JPH0626519B2 - Calcium enhancer - Google Patents
Calcium enhancerInfo
- Publication number
- JPH0626519B2 JPH0626519B2 JP1218305A JP21830589A JPH0626519B2 JP H0626519 B2 JPH0626519 B2 JP H0626519B2 JP 1218305 A JP1218305 A JP 1218305A JP 21830589 A JP21830589 A JP 21830589A JP H0626519 B2 JPH0626519 B2 JP H0626519B2
- Authority
- JP
- Japan
- Prior art keywords
- calcium
- organic acid
- calcium carbonate
- added
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Cereal-Derived Products (AREA)
- General Preparation And Processing Of Foods (AREA)
- Jellies, Jams, And Syrups (AREA)
Description
【発明の詳細な説明】 〔産業上の利用分野〕 本発明は食品添加用のカルシウム強化剤に関する。詳し
くは、穀類、パン類、麺類、菓子類などの食品へ添加し
てカルシウム分を強化させ、しかも酸臭、カルシウム由
来の褐変、黄変などを生じさせ難いカルシウム強化剤に
関する。DETAILED DESCRIPTION OF THE INVENTION [Industrial field of use] The present invention relates to a calcium fortifier for food additives. More specifically, the present invention relates to a calcium enhancer that is added to foods such as grains, breads, noodles, and confectioneries to enhance the calcium content, and is unlikely to cause acid odor, browning and yellowing due to calcium.
近年、日本人の食生活の変化により、カルシウム分の摂
取量不足が問題視されており、これを補うためのカルシ
ウム強化剤が種々販売されている。In recent years, due to changes in Japanese dietary habits, a shortage of calcium has been regarded as a problem, and various calcium enhancers for supplementing this have been sold.
しかしながら、これらの市販品は、いずれも水溶性カル
シウム塩や非水溶性カルシウム塩の粉末または、顆粒、
ないしこれらの混合物であるため、カルシウム強化剤と
して食品へ添加した場合には、次のような欠点を生ずる
ことが多い。However, these commercial products are all powders or granules of water-soluble calcium salt or water-insoluble calcium salt,
Since it is a mixture of these, when added to foods as a calcium enhancer, the following drawbacks often occur.
すなわち、水溶性カルシウム塩、例えば燐酸カルシウム
として使用する場合には、食品への分散は容易である
が、塩の解離に際して苦みなどを生じがちである。又、
この欠点をカバーするために有機酸塩、例えばクエン酸
カルシウムとして使用すると、苦みなどの点は緩和され
るものの、食品に酸臭などが残りやすく、いずれにして
も使用し難いものである。That is, when used as a water-soluble calcium salt such as calcium phosphate, it is easy to disperse it in foods, but bitterness tends to occur when the salt dissociates. or,
When an organic acid salt such as calcium citrate is used to cover this drawback, bitterness and the like are alleviated, but acid odors and the like tend to remain in foods, which makes it difficult to use in any case.
また、非水溶性カルシウム塩、例えば、入手が容易な炭
酸カルシウムの場合は、舌にざらつきを感じないよう粉
末化して使用するため、添加に際しては空気を抱きこみ
分散し難く、凝集し、いわゆる、ダマ状になりやすい。
しかも、添加した食品を褐変ないし黄変させやすく、い
ずれにしても実用上の難点の多いものである。Further, a water-insoluble calcium salt, for example, in the case of calcium carbonate that is easily available, since it is used by being powdered so that the tongue does not feel rough, it is difficult to embrace air when adding, it aggregates, so-called, It tends to be lumpy.
Moreover, the added foods are easily browned or yellowed, and in any case, there are many practical difficulties.
以上の諸点に鑑み、本発明者は、種々検討した結果、有
機酸カルシウム溶液中に炭酸カルシウム粉末を分散させ
た場合、前記課題を解決しうることを見出し、本発明を
完成させるに至った。In view of the above points, as a result of various studies, the present inventor has found that the problem can be solved when calcium carbonate powder is dispersed in an organic calcium salt solution, and has completed the present invention.
したがって、本発明は、有機酸カルウム溶液中に炭酸カ
ルシウム粉末を分散させてなるカルシウム強化剤であ
り、また、有機酸に炭酸カルシウム粉末を有機酸との反
応量以上に添加してあり、かつ未反応の炭酸カルシウム
粉末を分散させてあるカルシウム強化剤である。Therefore, the present invention is a calcium enhancer obtained by dispersing calcium carbonate powder in a solution of calcium organic acid, and the calcium carbonate powder is added to the organic acid in an amount not less than the reaction amount with the organic acid, and It is a calcium fortifier in which reactive calcium carbonate powder is dispersed.
本発明に於いて、有機酸カルシウム溶液とは、例えば有
機酸にカルシウム化合物を添加し溶解させて得られる、
有機酸とカルシウムが解離状態にある溶液をいう。In the present invention, the organic acid calcium solution is obtained, for example, by adding and dissolving a calcium compound in an organic acid,
A solution in which organic acid and calcium are in a dissociated state.
カルシウム化合物とは、食品に添加して問題の生じない
ものであればその種類は問わない。容易に入手し得るも
のとしては、炭酸カルシウムがあげられ、これには合成
品のほか、天然由来のものとして、卵殻、貝殻又はその
精製物などがあげられる。尚、後の工程に鑑み、炭酸カ
ルシウムの粉末を使用することが特に好ましい。The calcium compound may be of any type as long as it does not cause a problem when added to food. Examples of easily obtainable products include calcium carbonate, which includes synthetic products, and naturally-derived products such as egg shells, shells and purified products thereof. In view of the subsequent steps, it is particularly preferable to use calcium carbonate powder.
また、有機酸は、食品に添加して問題のない、カルシウ
ム溶解力の高いものを使用するのが好ましく、特に易水
溶性カルシウム塩を作り得るものが好適である。好まし
い有機酸としては、例えば酢酸、クエン酸、乳酸などが
あげられる。As the organic acid, it is preferable to use an organic acid having a high calcium-dissolving power, which does not cause any problem when added to foods, and particularly preferably an acid capable of forming a readily water-soluble calcium salt. Preferable organic acids include acetic acid, citric acid, lactic acid and the like.
さらに、有機酸カルシウム溶液中に分散させる炭酸カル
シウム粉末とは、上記の炭酸カルシウムを粉末状にした
もので、粉末の大きさは、舌にざらつきを感じ難くさせ
る意味で４００メッシュ以下が好ましい。Further, the calcium carbonate powder to be dispersed in the organic acid calcium solution is a powder of the above calcium carbonate, and the size of the powder is preferably 400 mesh or less in order to make the tongue less likely to be rough.
有機酸カルシウム溶液中の有機カルシウムの濃度（固形
分濃度）は有機酸の種類によって多少異なるけれども、
一般的に炭酸カルシウム粉末も含めた全重量中で５〜２
０％程度が好ましい。この割合があまり低いと、炭酸カ
ルシウム粉末に起因する変色（褐変など）が防ぎ難くな
り、また、あまり高いと、酸臭が出やすくなるからであ
る。また、有機酸カルシウム溶液中に分散させる炭酸カ
ルシウム粉末の割合は、一般的に、全重量中で５〜２０
％程度が好ましい。この割合があまり低いと酸臭緩和効
果が期し難く、また、あまり高いと褐変などの変色が生
じやすくなり、また粘度が高くなり、取扱が不便になる
からである。Although the concentration of organic calcium (concentration of solid content) in the organic acid calcium solution varies slightly depending on the type of organic acid,
Generally 5 to 2 in total weight including calcium carbonate powder
About 0% is preferable. This is because if this ratio is too low, it becomes difficult to prevent discoloration (browning, etc.) due to the calcium carbonate powder, and if it is too high, an acid odor is likely to occur. The proportion of calcium carbonate powder dispersed in the organic acid calcium solution is generally 5 to 20 in the total weight.
% Is preferable. This is because if the proportion is too low, the acid odor mitigating effect is difficult to achieve, and if it is too high, discoloration such as browning is likely to occur, and the viscosity becomes high, which makes handling inconvenient.
尚、前記の有機酸カルシウム（固形分）と、炭酸カルシ
ウム粉末との比率は、前者１部に対し後者１〜６部程度
の間にあることが好ましい。The ratio of the organic calcium salt (solid content) to the calcium carbonate powder is preferably between 1 part of the former and 1 to 6 parts of the latter.
本発明品を製するには、まず、カルシウム化合物を有機
酸、例えば、酸度１３％以上の高濃度酢酸に十分に溶解
させ、有機酸とカルシウム化合物を完全に反応させた有
機酸カルシウム溶液（有機酸カルシウムの固形分約５〜
２０％）を調整する。In order to manufacture the product of the present invention, first, a calcium compound is sufficiently dissolved in an organic acid, for example, high-concentration acetic acid having an acidity of 13% or more, and the organic acid and the calcium compound are completely reacted (organic acid solution (organic Calcium acid solid content of about 5
20%).
この場合、反応させるカルシウム化合物は粉末状のもの
が好ましいが、そうでなくとも差支えない。また、その
添加量は、有機散との反応を完全に行わしめるために、
反応量以上の量を添加した方が良く、残余のカルシウム
化合物は必要に応じ濾別してもよく、しなくてもよい。In this case, the calcium compound to be reacted is preferably powdery, but it does not matter if it is not. In addition, the amount added is in order to completely carry out the reaction with organic powder,
It is better to add more than the reaction amount, and the residual calcium compound may or may not be filtered out as necessary.
カルシウム化合物が炭酸カルシウムの場合には粉末のも
の（４００メッシュ以下のもの）を反応量以上用いれ
ば、改めて炭酸カルシウム粉末を添加する工程を簡略化
できる。When the calcium compound is calcium carbonate, if a powdery one (400 mesh or less) is used in a reaction amount or more, the step of adding the calcium carbonate powder again can be simplified.
以上のようにして得た有機酸カルシウム溶液に、カルシ
ウム化合物として反応量以上で、必要かつ十分なカルシ
ウム粉末を添加した場合を除き、さらに炭酸カルシウム
粉末（４００メッシュ以下のもの）を全体中の５〜２０
％になるように添加し分散させる。The calcium carbonate powder (400 mesh or less) is further added to the obtained organic acid calcium solution in a total amount of 5 in the whole amount except when necessary and sufficient calcium powder having a reaction amount or more as a calcium compound is added. ~ 20
% To add and disperse.
添加後、十分に分散させるためには、ミキサーなどで脱
気しながら攪拌すればよい。After the addition, in order to sufficiently disperse, stirring may be performed while degassing with a mixer or the like.
この後、水溶性界面活性剤、ガム類、微結晶セルロース
などを、一般的に１〜３％程度添加し、さらに攪拌する
と、均質化されたスラリー状のものを得ることができ、
有機酸カルシウム溶液中に炭酸カルシウムが一段と分散
された状態のカルシウム強化剤が得られる。Thereafter, a water-soluble surfactant, gums, microcrystalline cellulose, etc. are generally added in an amount of about 1 to 3% and further stirred to obtain a homogenized slurry.
A calcium enhancer in which calcium carbonate is further dispersed in an organic acid calcium solution is obtained.
さらに別の製法としては有機酸カルシウム塩を清水に溶
解させ、これに前記と同様の方法で炭酸カルシウム粉末
を添加し分散させれば、容易に同様のカルシウム強化剤
を得ることができる。As another production method, an organic acid calcium salt is dissolved in fresh water, and calcium carbonate powder is added to and dispersed in the same method as described above, whereby a similar calcium enhancer can be easily obtained.
本発明に係るカルシウム強化剤の用法は、カルシウム含
量によって一律ではないが、例えば米飯へ添加する場
合、日本人の１日のカルシウム必要摂取量は600 mgとさ
れているので、１回の食事でカルシウムを100 〜200 mg
程度摂取できるように添加すればよい。The usage of the calcium enhancer according to the present invention is not uniform depending on the calcium content, but when it is added to cooked rice, for example, the daily intake of calcium required by the Japanese is 600 mg, so one meal is enough. 100-200 mg of calcium
It may be added so that it can be ingested to some extent.
尚、原料の一つとして炭酸カルシウムを使用する理由
は、他のカルシウム化合物と比較した際、体内への吸収
率、蓄積率が高いためで、その中でも特に卵殻由来のカ
ルシウムは一段とすぐれている。The reason why calcium carbonate is used as one of the raw materials is that the absorption rate and the accumulation rate in the body are high when compared with other calcium compounds, and among them, calcium derived from eggshells is particularly excellent.
本発明品は、炭酸カルシウムの粉末を乾燥状態でなく、
あらかじめ有機酸カルシウム溶液中に分散させてあるた
め、粉末粒子間に空気を抱きこむことが少なく、従って
従来品に比べ、食品中に容易に分散させることができ
る。The product of the present invention is not a dry powder of calcium carbonate,
Since it is dispersed in the organic acid calcium solution in advance, air is less likely to be trapped between the powder particles, and therefore, it can be easily dispersed in food compared to conventional products.
また、炭酸カルシウムを使用しているにもかかわらず褐
変ないし黄変することがない。これは、有機酸カルシウ
ム溶液を併用しているため、有機酸の陰イオンが、食品
の成分と炭酸カルシウムとが反応するのを何らかの理由
で阻害しているからではないかと推察される。Further, it does not turn brown or yellow even though calcium carbonate is used. It is presumed that this is because the organic acid calcium solution is used in combination, and therefore the anion of the organic acid inhibits the reaction between the components of the food and calcium carbonate for some reason.
さらに食品へ添加した際、有機酸カルシウムを主体とす
る従来のカルシウム強化剤に比べ、炭酸カルシウムを併
用する分だけ有機酸カルシウムの使用割合も一段と少な
いので、食品には酸臭を与え難い。Furthermore, when added to foods, compared to conventional calcium fortifiers that are mainly composed of organic acid calcium, the proportion of organic acid calcium used is much lower due to the combined use of calcium carbonate, so it is difficult to impart acid odor to foods.
以下、本発明の実施例及び試験例を説明する。Hereinafter, examples and test examples of the present invention will be described.
尚、本発明において「％」はすべて「重量％」を、ま
た、「部」は「重量部」を各々示す。In the present invention, "%" means "% by weight", and "part" means "part by weight".
実施例１ 脱気装置付ミキサー内に４００メッシュ以下の卵殻粉末
５０kgと酸度１３％の酢酸９２kgを投入し、これを脱気
しながら緩やかに攪拌し１２時間反応させた。次に、キ
サンタンガム２kg、微結晶セルロース６kg、清水２５０
kg投入して攪拌しスラリー状の製品約４００kg得た。Example 1 50 kg of eggshell powder of 400 mesh or less and 92 kg of acetic acid having an acidity of 13% were put into a mixer equipped with a deaerator, and this was gently agitated and reacted for 12 hours while deaerating. Next, 2 kg of xanthan gum, 6 kg of microcrystalline cellulose, 250 fresh water
About 400 kg of a slurry product was obtained by adding kg and stirring.
実施例２ 脱気装置付ミキサー内にクエン酸カルシウム１２kgと清
水１２０kgとを投入して攪拌し、クエン酸カルシウムを
完全に溶解させた。次に４００メッシュ以下の炭酸カル
シウムを１５kg投入して脱気しながら攪拌した後、グア
ーガム0.7 kg、微結晶セルロース2.3 kgを投入して攪拌
し、スラリー状の製品約１５０kgを得た。Example 2 Calcium citrate (12 kg) and fresh water (120 kg) were placed in a mixer equipped with a deaerator and stirred to completely dissolve calcium citrate. Next, 15 kg of calcium carbonate of 400 mesh or less was added and stirred while being deaerated, then 0.7 kg of guar gum and 2.3 kg of microcrystalline cellulose were added and stirred to obtain about 150 kg of a slurry product.
実施例３ 脱気装置付ミキサー内に乳酸カルシウム２０kgと清水１
６０kgを投入して撹拌し、乳酸カルシウムを完全に溶解
させた。次に、４００メッシュ以下の炭酸カルシウム１
６kgを投入して脱気しながら撹拌した後、キサンタンガ
ム１kg、微結晶セルロース３kgを投入して撹拌し、スラ
リー状の製品約２００kgを得た。Example 3 20 kg of calcium lactate and 1 fresh water in a mixer with a deaerator
60 kg was added and stirred to completely dissolve calcium lactate. Next, calcium carbonate 1 of 400 mesh or less
After adding 6 kg and stirring while deaerating, 1 kg of xanthan gum and 3 kg of microcrystalline cellulose were added and stirred to obtain about 200 kg of a slurry product.
試験例１ 炊飯器に洗米した米１kgと清水1.2 kgを入れ、これに実
施例１で得た本発明品３０ml（炊飯米１５０ｇ当りカル
シウム約１１０mgに相当する。）を添加し、軽く攪拌し
た後に炊飯した米飯と、市販のカルシウム強化剤（固形
顆粒状）をカルシウム摂取量が同量になるように添加
し、同様に攪拌して炊飯した米飯について、それぞれ酸
臭、米の変色具合、及び呈味の状況を調べた結果を表−
１に示す。Test Example 1 1 kg of washed rice and 1.2 kg of fresh water were placed in a rice cooker, 30 ml of the product of the present invention obtained in Example 1 (corresponding to about 110 mg of calcium per 150 g of cooked rice) was added, and after light stirring, Cooked cooked rice and commercially available calcium enhancer (solid granules) were added so that the calcium intake would be the same, and the cooked cooked rice was stirred and cooked in the same manner. Table showing the results of examining the taste situation
Shown in 1.
尚、市販品Ａは炭酸カルシウムを主成分とするもの、市
販品Ｂはクエン酸カルシウムを主成分とするものであ
る。The commercially available product A is mainly composed of calcium carbonate, and the commercially available product B is mainly composed of calcium citrate.
対照品としてはカルシウム強化剤を添加しないで同様に
垂範した米飯を用いた。As a control product, cooked rice which was similarly used without the addition of the calcium enhancer was used.
表中の記号のうち、酸臭の○は臭いのないこと、△はわ
ずかに感じるもの、×はだれもが感じるものを示す。 Among the symbols in the table, ○ of acid odor indicates that there is no odor, Δ indicates that it is slightly felt, and × indicates that it is felt by everyone.
変色の○は変化のないもの、×は明らかに変色している
ものを示す。The discolored circle indicates that there is no change, and the cross indicates that the color is clearly discolored.
味の◎は優れているもの、○は普通であること、△はや
や劣ることを示す。The taste ⊚ indicates that the taste is excellent, ◯ indicates that the taste is normal, and Δ indicates that the taste is a little poor.
試験例２ 試験例１の本発明品と市販品Ａについて、試験例１と同
様に炊飯した後、攪拌することなしに１０等分し、各ブ
ロックに含まれているカルシウム濃度を原子吸光法にて
測定し、カルシウムの分散状態を確認した結果を表−２
に示す。Test Example 2 With respect to the product of the present invention and the commercial product A of Test Example 1, after cooking rice in the same manner as in Test Example 1, the mixture was divided into 10 equal parts without stirring, and the calcium concentration contained in each block was measured by an atomic absorption method. Table 2 shows the results of measuring the calcium dispersion and confirming the calcium dispersion state.
Shown in.
以上のように、本発明品は軽く攪拌しただけでほぼ均一
に分散していることが判る。 As described above, it can be seen that the product of the present invention is dispersed almost uniformly only by light stirring.
以上のように、本発明に係るカルシウム強化剤は、食品
に添加した場合、酸臭が感じにくいばかりでなく、容易
に、かつほぼ均一に分散する。また、有機酸を使用して
いるにもかかわらず、食品に添加した際の酸臭などを感
じ難いばかりでなく、炭酸カルシウムによる褐変ないし
黄変を抑制する。As described above, when the calcium fortifier according to the present invention is added to food, not only is it difficult to feel the acid odor, but also the calcium enhancer is easily and almost uniformly dispersed. Further, in spite of using the organic acid, not only is it difficult to feel acid odor when added to foods, but also browning or yellowing due to calcium carbonate is suppressed.
従って、種々の食品に添加しても摂食時に何ら違和感を
感じさせ難いのでカルシウム強化剤として最適である。Therefore, even if it is added to various foods, it does not cause any uncomfortable feeling when ingested, and it is most suitable as a calcium enhancer.
Claims (4)
粉末を分散させてなるカルシウム強化剤1. A calcium strengthening agent comprising calcium carbonate powder dispersed in an organic acid calcium solution.
の反応量以上に添加してあり、かつ未反応の炭酸カルシ
ウム粉末を分散させてあるカルシウム強化剤2. A calcium toughening agent in which calcium carbonate powder is added to an organic acid in an amount not less than the reaction amount with the organic acid, and unreacted calcium carbonate powder is dispersed.
のカルシウム強化剤3. The calcium enhancer according to claim 1, wherein the organic acid is acetic acid.
は(2)記載のカルシウム強化剤4. The calcium enhancer according to claim 1 or 2, wherein the calcium carbonate is eggshell.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1218305A JPH0626519B2 (en) | 1989-08-24 | 1989-08-24 | Calcium enhancer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1218305A JPH0626519B2 (en) | 1989-08-24 | 1989-08-24 | Calcium enhancer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0380054A JPH0380054A (en) | 1991-04-04 |
| JPH0626519B2 true JPH0626519B2 (en) | 1994-04-13 |
Family
ID=16717760
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1218305A Expired - Lifetime JPH0626519B2 (en) | 1989-08-24 | 1989-08-24 | Calcium enhancer |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH0626519B2 (en) |
Cited By (1)
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| WO2023089771A1 (en) * | 2021-11-19 | 2023-05-25 | 日本たばこ産業株式会社 | Method for analyzing nicotine distribution in nicotine-containing composition |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06319487A (en) * | 1993-05-10 | 1994-11-22 | Morio Tokoro | Liquid calcium and its production |
| US6232351B1 (en) * | 1998-05-22 | 2001-05-15 | Amway Corporation | Co-processed botanical plant composition |
| JP3339427B2 (en) * | 1998-10-30 | 2002-10-28 | 小川香料株式会社 | Water-insoluble edible composition and solid food containing the composition |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5739617B2 (en) * | 1975-01-20 | 1982-08-23 | ||
| JPS55122718A (en) * | 1979-03-01 | 1980-09-20 | Michinoku Kaihatsu:Kk | Preparation of health drink |
| JPS5840041A (en) * | 1981-09-02 | 1983-03-08 | Rokko Bataa Kk | Preparation of calcium-enriched process cheese |
| US4722847A (en) * | 1986-05-07 | 1988-02-02 | The Procter & Gamble Company | Fruit juice beverages and juice concentrates nutritionally supplemented with calcium |
| JPS63173556A (en) * | 1987-01-14 | 1988-07-18 | Snow Brand Milk Prod Co Ltd | Production of calcium carbonate complex having excellent dispersibility |
| JPS63240747A (en) * | 1987-03-30 | 1988-10-06 | Kanegafuchi Chem Ind Co Ltd | Production of filling materials |
-
1989
- 1989-08-24 JP JP1218305A patent/JPH0626519B2/en not_active Expired - Lifetime
Non-Patent Citations (1)
| Title |
|---|
| 岡村一弘著「食品添加物の使用法」全面改訂第６版（昭和５５年１０月３１日発行）食品と科学社Ｐ．１８７−１９３ |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023089771A1 (en) * | 2021-11-19 | 2023-05-25 | 日本たばこ産業株式会社 | Method for analyzing nicotine distribution in nicotine-containing composition |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0380054A (en) | 1991-04-04 |
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