JPH0916940A - Perpendicular magnetic recording medium - Google Patents

Perpendicular magnetic recording medium

Info

Publication number
JPH0916940A
JPH0916940A JP18804095A JP18804095A JPH0916940A JP H0916940 A JPH0916940 A JP H0916940A JP 18804095 A JP18804095 A JP 18804095A JP 18804095 A JP18804095 A JP 18804095A JP H0916940 A JPH0916940 A JP H0916940A
Authority
JP
Japan
Prior art keywords
magnetic
layer
recording
film
recording medium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP18804095A
Other languages
Japanese (ja)
Other versions
JP3019140B2 (en
Inventor
Toshio Ando
敏男 安藤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Victor Company of Japan Ltd
Original Assignee
Victor Company of Japan Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Victor Company of Japan Ltd filed Critical Victor Company of Japan Ltd
Priority to JP7188040A priority Critical patent/JP3019140B2/en
Publication of JPH0916940A publication Critical patent/JPH0916940A/en
Application granted granted Critical
Publication of JP3019140B2 publication Critical patent/JP3019140B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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  • Thin Magnetic Films (AREA)

Abstract

PURPOSE: To increase recording sensitivity and reproduction output by forming a perpendicular soft magnetic layer of soft magnetic with regard to a magnetic field in a perpendicular direction on a perpendicular recording layer. CONSTITUTION: When a perpendicular magnetic recording medium is produced as a discoid medium, a laminated film structure is formed by laminating a glass substrate 1, an intrasurface hard film 2 of CoSm having 150nm thickness, a soft magnetic film 3 made of CoZrNb having 600nm thickness, a perpendicular recording film 4 made of CoCrTa having 50nm thickness, a perpendicular recording film 5 made of CoPr having having 50-200nm thickness and a protective film 6 made of SiO2 having 15nm thickness. The compsn. of the CoPr 5 is controlled by varying the number of Pr chips on a discoid Co target. Since the resultant perpendicular magnetic recording medium has the layer 5 which is soft magnetic to a magnetic field in a perpendicular direction on the perpendicular recording layer 4, recording sensitivity and reproduction output are increased.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、垂直磁気記録媒体に関
するものであり、特に、その入出力特性の改良に関する
ものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a perpendicular magnetic recording medium, and more particularly to improvement of its input / output characteristics.

【0002】[0002]

【従来の技術】垂直磁気記録は、面内記録よりも高密度
化が可能な方式として研究開発が進められている。一般
に、垂直磁気記録の高密度化を図るためには、高い記録
感度と高い再生出力が要求される。このような垂直磁気
記録媒体として、例えば、特開昭57−113415号
公報(文献1)又は特開昭61−131228号公報
(文献2)で示すものが提案されている。文献1に開示
された垂直磁気記録媒体は、飽和磁化Msが小さく保磁
力Hcの大きい垂直異方性磁性薄膜からなる書き込み層
と飽和磁化Msが大きく保磁力Hcの小さい垂直異方性
磁性薄膜からなる読み出し層を重ねて2重構造としたも
のである。そして、このような構成により、情報の保存
性及び読み出し時のS/Nをよくすることができる旨が
示されている。
2. Description of the Related Art Perpendicular magnetic recording is being researched and developed as a method capable of higher density than in-plane recording. Generally, high recording sensitivity and high reproduction output are required in order to increase the density of perpendicular magnetic recording. As such a perpendicular magnetic recording medium, for example, ones disclosed in JP-A-57-113415 (reference 1) or JP-A-61-131228 (reference 2) have been proposed. The perpendicular magnetic recording medium disclosed in Document 1 is composed of a writing layer composed of a perpendicular anisotropic magnetic thin film having a small saturation magnetization Ms and a large coercive force Hc and a perpendicular anisotropic magnetic thin film having a large saturation magnetization Ms and a small coercive force Hc. The read layer is formed into a double structure. Further, it is shown that such a configuration can improve the storability of information and the S / N at the time of reading.

【0003】また、文献2に開示された垂直磁気記録媒
体は、基板上に高透磁率磁性体層を形成し、この高透磁
率磁性体層上に非磁性体層を介して膜面に垂直方向に磁
気異方性を有する磁性体層を設けてなる磁気記録媒体に
おいて、この膜面に対し垂直方向に磁気異方性を有する
磁性体層上に、面内方向に対して高透磁率である磁性体
層(Ni−Fe)を積層形成したものである。そして、
このような構成により、スペ−シングに対する記録密度
の変動を抑えるのに有効である旨が示されている。
Further, in the perpendicular magnetic recording medium disclosed in Document 2, a high magnetic permeability magnetic layer is formed on a substrate, and the high magnetic permeability magnetic layer is perpendicular to the film surface via a nonmagnetic layer. In a magnetic recording medium provided with a magnetic layer having magnetic anisotropy in the direction, on the magnetic layer having magnetic anisotropy in the direction perpendicular to the film surface, with high magnetic permeability in the in-plane direction. It is formed by laminating a certain magnetic layer (Ni-Fe). And
It has been shown that such a structure is effective in suppressing the fluctuation of the recording density with respect to the spacing.

【0004】[0004]

【発明が解決しようとする課題】しかし、文献1の垂直
磁気記録媒体ように、上の層である読み出し層が下の層
である書き込み層より飽和磁化Msが大きく、保磁力H
cが小さいというだけでは、下の高Hc層に信号を書き
込むことが困難であるという事情は変わらず、記録感度
は向上しない。また、記録時には、書き込み層と同時に
上の層である読み出し層(低Hc)にも記録されてしま
うため、必ずしも読み出し時のS/N比の向上は期待で
きない。また、文献2の垂直磁気記録媒体は、垂直記録
層の上に面内方向に対して高透磁率である磁性層を設け
たもので、スペ−シングに対する記録密度の変動を抑え
るのには有効であるが、ヘッドと高透磁率磁性層との間
で閉ル−プが形成されてしまうため、記録感度、再生出
力の点ではマイナスである。そこで、本発明は上記の点
に着目してなされたものであり、記録感度、再生出力の
両方を向上させることを目的とするものである。
However, as in the perpendicular magnetic recording medium of Document 1, the upper layer of the read layer has a larger saturation magnetization Ms than the lower layer of the write layer, and has a coercive force H.
Just because c is small does not change the situation that it is difficult to write a signal in the high Hc layer below, and the recording sensitivity is not improved. Further, at the time of recording, since the data is recorded on the upper layer, ie, the reading layer (low Hc), simultaneously with the writing layer, it is not necessarily expected that the S / N ratio at the time of reading is improved. Further, the perpendicular magnetic recording medium of Document 2 is one in which a magnetic layer having a high magnetic permeability in the in-plane direction is provided on the perpendicular recording layer, and it is effective for suppressing the fluctuation of the recording density due to the spacing. However, since a closed loop is formed between the head and the high-permeability magnetic layer, the recording sensitivity and the reproduction output are negative. Therefore, the present invention has been made in view of the above points, and an object thereof is to improve both recording sensitivity and reproduction output.

【0005】[0005]

【課題を解決するための手段】本願発明は、斯かる問題
に鑑みなされたものであり、請求項1に係る発明は、
「垂直記録層の上に、垂直方向の磁界に対して軟磁性で
ある垂直軟磁性層を有することを特徴とする垂直磁気記
録媒体。」を提供するものであり、請求項2に係る発明
は、「該垂直軟磁性層は、CoPrを主成分とする合金
であることを特徴とする請求項1記載の垂直磁気記録媒
体。」を提供するものであり、請求項3に係る発明は、
「該垂直軟磁性層のCoPrを主成分とする合金は、P
rの組成比が4atm%乃至30atm%であることを特徴と
する請求項2記載の垂直磁気記録媒体。」を提供するも
のである。
The present invention has been made in view of such problems, and the invention according to claim 1 is
The invention according to claim 2 provides "a perpendicular magnetic recording medium having a perpendicular soft magnetic layer which is soft magnetic with respect to a perpendicular magnetic field on the perpendicular recording layer." , "The perpendicular soft magnetic layer is an alloy containing CoPr as a main component, and the perpendicular magnetic recording medium according to claim 1."
“The alloy containing CoPr as the main component of the perpendicular soft magnetic layer is P
3. The perpendicular magnetic recording medium according to claim 2, wherein the composition ratio of r is 4 atm% to 30 atm%. ”.

【0006】[0006]

【作用】記録時には、ヘッドから発生する磁束が効率良
く集束し、垂直記録層において小さな起磁力で大きなヘ
ッド磁界が得られる。この結果、記録感度が向上する。
また、再生時には、垂直記録層から発生した磁界が、垂
直軟磁性層によって増幅され、再生出力が向上する。
In recording, the magnetic flux generated from the head is efficiently focused, and a large head magnetic field can be obtained with a small magnetomotive force in the perpendicular recording layer. As a result, the recording sensitivity is improved.
Further, during reproduction, the magnetic field generated from the perpendicular recording layer is amplified by the perpendicular soft magnetic layer, and the reproduction output is improved.

【0007】[0007]

【実施例】以下、図面を参照して本発明の実施例につい
て説明する。図1は、本発明の垂直磁気記録媒体をディ
スク状の媒体として実施した場合の積層膜構造を示す断
面図である。同図において、1はガラス基板、2はCo
Smからなる面内ハード膜(膜厚150nm)、3はC
oZrNbからなる軟磁性膜(膜厚600nm)、4は
CoCrTaからなる垂直記録膜(膜厚50nm)、5
はCoPrからなる垂直軟磁性層(膜厚50〜200n
m)、6はSiO2からなる保護膜(膜厚15nm)を
それぞれ示す。なお、CoPr垂直軟磁性層5をCoC
rTa垂直記録層4の上に成膜するのにはDCマグネト
ロンスパッタ法を用いた。この際、CoPrの組成は、
Coの円板状のタ−ゲットの上にPrのチップを配置
し、このPrのチップ数を変えることにより制御した。
Embodiments of the present invention will be described below with reference to the drawings. FIG. 1 is a cross-sectional view showing a laminated film structure when the perpendicular magnetic recording medium of the present invention is implemented as a disk-shaped medium. In the figure, 1 is a glass substrate, 2 is Co
In-plane hard film made of Sm (film thickness 150 nm), 3 is C
Soft magnetic film made of oZrNb (film thickness 600 nm), 4 is a perpendicular recording film made of CoCrTa (film thickness 50 nm), 5
Is a perpendicular soft magnetic layer made of CoPr (film thickness 50 to 200 n
m) and 6 are protective films made of SiO 2 (film thickness 15 nm), respectively. The CoPr perpendicular soft magnetic layer 5 is formed of CoC.
A DC magnetron sputtering method was used to form a film on the rTa perpendicular recording layer 4. At this time, the composition of CoPr is
A Pr chip was placed on a Co disk-shaped target, and control was performed by changing the number of Pr chips.

【0008】次に、ここで用いたCoPr垂直軟磁性層
の磁気特性について説明する。図2に、CoPr膜の膜
面垂直方向と面内方向の典型的なM−Hカ−ブを示す。
同図において、カーブAは膜面に垂直な方向のM−Hカ
ーブを示し、カーブBは面内方向のM−Hカーブを示
す。垂直方向の保磁力Hcは、200 Oe以下と小さ
い。また、異方性磁界Hkを同図のように面内方向のカ
−ブBの接線から求めると、約4KOeと大きい。更に
垂直方向のカ−ブをHd=4πMで反磁界補正して得ら
れる角型比Rsはほぼ1である。以上のことから、この
CoPr膜は垂直磁気異方性が極めて強く、かつ垂直方
向の磁界に対して軟磁性を示しているといえる。
Next, the magnetic characteristics of the CoPr perpendicular soft magnetic layer used here will be described. FIG. 2 shows typical MH curves of the CoPr film in the direction perpendicular to the film surface and the in-plane direction.
In the figure, a curve A shows an MH curve in a direction perpendicular to the film surface, and a curve B shows an MH curve in an in-plane direction. The coercive force Hc in the perpendicular direction is as small as 200 Oe or less. Further, when the anisotropic magnetic field Hk is calculated from the tangent line of the curve B in the in-plane direction as shown in FIG. Further, the squareness ratio Rs obtained by demagnetizing the vertical curve with Hd = 4πM is approximately 1. From the above, it can be said that this CoPr film has extremely strong perpendicular magnetic anisotropy and exhibits soft magnetism with respect to a magnetic field in the perpendicular direction.

【0009】図3は、CoPrの組成比と磁気特性との
関係を示したものである。同図(A)、(B)、(C)
の横軸は何れも、CoPr合金中のPrの組成比(at
m%)を表し、縦軸は、それぞれ飽和磁化Ms、異方性
磁界Hk、保磁力Hcを表す。なお、CoPrの膜厚は
何れも0.1μmである。垂直記録層4の上に設ける垂
直軟磁性層5としては、Ms≧500 emu/cc、
Hk≧1 kOe、Hc≦200 Oe、Rs≧0.9で
あることが望ましい。即ちPrの組成比は、4〜30 a
tm%が望ましい。
FIG. 3 shows the relationship between the composition ratio of CoPr and the magnetic characteristics. The same figure (A), (B), (C)
The abscissa of each of the graphs is the composition ratio of Pr in the CoPr alloy (at
m%), and the vertical axis represents the saturation magnetization Ms, the anisotropic magnetic field Hk, and the coercive force Hc, respectively. The film thickness of CoPr is 0.1 μm. As the perpendicular soft magnetic layer 5 provided on the perpendicular recording layer 4, Ms ≧ 500 emu / cc,
It is desirable that Hk ≧ 1 kOe, Hc ≦ 200 Oe, and Rs ≧ 0.9. That is, the composition ratio of Pr is 4 to 30 a.
tm% is desirable.

【0010】次に、図1に示した本発明の垂直磁気記録
媒体の電磁変換特性について図4を参照して説明する。
図4は、横軸に記録電流(mA)、縦軸に孤立波再生出
力(mV)をとったものであり、同図中、カーブCは垂
直軟磁性層5としてCoPrを50nm形成したサンプ
ルの特性を示し、カーブDは同様に垂直軟磁性層5とし
てCoPrを100nm形成したサンプルの特性を示
し、カーブEは同様に垂直軟磁性層5としてCoPrを
200nm形成したサンプルの特性を示す。なお、図5
は、比較例として、垂直軟磁性層5を形成していないサ
ンプルの特性であり、カーブFは垂直記録膜4としてC
oCrTaを50nm形成したサンプルの特性を示し、
カーブGは垂直記録膜4としてCoCrTaを100n
m形成したサンプルの特性を示す。なお、これらの特性
評価は、トラック幅7μm、主磁極厚0.3μm、コイ
ル40タ−ンの単磁極ヘッドを用いて行なった。また、
測定条件は、相対速度21.4m/s、スペ−シング
0.17μmとした。
Next, the electromagnetic conversion characteristics of the perpendicular magnetic recording medium of the present invention shown in FIG. 1 will be described with reference to FIG.
FIG. 4 shows the recording current (mA) on the horizontal axis and the solitary-wave reproduction output (mV) on the vertical axis. In FIG. 4, a curve C represents a sample in which CoPr of 50 nm is formed as the perpendicular soft magnetic layer 5. Curve D shows the characteristics of the sample in which CoPr was formed to 100 nm as the vertical soft magnetic layer 5, and curve E similarly shows the characteristics of the sample in which CoPr was formed to 200 nm as the vertical soft magnetic layer 5. FIG.
Is a characteristic of a sample in which the perpendicular soft magnetic layer 5 is not formed as a comparative example, and the curve F is C as the perpendicular recording film 4.
Shows the characteristics of a sample in which oCrTa is formed to 50 nm,
The curve G is 100 n of CoCrTa for the perpendicular recording film 4.
m shows the characteristics of the formed sample. The evaluation of these characteristics was performed using a single magnetic pole head having a track width of 7 μm, a main magnetic pole thickness of 0.3 μm, and a coil 40 turn. Also,
The measurement conditions were a relative speed of 21.4 m / s and a spacing of 0.17 μm.

【0011】これらの測定結果から明かなように、Co
Pr垂直軟磁性層がない場合、飽和記録ができておらず
再生出力も小さい。これに対し、本発明の実施例に係る
垂直磁気記録媒体では、垂直記録膜4の上に垂直軟磁性
膜5としてCoPrを設けることにより、小さな起磁力
M.M.Fでも充分飽和した高い記録感度が得られると
ともに、大きな再生出力が得られる。
As is clear from these measurement results, Co
When the Pr perpendicular soft magnetic layer is not provided, saturated recording is not achieved and the reproduction output is small. On the other hand, in the perpendicular magnetic recording medium according to the embodiment of the present invention, by providing CoPr as the perpendicular soft magnetic film 5 on the perpendicular recording film 4, a small magnetomotive force M.M. M. Even at F, a sufficiently saturated high recording sensitivity can be obtained and a large reproduction output can be obtained.

【0012】[0012]

【発明の効果】以上説明したように本発明の、垂直記録
層の上に、垂直方向の磁界に対して軟磁性である層を有
する垂直磁気記録媒体によれば、記録感度および再生出
力が高くなるという効果がある。
As described above, according to the perpendicular magnetic recording medium of the present invention, which has the soft magnetic layer against the perpendicular magnetic field on the perpendicular recording layer, the recording sensitivity and the reproduction output are high. There is an effect that.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の実施例に係る垂直磁気記録媒体の積層
膜構造を示す断面図である。
FIG. 1 is a cross-sectional view showing a laminated film structure of a perpendicular magnetic recording medium according to an example of the present invention.

【図2】CoPr膜の膜面垂直方向と面内方向のM−H
カ−ブを示す図である。
FIG. 2 is an MH in a direction perpendicular to the film surface of the CoPr film and in the in-plane direction.
It is a figure which shows a curve.

【図3】CoPrの組成比と磁気特性との関係を示す図
である。
FIG. 3 is a diagram showing a relationship between a composition ratio of CoPr and magnetic characteristics.

【図4】本発明の実施例に係る垂直磁気記録媒体の入出
力特性を示す図である。
FIG. 4 is a diagram showing input / output characteristics of a perpendicular magnetic recording medium according to an example of the present invention.

【図5】比較例に係る垂直磁気記録媒体の入出力特性を
示す図である。
FIG. 5 is a diagram showing input / output characteristics of a perpendicular magnetic recording medium according to a comparative example.

【符号の説明】[Explanation of symbols]

1 ガラス基板 2 CoSmからなる面内ハード膜 3 CoZrNbからなる軟磁性膜 4 CoCrTaからなる垂直記録膜 5 CoPrからなる垂直軟磁性層 6 SiO2からなる保護膜DESCRIPTION OF SYMBOLS 1 Glass substrate 2 In-plane hard film made of CoSm 3 Soft magnetic film made of CoZrNb 4 Perpendicular recording film made of CoCrTa 5 Vertical soft magnetic layer made of CoPr 6 Protective film made of SiO 2

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】垂直記録層の上に、垂直方向の磁界に対し
て軟磁性である垂直軟磁性層を有することを特徴とする
垂直磁気記録媒体。
1. A perpendicular magnetic recording medium comprising a perpendicular soft magnetic layer which is soft magnetic with respect to a perpendicular magnetic field on the perpendicular recording layer.
【請求項2】該垂直軟磁性層は、CoPrを主成分とす
る合金であることを特徴とする請求項1記載の垂直磁気
記録媒体。
2. The perpendicular magnetic recording medium according to claim 1, wherein the perpendicular soft magnetic layer is an alloy containing CoPr as a main component.
【請求項3】該垂直軟磁性層のCoPrを主成分とする
合金は、Prの組成比が4atm%乃至30atm%であるこ
とを特徴とする請求項2記載の垂直磁気記録媒体。
3. The perpendicular magnetic recording medium according to claim 2, wherein the alloy containing CoPr as a main component in the perpendicular soft magnetic layer has a Pr composition ratio of 4 atm% to 30 atm%.
JP7188040A 1995-06-29 1995-06-29 Perpendicular magnetic recording media Expired - Lifetime JP3019140B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP7188040A JP3019140B2 (en) 1995-06-29 1995-06-29 Perpendicular magnetic recording media

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP7188040A JP3019140B2 (en) 1995-06-29 1995-06-29 Perpendicular magnetic recording media

Publications (2)

Publication Number Publication Date
JPH0916940A true JPH0916940A (en) 1997-01-17
JP3019140B2 JP3019140B2 (en) 2000-03-13

Family

ID=16216629

Family Applications (1)

Application Number Title Priority Date Filing Date
JP7188040A Expired - Lifetime JP3019140B2 (en) 1995-06-29 1995-06-29 Perpendicular magnetic recording media

Country Status (1)

Country Link
JP (1) JP3019140B2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8498081B2 (en) 2011-03-24 2013-07-30 Kabushiki Kaisha Toshiba Perpendicular magnetic recording medium including soft-magnetic-particles-mixed protective layer on top of recording layer and magnetic disk device having the same

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8498081B2 (en) 2011-03-24 2013-07-30 Kabushiki Kaisha Toshiba Perpendicular magnetic recording medium including soft-magnetic-particles-mixed protective layer on top of recording layer and magnetic disk device having the same

Also Published As

Publication number Publication date
JP3019140B2 (en) 2000-03-13

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