JPH0830074B2 - ２，３，６，３´，４´―ペンタ―ｏ―アセチルスクロースの製造法 - Google Patents

２，３，６，３´，４´―ペンタ―ｏ―アセチルスクロースの製造法

Info

Publication number
JPH0830074B2
JPH0830074B2 JP61247656A JP24765686A JPH0830074B2 JP H0830074 B2 JPH0830074 B2 JP H0830074B2 JP 61247656 A JP61247656 A JP 61247656A JP 24765686 A JP24765686 A JP 24765686A JP H0830074 B2 JPH0830074 B2 JP H0830074B2
Authority
JP
Japan
Prior art keywords
added
penta
acetylsucrose
solution
hours
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP61247656A
Other languages
English (en)
Japanese (ja)
Other versions
JPS62155289A (ja
Inventor
ウイリアム・タリイ
ニコラス・エム・バーノン
ピーター・エイ・ウオルシユ
Original Assignee
マクニ−ラブ・インコ−ポレ−テツド
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by マクニ−ラブ・インコ−ポレ−テツド filed Critical マクニ−ラブ・インコ−ポレ−テツド
Publication of JPS62155289A publication Critical patent/JPS62155289A/ja
Publication of JPH0830074B2 publication Critical patent/JPH0830074B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Saccharide Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP61247656A 1985-10-21 1986-10-20 ２，３，６，３´，４´―ペンタ―ｏ―アセチルスクロースの製造法 Expired - Lifetime JPH0830074B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB858525953A GB8525953D0 (en) 1985-10-21 1985-10-21 Preparation of galactopyranoside
GB8525953 1985-10-21

Publications (2)

Publication Number Publication Date
JPS62155289A JPS62155289A (ja) 1987-07-10
JPH0830074B2 true JPH0830074B2 (ja) 1996-03-27

Family

ID=10587018

Family Applications (1)

Application Number Title Priority Date Filing Date
JP61247656A Expired - Lifetime JPH0830074B2 (ja) 1985-10-21 1986-10-20 ２，３，６，３´，４´―ペンタ―ｏ―アセチルスクロースの製造法

Country Status (20)

Country Link
US (1) US4801700A (de)
EP (1) EP0220907B1 (de)
JP (1) JPH0830074B2 (de)
KR (1) KR940000484B1 (de)
AT (1) ATE84791T1 (de)
AU (1) AU593293B2 (de)
CA (1) CA1273918A (de)
DE (1) DE3687564T2 (de)
DK (1) DK503286A (de)
ES (1) ES2044837T3 (de)
FI (1) FI83783C (de)
GB (2) GB8525953D0 (de)
IE (1) IE59559B1 (de)
IL (1) IL80371A (de)
MX (1) MX168351B (de)
NO (1) NO167033C (de)
NZ (1) NZ218010A (de)
PT (1) PT83581B (de)
RU (1) RU1771476C (de)
ZA (1) ZA867949B (de)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0067535B1 (de) * 1981-05-22 1985-01-30 TATE & LYLE PUBLIC LIMITED COMPANY Brom substituierte Derivate von Sucrose
GB8525954D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Chlorination of carbohydrates &c alcohols
GB8622342D0 (en) * 1986-09-17 1986-10-22 Tate & Lyle Plc Process
US4986991A (en) * 1987-05-15 1991-01-22 Wm Wrigley, Jr., Company Chewing gum having an extended sweetness
US5136031A (en) * 1990-07-09 1992-08-04 Tate & Lyle Public Limited Company Chlorination of sugars
US5122601A (en) * 1990-12-07 1992-06-16 Hawaiian Sugar Planters'association Synthesis of 2,3,3',4,4'-penta-o-methylsucrose
NZ240818A (en) 1990-12-14 1993-08-26 Mcneil Ppc Inc Liquid sucralose concentrate compositions containing preservative, buffer and liquid
EP1280753A1 (de) * 2000-04-21 2003-02-05 Rhodia/Chirex, Inc. Verfahren zur herstellung von r-1-(aryloxy)propan-2-ol
KR100854528B1 (ko) 2000-11-17 2008-08-26 테이트 앤드 라일 퍼블릭 리미티드 컴파니 개선된 수크랄로즈 조성물 및 이의 제조방법
AU3955002A (en) 2000-11-17 2002-06-03 Mcneil Ppc Inc Meltable form of sucralose
US6943248B2 (en) * 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
CN1176094C (zh) * 2003-05-23 2004-11-17 广东省食品工业研究所 一种三氯蔗糖的合成方法
WO2006061855A2 (en) * 2004-12-10 2006-06-15 Pharmed Medicare Private Limited Salts assisted selective extraction of 6-acetyl-4.1', 6' trichlorogalactosucrose and 4, 1 ', 6' trichlorogalactosucrose from aqueous reaction mixture
US7750146B2 (en) 2005-03-18 2010-07-06 Tate & Lyle Plc Granular sucralose
US20060247180A1 (en) * 2005-04-29 2006-11-02 Bergey James L Purgative composition and uses thereof
WO2006127605A2 (en) * 2005-05-23 2006-11-30 Cadbury Adams Usa Llc Confectionery composition including an elastomeric component, a cooked saccharide component, and a sweetener
US20100184969A1 (en) * 2005-11-08 2010-07-22 Mangesh Rajadhyaksha Process to Prepare Sucralose
US7741477B2 (en) * 2006-01-10 2010-06-22 Alembic Limited Process for purification of sucralose
WO2007096726A2 (en) * 2006-02-20 2007-08-30 Emcure Pharmaceuticals Limited Process for the preparation of a glucose derivative
CN100418976C (zh) * 2006-04-03 2008-09-17 广州科宏食品添加物有限公司 一种三氯蔗糖的制备方法
WO2008004246A1 (en) * 2006-07-06 2008-01-10 Alembic Limited An improved process for the preparation of sucralose of high purity
US20080166449A1 (en) * 2006-11-29 2008-07-10 Cadbury Adams Usa Llc Confectionery compositions including an elastomeric component and a saccharide component
AU2007328222A1 (en) * 2006-12-05 2008-06-12 Tate & Lyle Technology Ltd. Trityl chloride recovery
CN101012253B (zh) * 2007-02-06 2010-04-14 启东东岳药业有限公司 6-pas的制备方法
CN101245085B (zh) 2007-12-19 2012-02-01 上海同辰生物科技有限公司 一种三氯蔗糖的合成及纯化工艺
CN101759728B (zh) * 2010-01-08 2012-01-11 江苏巨邦制药有限公司 三氯蔗糖的生产及精制方法
CN102690299B (zh) * 2012-05-25 2015-04-08 浙江海森药业有限公司 一种串联反应制备三氯蔗糖-6-乙酸酯的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1492791A (en) * 1974-03-05 1977-11-23 Tate & Lyle Ltd Sucrose derivatives
US4435440A (en) * 1976-01-08 1984-03-06 Tate & Lyle Limited Sweeteners
DE3065399D1 (en) * 1979-12-18 1983-11-24 Tate & Lyle Plc Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3062467D1 (en) * 1979-12-20 1983-04-28 Tate & Lyle Plc Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3165986D1 (en) * 1980-07-08 1984-10-18 Tate & Lyle Plc Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs)
US4692514A (en) * 1985-12-20 1987-09-08 Uop Inc. Process for separating ketoses from alkaline- or pyridine-catalyzed isomerization products
JPS61247655A (ja) * 1985-04-24 1986-11-04 トヨタ自動車株式会社 高強度セラミツクス
GB8525954D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Chlorination of carbohydrates &c alcohols

Also Published As

Publication number Publication date
ES2044837T3 (es) 1994-01-16
DE3687564T2 (de) 1993-07-15
FI83783B (fi) 1991-05-15
KR870003718A (ko) 1987-05-04
US4801700A (en) 1989-01-31
NO864190D0 (no) 1986-10-20
EP0220907B1 (de) 1993-01-20
FI864237L (fi) 1987-04-22
IE59559B1 (en) 1994-03-09
ATE84791T1 (de) 1993-02-15
JPS62155289A (ja) 1987-07-10
AU6421486A (en) 1987-04-30
GB8625107D0 (en) 1986-11-26
FI864237A0 (fi) 1986-10-20
FI83783C (fi) 1991-08-26
MX168351B (es) 1993-05-19
GB2182038B (en) 1989-09-20
RU1771476C (ru) 1992-10-23
NO167033C (no) 1991-09-25
GB8525953D0 (en) 1985-11-27
DK503286A (da) 1987-04-22
CA1273918A (en) 1990-09-11
EP0220907A2 (de) 1987-05-06
NO864190L (no) 1987-04-22
IE862763L (en) 1987-04-21
NO167033B (no) 1991-06-17
IL80371A (en) 1990-12-23
KR940000484B1 (ko) 1994-01-21
DK503286D0 (da) 1986-10-20
PT83581A (en) 1986-11-01
PT83581B (pt) 1989-05-31
AU593293B2 (en) 1990-02-08
NZ218010A (en) 1988-11-29
DE3687564D1 (de) 1993-03-04
IL80371A0 (en) 1987-01-30
EP0220907A3 (en) 1988-12-07
ZA867949B (en) 1988-05-25
GB2182038A (en) 1987-05-07

Similar Documents

Publication Publication Date Title
JPH0830074B2 (ja) ２，３，６，３´，４´―ペンタ―ｏ―アセチルスクロースの製造法
EP0223421B1 (de) Chlorination von Carbohydraten und anderen Alkoholen
EP0031651B1 (de) Verfahren zur Herstellung von 4,1',6'-Trichlor-4,1',6'-trideoxy-galactosucrose
AU594502B2 (en) Sucrose derivatives
US4380476A (en) Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxygalactosucrose (TGS)
US20080300401A1 (en) Novel chlorination process for preparing sucralose
JP3055910B2 (ja) 糖類の塩素化方法
AU2007308948A1 (en) Process for the preparation of sucrose-6-ester by esterification in the presence of solid superacid catalyst
GB2079749A (en) Process for the preparation of 4,1',6'-trichloro-4,1',6'- trideoxygalactosucrose
US20080300392A1 (en) Novel chlorination process for preparing sucralose
GB2065648A (en) Preparation of 4,1',6'-trichloro-4, 1',6'-trideoxygalactosucrose
JPS6338999B2 (de)
JPH0778071B2 (ja) スクロース誘導体の製造法
KR850000078B1 (ko) 4,1',6'-트리클로로-4,1',6'-트리데옥시-갈락토슈크로오스의 제법
IE50762B1 (en) Process for the preparation of 4,1',6',trichloro-4,1',6',trideoxy-galactosucrose

Legal Events

Date Code Title Description
R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term