの粒子径を有する粉体の含有率を表わ
すものである。
実施例１フエイスパウダー[Table] As is clear from the results in Table 2, the cosmetics containing the fine particle powder of the present invention have better powder shape and adhesion due to the fine particles than commercially available products and comparative products.
Not only does it not feel thick or sticky and blends well into the skin, it also has a highly uniform particle size that gives it a mild feel on use and a natural finish that has been highly rated. There is. As described above, by selecting fine particle powder having a specific shape and particle size according to the present invention,
Makeup that blends easily into the skin, has a mild feeling of use, and has excellent adhesion, giving the skin a uniform, mild luster and translucence, and a natural finish without leaving any thick spots. fees can be obtained. Next, examples of the cosmetics of the present invention will be shown. The blending ratio is in parts by weight. In the Examples, the average particle size refers to the particle size of the main component in the powder, and the content refers to the content of powder having a particle size of 1 to 5 μm in the total powder. Example 1 Face powder
【表】
（方法）
Ａをナウターミキサーで20分間混合した後、粉
砕機で粉砕混合する。次いで、粉砕混合物をヘン
シエルミキサーに移し、常温にて、高速回転で攪
拌しながらＢを注入して５分間攪拌し、更にＣを
注入し３分間攪拌混合後、取り出し、ブロワーシ
フターを通し容器に充填して製品とする。
実施例２乳化型フアンデーシヨン[Table] (Method) Mix A with a Nauta mixer for 20 minutes, then grind and mix with a pulverizer. Next, the pulverized mixture was transferred to a Henschel mixer, and while stirring at high speed at room temperature, B was injected and stirred for 5 minutes. C was further injected and mixed for 3 minutes, then taken out and passed through a blower sifter into a container. Fill it and make it into a product. Example 2 Emulsified foundation
【表】
Ｂ〓
[Table] B〓
Claims (1)
記粉体の粒子径が１〜10μで且つそのうち１〜5μ
のものの占める割合が50重量％以上であり、更に
全平均粒子径が2.5〜5μである微粒子粉体を一種
以上配合することを特徴とする化粧料。1 Consisting of irregularly shaped plate-like powder or spherical powder, the particle size of the powder is 1 to 10μ, and among them, 1 to 5μ
1. A cosmetic comprising at least 50% by weight of fine particles and at least one type of fine powder having a total average particle diameter of 2.5 to 5 μm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11187584A JPS60255710A (en) | 1984-05-31 | 1984-05-31 | Cosmetic |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11187584A JPS60255710A (en) | 1984-05-31 | 1984-05-31 | Cosmetic |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60255710A JPS60255710A (en) | 1985-12-17 |
| JPH0574563B2 true JPH0574563B2 (en) | 1993-10-18 |
Family
ID=14572343
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11187584A Granted JPS60255710A (en) | 1984-05-31 | 1984-05-31 | Cosmetic |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60255710A (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5766577A (en) * | 1992-09-10 | 1998-06-16 | Elizabeth Arden Co., Division Of Conopco, Inc. | Color cosmetic composition |
| JP3505677B2 (en) * | 1999-07-12 | 2004-03-08 | 独立行政法人農業生物資源研究所 | Cosmetics containing ultrafine crystalline silk powder |
| JP5823931B2 (en) * | 2012-07-23 | 2015-11-25 | 日本メナード化粧品株式会社 | Oily liquid sunscreen agent |
-
1984
- 1984-05-31 JP JP11187584A patent/JPS60255710A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS60255710A (en) | 1985-12-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |