JPH10215856A - 蒸留方法 - Google Patents
蒸留方法Info
- Publication number
- JPH10215856A JPH10215856A JP2823398A JP2823398A JPH10215856A JP H10215856 A JPH10215856 A JP H10215856A JP 2823398 A JP2823398 A JP 2823398A JP 2823398 A JP2823398 A JP 2823398A JP H10215856 A JPH10215856 A JP H10215856A
- Authority
- JP
- Japan
- Prior art keywords
- fusel oil
- alcohol
- distillation
- fraction
- aqueous fraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims abstract description 40
- 238000004821 distillation Methods 0.000 title claims description 70
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 139
- 239000001760 fusel oil Substances 0.000 claims abstract description 77
- 239000012223 aqueous fraction Substances 0.000 claims abstract description 36
- 230000001476 alcoholic effect Effects 0.000 claims abstract description 26
- 238000001816 cooling Methods 0.000 claims abstract description 12
- 238000000926 separation method Methods 0.000 claims description 20
- 235000013334 alcoholic beverage Nutrition 0.000 claims description 12
- 235000013522 vodka Nutrition 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 8
- 238000002194 freeze distillation Methods 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 6
- 238000011084 recovery Methods 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 235000019441 ethanol Nutrition 0.000 description 76
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 17
- 239000000203 mixture Substances 0.000 description 10
- QPRQEDXDYOZYLA-UHFFFAOYSA-N 2-methylbutan-1-ol Chemical compound CCC(C)CO QPRQEDXDYOZYLA-UHFFFAOYSA-N 0.000 description 9
- 239000002609 medium Substances 0.000 description 9
- 239000008346 aqueous phase Substances 0.000 description 8
- 239000012071 phase Substances 0.000 description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 7
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 6
- PHTQWCKDNZKARW-UHFFFAOYSA-N isoamylol Chemical compound CC(C)CCO PHTQWCKDNZKARW-UHFFFAOYSA-N 0.000 description 6
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 6
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 6
- 150000001298 alcohols Chemical class 0.000 description 5
- 235000013405 beer Nutrition 0.000 description 5
- 235000013361 beverage Nutrition 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 4
- 235000015096 spirit Nutrition 0.000 description 4
- 239000002351 wastewater Substances 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 3
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 235000013339 cereals Nutrition 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 239000002045 hydroalcoholic fraction Substances 0.000 description 3
- 239000007791 liquid phase Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 241000209140 Triticum Species 0.000 description 2
- 235000021307 Triticum Nutrition 0.000 description 2
- 235000020051 akvavit Nutrition 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000003113 dilution method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 235000013531 gin Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 235000021577 malt beverage Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H6/00—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
- C12H6/02—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by distillation
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H6/00—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
- C12H6/04—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by freezing
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Food Science & Technology (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
- Alcoholic Beverages (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB9702659.5 | 1997-02-10 | ||
| GB9702659A GB2305935B (en) | 1997-02-10 | 1997-02-10 | Freeze distillation process and alcohol-containing product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH10215856A true JPH10215856A (ja) | 1998-08-18 |
Family
ID=10807352
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2823398A Withdrawn JPH10215856A (ja) | 1997-02-10 | 1998-02-10 | 蒸留方法 |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JPH10215856A (da) |
| CA (1) | CA2228908C (da) |
| DE (1) | DE19804130A1 (da) |
| DK (1) | DK18498A (da) |
| GB (1) | GB2305935B (da) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| LV13003B (en) | 2002-10-03 | 2003-07-20 | Spirits Product Internat Intel | Method for processing vodka |
| DE602007008548D1 (de) * | 2007-06-26 | 2010-09-30 | Foss Analytical As | Vorrichtung und Verfahren zum Testen einer Vinifikationsflüssigkeit |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1570944A (en) * | 1977-03-19 | 1980-07-09 | Douwe Egberts Tabaksfab | Process for the concentration of aqueous solutions |
| GB2261442A (en) * | 1991-11-08 | 1993-05-19 | David George Pollard | Process for freeze-concentrating beer |
| US5304384A (en) * | 1993-03-23 | 1994-04-19 | Labatt Brewing Company Limited | Improvements in production of fermented malt beverages |
-
1997
- 1997-02-10 GB GB9702659A patent/GB2305935B/en not_active Expired - Lifetime
-
1998
- 1998-02-03 DE DE19804130A patent/DE19804130A1/de not_active Withdrawn
- 1998-02-05 CA CA2228908A patent/CA2228908C/en not_active Expired - Lifetime
- 1998-02-09 DK DK199800184A patent/DK18498A/da not_active Application Discontinuation
- 1998-02-10 JP JP2823398A patent/JPH10215856A/ja not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| CA2228908C (en) | 2010-06-29 |
| GB9702659D0 (en) | 1997-04-02 |
| DK18498A (da) | 1998-08-11 |
| DE19804130A1 (de) | 1998-08-13 |
| GB2305935A (en) | 1997-04-23 |
| GB2305935B (en) | 1997-10-01 |
| CA2228908A1 (en) | 1998-08-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4867997A (en) | Process for producing alcohol-reduced or alcohol-free beverages made by natural fermentation | |
| US5304384A (en) | Improvements in production of fermented malt beverages | |
| US5356641A (en) | Process for preparing an oak wood extract and distillate | |
| CA1236035A (en) | Method for decreasing the alcohol content of alcohol- containing beverages, particularly wine and sparkling wine | |
| US4885184A (en) | Process for preparing malt liqueur | |
| TWI668306B (zh) | 啤酒風味飲料之製造方法 | |
| US5077061A (en) | Method of making alcohol-free or nearly alcohol-free beer | |
| US5034238A (en) | Process for the reduction of the alcohol content of alcoholic beverages | |
| EP0679419B1 (en) | Extraction of hops | |
| CA1245171A (en) | Method of enhancing the bitterness of beer | |
| US5079025A (en) | Process for the removal of ethanol from drinks produced utilizing extraction with compressed carbon dioxide and carbon dioxide regeneration | |
| US4971807A (en) | Process for the production of beer with a low alcohol content | |
| JP6807928B2 (ja) | 発酵飲料の製造方法 | |
| JPH10215856A (ja) | 蒸留方法 | |
| JP6420047B2 (ja) | 発酵麦芽飲料 | |
| US3821418A (en) | Preparation of alcoholic malt beverages | |
| JP6420044B2 (ja) | 発酵麦芽飲料 | |
| BE900359A (nl) | Alcoholvrije wijn en bereiding ervan. | |
| US613915A (en) | Manufacture of non-intoxicating beverages | |
| JPS611374A (ja) | ビ−ルの苦味の増強方法 | |
| US4790993A (en) | Process for the production of alcohol-free, yeast white beer | |
| JP6371070B2 (ja) | 発酵麦芽飲料 | |
| RU2676909C1 (ru) | Способ производства безалкогольного пива | |
| JP6420045B2 (ja) | 発酵麦芽飲料 | |
| EP1866406B1 (en) | Method and apparatus for the production of distilled spirits |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A300 | Withdrawal of application because of no request for examination |
Free format text: JAPANESE INTERMEDIATE CODE: A300 Effective date: 20050510 |