JPH1088103A - Nephrite powder-containing material - Google Patents

Abstract

PROBLEM TO BE SOLVED: To obtain the subject material containing a specific amount of nephrite powder, capable of affording synthetic resin products improved in physical properties along with having medically and physically excellent effect such as heavy metal removing function. SOLUTION: This material contains 5-15wt.% nephrite powder with a particle size corresponding to pref. 100-350mesh. It is preferable that the nephrite powder is magnesia-based tremolite nephrite, being zero in negative value σ<18> and consisting of a composition comprising 34wt.% silicon, 10wt.% magnesium, 4.9wt.% calcium, 23wt.% iron, 0.16wt.% aluminum, 0.17wt.% copper, 0.046wt.% cobalt, 0.14wt.% manganese, 0.024wt.% tin, 0.00072wt.% beryllium, 0.0013wt.% silver, 0.0038wt.% titanium, 0.0028wt.% nickel, 0.0030wt.% chromium, and 0wt.% others.

Description

DETAILED DESCRIPTION OF THE INVENTION

[0001]

TECHNICAL FIELD The present invention relates to a soft ball (Nephrite Jad
e) A new material (matrix (base material)) containing (as the main material) containing the fine powder of (1). More specifically, the present invention comprises fine particles of soft jade in which the fibers of the amphibole-positive stone series have a very fine interwoven fiber suspension structure, and are used for medical supplies, packaging supplies, container supplies, and interior supplies. ,
Manufacture of industrial goods, transportation goods, transportation goods, daily necessities, leisure goods, sports goods, agricultural goods, fishing equipment, electronic equipment, precision equipment goods, etc. In particular, it excels in treating human body diseases (headache, insomnia, indigestion, numbness of limbs, etc.), removing impurities (heavy metals, etc.) from objects, improving water quality, promoting the growth of animals and plants, etc. It relates to a novel material which enables the production of a wide variety of articles of outstanding efficacy which can be widely used for a beneficial life.

[0002]

2. Description of the Related Art As is well known, jade is roughly divided into hard jade and soft jade, and jadeite is classified as pyroxene fa.
mily) is a pyroxene group mineral and is a monoclinic substance composed of silicic acid, aluminum oxide and soda. Its hardness is equal to that of a dense mass such as quartz, and its color is black, blue-green or green, transparent or translucent, and usually a ball indicates this hard ball.

[0003] Nephrite Jade is an inosilicate (In
osilicates) is a monoclinic pyroxene mineral body, which is divided into soft jade and serpentinized ultrabasic soft jade among mafic marbles, and their quality is fine structure, that is, hornblende-positronite crystallite. Is determined by the degree of coarseness of the bundle and the fibers, and it is known that the finer the fibers, the better the quality.

A report published in the German prestigious medical literature (KRAFF der KR by Mauda Palmer Die Verborgene)
According to ISTALLE und der EDELSTEINE "), jadeite and soft jade are two different ores that contain silicon and oxygen like most gemstones, but jadeite is composed of granular crystals. On the other hand, soft jade is composed of countless crystals such as fibrous and hair and fine aggregates.In particular, soft jade is different from the sodium and aluminum components in jade, and three minerals that are beneficial to the human body. ,
In other words, it has been recently described that, since it contains calcium, iron, and magnesium as main components, wearing soft balls has a great effect on healing of diseases caused by high blood pressure, diabetic cardiovascular disorder, heart disease and kidney disorder.

[0005] According to the Eastern medicine treasure book, which is a classic of Oriental medicine, if you put the balls in Umeshu and Jiyu sake, they will turn into water, and if you put them in sizzle water, it will be easy to drink, and you will eat the balls in the size of mazu. And waste products are discharged outside the body. One shod of litter, one sho of Jinyu grass, one sho of rice and rice, and three sho of white dew are mixed together and put in a copper pot to cook rice. It is known as a soybean liquor, so-called Shinsen Tamazuro. In addition, according to Shinnobu herb, Karamoto herb, and Herbaceae, crushing balls into powder and making them like sesame seeds not only has the effect of enriching the stomachs and excreting waste products in the body, It removes fever and is effective on digestive system, produces asthma and body heat, good for chest anemia, rests thirst, crushes like sesame seeds and takes it for a long time, lightens as if you fly away It has a long life, lubricates the functioning of the lungs, helps vocal vocalization, is good for the throat, affects the hair, promotes the functioning of the viscera, and has the effect of particularly relieving stress-related nervous diseases. In addition, when muscle tension and convulsions occur, it is good to crush white balls into powder and eat it,
It has been known from a long time ago that the main components of soft balls exhibit excellent effects on the human body with almost no side effects, such as when scars are rubbed with soft balls for several days when there are scars on the face and body.

[0006]

However, despite the fact that soft beads are known for their outstanding medical efficacy due to their rarity, they are not suitable for use in neck wraps, rings, and the like.
It is limited to the use of jewelry such as bangles, etc., and it requires a long effort and delicate attention to processing soft beads, so it must be performed by a skilled person with a long experience. It is economically disadvantageous because it cannot be worked on, and it is economically disadvantageous, and there is almost no development as a general living article using soft balls. Therefore, research and development of this is urgently required. Have been.

[0007] The present inventor has paid attention to the outstanding medical effects of such soft balls, and after conducting research and experiments for more than ten years, began to develop all kinds of daily necessities, agricultural goods, industrial goods, and fisheries. Supplies, medical supplies, electronic apparatus supplies, to each article, such as civil engineering article, nephrite, especially a tremolite in bitter soil Dali Iwao, or manufactured nephrite powder defined by a negative value [delta] ¹⁸ 0, these During the manufacturing process of the article, when soft ball powder is added to the raw material of each article, and then mixed and molded by a normal method, the manufactured synthetic resin product has a heavy metal removing function, a bad smell removing function, a plant growth promoting function, The present inventors have found that they not only have excellent medical and physical effects such as a water quality improving function, but also have an increasing effect of improving the physical properties of each article itself, and have completed the present invention.

Accordingly, the main object of the present invention is to use the above-mentioned excellent effects of softballs and flourballs for daily use such as kitchen goods, leisure goods, sports goods, agricultural goods such as facility gardening, fish boxes and the like. Widely applied to daily life such as fishing goods, transportation such as automobile parts, transportation goods, packaging goods such as food packaging film, medical supplies such as eyeglass parts, electronic equipment such as electric and electronic parts, etc. An object of the present invention is to provide a novel material having excellent medical and physical effects.

[0009] Another object of the present invention is to maximize the use of flour powder that is treated as a residue or waste derived during mining or jewelry processing of rare flour consisting of unique components. It is to be. Other objects and advantages of the present invention are specified below.

[0010]

As a means for solving the above-mentioned problems of the prior art, the material containing soft powder according to the first aspect of the present invention contains 5 to 15% by weight of soft powder. It is characterized by being. The material containing soft flour powder according to the second aspect of the present invention is characterized in that the soft flour powder described in the first aspect has a particle size of 100 to 350 mesh.

[0011] Materials nephrite powder is contained according to the invention of claim 3, in tremolite nephrite nephrite powder in bitter soil Dali Iwao, as described in the claim 1 or 2, it is a negative value [delta] ¹⁸ 0 , Comprising the following composition (% by weight): Silicon 34 Magnesium 10 Calcium 4.9 Iron 0.23 Aluminum 0.16 Copper 0.17 Cobalt 0.046 Manganese 0.14 Tin 0.024 Beryllium 0.00072 Silver 0.0013 Titanium 0.0038 Nickel 0.0028 Chromium 0 .0030 Other 0

[0012]

BEST MODE FOR CARRYING OUT THE INVENTION In the present invention, each article means, in a non-limiting sense, a variety of types that require or are intended to be mixed with flour flour. Although the specification focuses on plastics that have a wide range of direct or indirect effects on human life, the materials of the present invention are not limited to plastic articles.

Accordingly, among the plastic raw materials described in this specification, thermoplastic synthetic resins are defined as polyvinyl chloride (PVC), polyvinyl acetate (PVAC), polyvinyl alcohol (PVA, PVAL), polyvinyl Acetal, polyvinyl formal (PVFM), polyvinyl butyral (PVB), polyvinylidene chloride (P
VDC), polyvinylidene chloride-polyvinyl chloride copolymer, polyethylene (PE), polypropylene (PP), polystyrene (PS), styrene-butadiene copolymer (SB, HIPS), polystyrene form (EPS, FS), acrylonitrile-styrene copolymer ( AS, SAN), acrylonitrile-butadiene-styrene copolymer (ABS), ethylene-vinyl copolymer (EVA), ionomer
, Polycarbonate (PC), polyvinyl ether-
Polyvinyl methyl ether, polyvinyl ketone, polytetrafluoroethylene (PTFE), polychlorotrifluoroethylene (PCTFE), polyvinyl fluoride, polyvinylidene fluoride, tetrafluoroethylene-hexafluoropropylene copolymer,
Polyamide (PA, Nylon), polyacrylamide, polyacrylonitrile (AN), polyester, polyethylene terephthalate (PET), polybutylene terephthalate (PBT), polyacetal, polyoxymethylene (POM), polyethylene oxide, polyphenylene oxide (PPO), Polyacrylate (= polyacrylic ester), polymethacrylate (= polymethacrylic ester), polyurethane (PUR.AU.E)
U), polyphenylene sulfide (PPS), polysulfone (PSU), polymethacrylonitrile and the like.

The thermosetting resin includes phenol resin (PF), urea resin (UF), and melamine resin (M
F), unsaturated polyester resin (UP), diallyl phthalate resin (PDAP, DAP), aniline-formaldehyde, epoxy resin (EP), furan, xylene-
Formaldehyde, sulfonamide-formaldehyde, silicon (SI), polyurethane form, formaldehyde resin, ketone resin and the like are shown.

The synthetic resin products produced by containing the soft-ball flour of the present invention include not only daily necessities such as tableware, but also
It is needless to say that it can be manufactured and used by applying to accessories such as wrist rings and rings. Products made from the materials of the present invention include, in the case of plastic production, plastic films (industrial, agricultural), plastic lumps, plastic floor sheets, plastic rods, tubes and profiles, plastic leather,
It can be manufactured into plastic conveyor belts, vinyl wallpaper, recycled plastic raw materials (powder), and other plastic primary molded products.

On the other hand, in the case of a plastic foam molded product, it can be applied to expanded polystyrene (such as styrene) and industrial foam molded products (including soft and hard products). In reinforced plastic molded products, it can be manufactured into other reinforced plastic molded products such as plastic machinery parts (durability, addition of special reinforcing material). In industrial plastic molded products, plastic electric and electronic machine parts, plastic automobile parts It can be applied to cabinets for household equipment of plastic materials (television, electric storage, sewing machine cabinet, etc.), plastic furniture and other mechanical parts for plastic industry (pure plastic).

In the case of household plastic products, plastic tableware and kitchen utensils (tableware, dishes, cups, knives, spoons, etc.), plastic hygiene and cosmetics products (basins, bathtubs, soap boxes, trash boxes, etc.), Can be manufactured into plastic buttons, plastic decorations and other household plastic molded products. In the case of plastic molded packaging containers, it can be manufactured into plastic boxes (fish boxes, etc.), plastic bottles, tubs, similar containers, and other plastic packaging containers. it can.

That is, as the synthetic resin molded product using the material of the present invention, various products can be produced according to the classification of the synthetic resin raw materials as follows. PE: bottle, tube, wire coating, food packaging, film,
Pipes PS: Dolls, kitchen equipment, tableware, pipes, heat insulating materials, packaging supplies, office supplies, automobile, electricity, electronics, and other related industrial parts PP: EPDM, rubber for containers, pipes, films, artificial leather, packaging, etc. , Glass, etc. are used for automotive parts AS: kitchen supplies, telephone parts, pipes PVC: pipes, films, bottles, dolls, record boards, food containers, electric wire coatings Acryl: optical lenses, automotive supplies, television Protective plate PA: Bearing, hose, film PC: Electric parts Fluororesin: Gasket, for painting fly fan Polyester: Various springs (elastic plate), metal insert, gear bearing PF: Telephone parts, electric products, cups, car handle UF : Button, lighting equipment, clock, container, tableware, radio case MF: Bathtub, button, safety hat, tableware Unsaturated polyester: aircraft parts, fuel tanks, pipes, car bodies, helmets, fishing rods EP: car parts, electric parts, medical equipment PDAP: electric parts, terminal boards, micro switch boards PUR: electric wire coating, rubber SI: tape, release Molding agent, defoaming agent Furan: Laminated board, electrical insulating material Xylene: Laminated board molded article Aniline: Electrically insulating product, laminated board In addition, ABS, which is a high-grade resin intermediate between general-purpose resin and engineering plastic, is used for telephones, Radio, toys, dolls and other electrical and electronic products,
It can be manufactured into auto parts, and in the agricultural field,
For insect rescue of cereals, plastic greenhouses, flowerpots, etc., for fisheries, containers, artificial seaweeds, fish gear (ropes, fishing nets, floats), etc .; for foods, for food containers or packaging; Used for blood vessels, esophagus, urethra, ureters, joints, etc. and teeth, eyes, nose, ears, skin, etc. and other injection tubes and diapers used outside the body, and in the pharmaceutical field, coated granules and tablets etc. In the acoustic field, soundproofing agents, vibration damping agents, etc., in the optical field, eyeglass lenses, contact lenses, safety glasses,
In the field of textiles, such as nonwoven fabrics, carpets, rainwear, etc., in the field of paper, PE processed paper, plastic foam (pspaper), etc. In the field of office supplies, such as desks and chairs. In the field of household goods, tableware and tableware such as cutting boards, sinks, dishes, baby items such as tableware, dolls, toys, breast milk bottles, buckets, vegetable boxes, bathroom items, etc. In the sports field, boats, sports cars, skates, tennis rackets, golf clubs, etc. In the mechanical field, bearings, gears, brake shoes, etc. In the aircraft field, wings (main, tail, auxiliary), fuselage, windows, indoor bulletin boards In the marine field, ships, porthole frames, portholes, cabin doors, etc .; in the automotive and vehicle fields, safety glass, bumpers, body insulation, foam foam sheets. In the telecommunications field, such as telephones, exchanges, and terminal boxes for telephones, in the electronics industry, such as organic semiconductors, and in the electrical supplies field, such as electric fans, washing machines, televisions, radios, refrigerators, and barbers. In the field, interior and exterior materials such as zenith materials, wall materials, flooring materials, tiles, veranda boards, etc., in the civil engineering field, admixtures (eg, cement), water stoppage boards, greening of deserts, etc. For synthetic resin type, synthetic resin duplicated board, synthetic resin electric type, magnetic tape, etc., for reactors and various coating materials in the nuclear power field, for liquid hydrogen and liquid oxygen storage tanks in the space development field, and for packaging containers. Can be produced in plastic containers, plastic films, etc.

Although a method for molding a synthetic resin using the material of the present invention is known, the method shown in Table 1 below is used.

[0020]

[Table 1]

The particle size of the softball powder used in the material of the present invention is selected in consideration of the material of the article to be manufactured, the use of the molded product, and the like, but is generally preferably 100 to 350 mesh. reference). When the softness is to be increased as in the case of a molded article having a complicated shape or a thin article, it is more advantageous to use softball powder of about 250 to 300 mesh, which is finer particles, A general molded product is used after adding softball powder of 100 to 500 mesh. If the particle size of the soft powder is larger than the above range, the surface roughness of the product is undesirably severe, and particles finer than the above range are not easily crushed, which is not desirable.

In addition, when soft flour powder is added to an article sample to be manufactured, the amount of addition is 5%.
If the addition amount is less than 5%, the effect of the addition of the softball is not expected, which is not desirable. As the addition amount of the softball powder increases, the solid effectiveness of the softball increases, but the addition amount is small. If the amount is too large, the properties of the raw material resin, particularly the softness, are reduced to make the product fragile, and the molding fluidity may be lowered. 15% or less is suitable.

The product to which the material of the present invention is added, to which flour is added, can be used after making products such as jewelry, bowls, sculptures and the like using fluff, and the remaining stone can be crushed and used. It is economically advantageous in terms of quality, and is also highly evaluated economically in that a practical synthetic resin product having properties unique to a soft ball can be obtained at a lower unit price for a product such as an expensive jade.
In addition, various products made of the material of the present invention have higher mechanical properties and thermal properties, that is, heat resistance, tensile strength, compressive strength, and the like, than general synthetic resins containing no soft beads.

The soft jade flour used in the material of the present invention is an amphibole soft jade in magnesite daiwa, and has a negative value δ.
It is most preferable in terms of effect that the composition ratio is specified by ¹⁸⁰ and has the following composition ratio in [Table 2].

[0025]

[Table 2] Semi-quantitative analysis value (Semi-Qua) of the ball dust sample of the present invention
ntitative Analysis) (%) Silicon 34 Magnesium 10 Calcium 4.9 Iron 0.23 Aluminum 0.16 Copper 0.17 Cobalt 0.046 Manganese 0.14 Tin 0.024 Beryllium 0.00072 Silver 0.0013 Titanium 0.0038 Nickel 0.0028 Chromium 0.0030 Others 0 The production of the synthetic resin product to which the above-mentioned material of the present invention is used and to which a soft ball powder is added, and the effects exhibited by the product will be described in detail in the following examples.

[0026]

【Example】

<Example 1> 10 parts by weight of fluffy flour pulverized to a particle size of 150 mesh was added to and mixed with 90 parts by weight of polyethylene as a thermoplastic resin. The mixed raw materials were injected into the injection molding machine through a hopper of the injection molding machine, and then heated to 100 to 130 [deg.] C. to increase the softness and pressurized while pressing the raw materials into the mold.

The molded article cooled by the mold is drawn out at the same time as the mold is opened, and is provided in various forms of products (various containers such as tableware, accessories such as neckbands, bracelets, cormorants, and other decorative articles).
Was obtained. <Example 2> A raw material obtained by mixing 10 parts by weight of fluffy flour crushed to a particle size of 150 mesh with 90 parts by weight of a polyethylene resin was injected into an injection molding machine, and the mixture was heated to 35 to 45 ° C.
By pressing the raw material into the mold by pressurizing with a ram while increasing the softness to obtain a product of a certain shape (for example, tableware, bowls, ornaments, neckbands, bracelets, rings, earrings, etc.) ). <Example 3> A raw material obtained by mixing 10 parts by weight of soft ball powder crushed to a particle size of 300 mesh with 90 parts by weight of an acrylic resin is injected into an injection molding machine and heated to 35 to 45 ° C to be soft. By pressing the raw material into the mold by pressing with a ram while increasing the size, a product of a certain shape was obtained (for example, tableware, bowls, ornaments, neckbands, armbands, rings,
Earrings).

As shown in the above Examples 1-3, the manufactured synthetic resin product not only improves heat resistance and impact resistance, etc., but also is used as tableware due to the influence of far infrared rays generated from soft balls. In this case, the freshness of food and drink can be maintained for a long time, and when it is made into jewelry and worn, it has a therapeutic effect. <Experimental Example 1> The following experiment was conducted to test the presence of lead, heavy metals and other toxic components in the softball powder used in the production of the material in the examples of the present invention.

[0029]

[Table 3]

[0030]

[Table 4]

[0031]

[Table 5]

As shown in the above experimental results, the flour powder used in the production of the material of the present invention was composed of lead, heavy metal,
No other toxic components were detected, which proved to be safe when used as tableware. <Experimental Example 2> The test cup and the control cup (polyethylene material) manufactured in Example 2 of the present invention were filled with homogeneous Class A milk, left at ambient temperature for 48 hours, and then analyzed. The results are shown in Table 6 below.

[0033]

[Table 6]

Conclusion: A decrease in microorganisms harmful to the human body appeared. <Experimental Example 3> In this experiment, tap water was purified with a filter impregnated with the material of the present invention, and the effect of the purified soft water on the growth and development of silkworms and on the silkiness was examined (FIGS. 1 and 2). ,
(See FIG. 3). Materials and Methods Announced silkworm variety: Shiratama silkworm 2. 2. Breeding time: hatching nest silkworm (11-December) Rearing method: constant temperature and humidity, all-age mulberry leaf growth 4. Announced head count: control-150 animals, 2 repetitions Processing-130 animals, 2 repetitions Treatment content: Control-Spraying mulberry leaves with sprayed distilled water Treatment-Spraying soft ball water with mulberry leaves Treatment time: From the 2nd instar silkworm

[0035]

[Table 7]

[0036]

[Table 8]

[0037]

[Table 9]

[0038]

[Table 10]

◎ Results In terms of the weight of the larvae, the softball water treatment device was heavier than the control device, which was a distilled water treatment device, in particular, and the mature silkworm weighed 0.48 g per individual in all ages. 2. The ratio of cultivation is about 15% lower than that of the control with the soft ball soup plant 7
1.2%, and the amount of 10,000 silk collected was 7% lower than that of the control1
It was 5.4 g.

3. The total silk weight of the soft-ball plant is 2.14 g, which is about 6% heavier than the control, and the silk layer weight is also about 9% heavier.
It was 5 cg. The silk layer ratio appeared 2% higher in index than the control. 4. The soft-ball inlaying device had generally better threading results than the control. In particular, the length of the silk thread was long, the amount of the silk thread was large, and the disintegration rate was approximately 9% higher than that of the control by an index, and the disintegration thread amount was several times higher.

5. Regarding the yarn quality, the soft-ball-planted plant had a slightly thicker fineness, higher strength, elongation, and a higher raw silk ratio than the control. However, the amount of silk was small and the amount of the 10,000 raw silk was lower than the control. 6. No large difference was found between the control device and the treatment device in the surface structure of the silk thread. 7. The hypoglycemic effect of the silkworm larvae planted with soft jelly was 2 times higher than that of the control.
It was 70.3%, 4% higher.

8. The crystal structure of the planted soft ball had a pointed rod-like structure. <Experimental Example 4> In this experiment, tap water was purified with a filter impregnated with the material of the present invention, and changes in the activity of rats on day 20 of drinking the purified water for drinking potatoes were observed. Experimental result,
As shown in FIG. 4, in the stabilizing effect experiment, the central nervous system of the positive control group began to stabilize 5 minutes after drinking the Ubavit (Chinese name) drug, and gradually recovered to normal after 30 minutes. On the other hand, the rats in the general control group showed undulations in the activity rate and showed a tendency to decrease overall.

The activity rate of the drinking test water of the present invention (day 20 rats) is similar to that of the general control group, but the average area of the total activity rate is higher than that of the general control group and also positive. It can be seen that an even more significant difference occurs when compared to the control group. <Experimental Example 5> In this experimental example, an infrared experiment was performed on a soft ball used in the material of the present invention.

[0044]

[Table 11]

Morphology: Liquid liquefied tetrahydrofuran thin film Appears as a pattern conforming to the pattern of the polycarbonate resin, and appeared as an electromagnetic wave having a wavelength of 6 to 52 μm. <Experimental Example 6> In this experimental example, an experiment was performed on the chemical and biological oxygen demands for the ball meal sample used for the material of the present invention.

[0046]

[Table 12]

<Experimental Example 7> In this experimental example, an experiment was conducted on the influence of the softball powder used for the material of the present invention on the experimental device (rabbit).

[0048]

[Table 13]

Experimental procedure: 0.1 ml of the extract is placed on the inverted lower eyelid of the first side and then gently grasped for 1 second before releasing the upper and lower eyelids. The other side is not treated and is observed as a control. The treated eyes of the six rabbits are kept unwashed, and the eyes of the three rabbits are washed immediately after treatment with a stream of warm water for 1 minute. The eyes were pre-examined by fluorescence before treatment with the samples, and only animals that did not show corneal damage were used for the test. Eye lesions were observed at 24, 48, 72, 7 and 14 days after treatment.

[0050]

[Table 14]

I. Cornea (A) Opacity-Density (area for detoxification) Normal-0 Diffusion areas are scattered-Iris details are clearly visible-1 Translucent areas that are easily identified, details of the iris are slightly faint -2 Milky white area, iris detail not visible, pupil size almost indistinguishable -3 Opaque, iris invisible-4 (B) Corneal area Normal-0 1/4 or less, but non-zero-1 1/4 or more, 1/2 or less-2 1/2 or more, 3/4 or less-3/4 or more, total area or less-4 points: A x B x 5, total maximum value = 80 II. Iris (A) value Normal-0 Folded more than normal, hyperemia, swelling, pericardial congestion (these symptoms appear alone or in combination at any size), and the iris responds to light before (slow) (Remarkable response) -1 No response to light, bleeding, total destruction (one or all of these symptoms)-2 points A x 5, total possible maximum = 10 III. Conjunctiva (A) Red tide (relevant only to the conjunctiva of the eyelid) Normal-0 The blood vessels are significantly more reddened than normal-1 More diffuse, deeper crimson appears, and each blood vessel is easily distinguished-2 Diffuse Is red like raw beef -3 (B) chemosis no swelling -0 any swelling phenomena above normal (including swelling membrane) -1 apparent swelling with partial reversal of eyelid -2 Approximately half closed and swollen -3 About half of eyelid to complete swelling -4 (C) Secretion Normal-0 Optional phenomena different from normal (does not include small amounts observed in the medial eye end of normal animals) -1 Eye Secretion wet only on the eyebrows adjacent to the lid and eyelid-2 occupies a considerable area around the eye-3 points (A + B + C) x 2, total maximum = 20 Conclusion: This sample has no irritation to the eyes Is determined. Therefore, it was understood to be suitable for eye makeup products.

[0052]

[Table 15]

Experimental procedure: A patch test technique was used on the peeled and original skin of white rabbits. Hair was shaved short on the back and flank. Two regions on the back about 10 cm apart were selected as patch positions. On one side, make a small incision in four places in the patch area and peel off the skin (two of which are perpendicular to the rest in a "tic-tac-toe" manner). A one inch square patch of surgical gauze is applied using a rubber band and adhesive tape. The sample is introduced in a volume of 0.5 ml (g) below the patch at each site. Animal torso
Wrap with a rubberized cloth for an exposure time of 4 hours. Animals become immobile during the exposure time. After removing the patch,
The results of evaluating the reactions that appeared at each site based on the following scores are as follows.

Evaluation of skin reaction : Erythema and erythema formation No erythema-0 Very faint erythema (slightly recognizable) -1 Erythema roughly recognized-2 Normal to severe erythema-3 Severe erythema (beat) Edema formation no edema-0 very weak edema (slightly perceptible) -1 slight edema (significant edge of area) Is)
-2 Normal edema (about 1 mm swelling) -3

[0055]

[Table 16]

Conclusion: This sample is judged to have no skin irritation. Therefore, it appeared to be suitable for use in skin cosmetic products.

[0057]

[Table 17]

Preparation of sample: A portion of the sample was put into sterile distilled water, extracted by boiling for 10 minutes, and the extract was administered by intubation in an amount of 0.5 g per 100 g of body weight. Conclusion: The sample met the criteria that should not have oral toxicity. <Experimental Example 8> In this experimental example, an experiment was performed on the food decomposition rate of a rice bowl made of a synthetic resin prepared by adding a soft ball used for manufacturing the material of the present invention.

[0059]

[Table 18]

Experimental method: Five jade roses (test group) and the same number of general porcelain flat roses (control group) were filled with a mixture of rice and a sterilized number of 1: 1 and allowed to stand at room temperature for 24 hours. The flat rose lid was removed so that it was completely exposed to the air, and the two groups were placed approximately 1 meter apart. At the time point shown in the following results, the standard fine plate coefficient (Standard Plate Count) was performed.

[0061]

[Table 19]

Conclusion: In the decomposition of the food contents of the test group flat roses and the control group flat roses, the food decomposition rate of the test group flat roses was relatively lower than that of the control group flat roses. From this, it seems to have a good effect on food storability. <Experimental example 9> In this experimental example, as another method for investigating the various effects of the ball dust used in the material of the present invention on the living body, whether or not it actually has a good effect on the activity of plant cells In order to know whether it is Digitalis Lanata (Digit
alis lanata) The experiment on the effect on the growth of plant cells was performed by requesting the Bioinformatics Engineering Laboratory of Inha University.

Next, the results of medical biomechanical research experiments on the biological effects of softballs will be described in detail. In this experiment, 70% of the constituents of the human body were water, so it was determined that there would be a large relationship between the change in water and the effect on the human body, and what kind of effect it had on hard water was investigated.
Experiments on effects on the growth of plant cells (Digitalis lanata) were performed. A. Change in Hard Water <Experiment 1> After 100 mL of artificially made hard water was transferred to each of four flasks by 50 ml, soft balls were placed on the bottoms of two flasks for about 10 minutes.

In order to know the change in hardness, an appropriate method using EDTA (titer: 2.9412) was used. pH 10
1 ml of the above buffer solution and the indicator EBT were used. The change in hardness was measured by the amount of EDTA up to the moment when the color of the hard water was changed by EDTA. At this time, the color may return to the original color over time, but in this experiment, the measurement was performed based on the moment when the color changed. <Result 1> 1.70 ml of EDTA at 100 ppm of hard water
Required, 1.25 ml EDTA required after softball experiment, therefore 1
The hardness at 00.00 ppm drops to 73.53 ppm. That is, the hardness of 100.00 ppm was softened by 26.47%. <Experiment 2> 200 ml of 100 ppm hard water produced in the same manner as in Experiment 1 was transferred to a beaker, and soft balls were pickled.

After about 30 minutes, the water filled in the beaker was divided into three flasks and the change in hardness was measured. In this experiment, the color of the hard water was changed to EDTA to perform a more precise experiment.
EDTA until no further change after changing
And the hardness at that time was measured. <Result 2> The hard water of 100 ppm before the softball experiment was 89.26 ppm, 91.19 ppm, and 89.62 pp, respectively.
m means an average of 90.14 ppm, and thus a 9.9% decrease in hardness. <Experiment 3> This experiment was conducted using ordinary tap water. After filling the containers with tap water, the flasks were transferred to six flasks, and soft balls were placed on the bottoms of three flasks, and the hardness was measured after about 5 minutes. <Result 3> 97.48p of tap water without soft ball experiment
pm, 97.48 ppm, 97.48 ppm, average 9
7.48 ppm, and the tap water after the softball experiment was 91.1
9 ppm, 91.19 ppm, and 91.19 ppm, and the average was 91.19 ppm, which means that the average hardness was reduced by 6.5%. B. Effect of soft jade on proliferation of digitalis lanata (Digitalis lanata) suspension plant cells Digitalis lanata on growth medium
a) Effect of soft jade on cell growth

[0066]

[Table 20]

[0067]

[Table 21]

[0068]

[Table 22]

[0069]

[Table 23]

In [Table 20]-[Table 23],
[Table 20] shows the change in the total volume of the culture solution of the cells growing in the growth medium for 11 days. As time elapses, the depletion of the medium components and the evaporation of the medium occur in proportion to the increase in the number of cells that grow, so that the change in the volume of the whole culture medium reflects such factors. In particular, the humidity or temperature of the atmosphere is closely related to the evaporation of the medium, and such factors also influence the cell growth rate. As shown in the table, when soft beads were used, the volume of the whole culture solution was gradually reduced as compared with the control group not used. This is because the use of softballs compared to the control group has a faster cell growth rate with respect to medium evaporation or nutrient depletion, thus offsetting the rapid decrease in medium depleted to some extent. As shown in Table 21, the change in volume of only the sinking cells was measured. As shown in Table 21, cells were continuously used from day 4 to day 11 after inoculation. It can be inferred from the fact that the volume is observed to exhibit a larger increase. Therefore, when the soft jade was used, the growth rate was faster than in the control group where no soft jade was used.
Such a result can be said to be the result of offsetting nutrient depletion and the decrease in the volume of the whole culture medium due to evaporation of the medium, and the rate of decrease in the total volume is slower than that of the control group. Also, the result of comparing the volume of the increased cells alone is observed to have a tendency to gradually increase the cell volume from 4 days later, and thus it is thought that such a result can be boosted.

As a method for measuring the growth state of cells, the biological weight and dry weight of cells, which are the most common measures, are measured.
In general, the growth curves of all cells are displayed as S-shaped curves, which are classified into four stages. In other words, there is a lag phase in which the cells do not proliferate as a period of adaptation to the medium and remain in a state where the mass does not increase, and a curve having a steep gradient with the mass increasing to a rapid growth rate after this period has elapsed and a rapid growth rate has elapsed. The exponential phase, which shows the maximum growth and the growth arrested, and the stationary phase, in which growth does not show any further mass increase, and the cell depletion due to nutrient depletion, excretion of toxic components and saturation of cell density The tendency to rupture and die is divided into a dead phase in which the total cell volume and mass decrease.

[Table 22] and [Table 23] are the results of measuring the cell biological weight and dry weight. [Table 22] follows a four-stage growth curve. When the soft jade was used, compared to the control group that did not use the soft jade after 7 days, the growth rate was gradually increased, and then the growth was stopped, unlike the control group, which showed a decrease in cell biomass. It shows a tendency to be maintained until the day after. Compared to the change in the concentration of glucose, a nutrient that acts as the main metabolic substrate in the medium, cell growth continues even when this nutrient is almost depleted and the concentration in the medium becomes zero. Note the points. At this point when nutrients are depleted, as in the control group that did not use soft jade, it is common to show a tendency for growth to stop and the growth rate to decrease, but this is not the case when soft jade is used. Considering the fact that different phenomena are exhibited, it is presumed that there is an effect of softballs on cell growth. As can be seen from the results of measuring the dry cell weight in Table 23, the results show that the cells grew at a higher rate than the control group after the third day, and from Table 9 onwards, the cells grew from the ninth day. ].

As a result, cells grown close to the soft jade in the growth medium had a better effect on cell growth than the control group that did not. Digitalis lanata plant cells exhibiting a growth limit period of about 10 days. When cultured using soft jade, plant cells are stable even after 10 days without necrosis of the cells without replacement with a new medium. It is expected that this method can be applied as an advantageous method for optimizing cell growth and concentration in a production process for producing a useful substance, in order to maintain the state of cell growth and to exhibit a cell proliferation phenomenon.

Effect of Soft Jade on Changes in Medium pH

[0075]

[Table 24]

[0076]

[Table 25]

[Table 24] shows changes in the pH of the medium in the case where soft jade was used in the growth medium and in the control group where no soft jade was used. The control group shows a pH tendency in the medium applied to the case of general plant cells, and gradually becomes lower with the passage of time, and shows a phenomenon that the line is maintained.
However, when the soft jade was used, until the 7th day, the appearance was similar to that of the control group and then gradually increased. Such a phenomenon is extremely manifested in the results of [Table 25] which shows the results in a production medium in which flour powder is directly added to a culture solution. In the case of the control group to which no flour powder was added, the pH continuously decreased, but when the soft flour powder was added, the value tended to be maintained. This is presumed to be caused by the ionic reaction caused by the mineral organisms contained in the soft jade.

Table 26 and Table 27 below show the state of the analytical measuring instrument and the analytical results. These data are summarized for each sample and shown in Table 28. ] To [Table 31]. [Table 2
8] is a measurement of each analysis item for 48 hours (Sample 1) after 20 g of soft globules were put into the solution. In this table, there is no change in each measurement item, and no influence by the softball appears. [Table 29] shows that 2
Forty-eight hours have elapsed since the 0 g of the soft-bead was placed (Sample 2), the measurement values were obtained for each analysis item. In this experiment, no change appeared for each analysis item. Even when flour powder was placed outside the solution shown in [Table 31] (Sample 4), there was no change for each analysis item. In the case of Sample 3, data obtained by measuring each analysis item of the sample 48 hours after the addition of 20 g of soft-ball flour in the solution is shown in [Table 30]. Many changes that can be seen from this table are as follows.

Cr, Pb, Ni and Co harmful to the human body are 4
After 8 hours, it changed greatly. When Cr was not added, that is, 45.30 mg before the reaction, Cr was reduced to 0 48 hours after the addition of the flour, and Cr was also reduced from 13.76 mg to 0. It has been completely removed. Ni decreased from 51.8 mg to 1.733 mg, and Co also decreased from 52.69 mg to 11.94 m.
g.

Mg, one of the elements necessary for the human body, is 4
It increased from 8.36 mg to 55.74 mg. This increased in combination with the components of the softball itself, but there was no change in hardness. The hydrogen ion concentration of the distilled water was acidic at pH 3.5, but after the reaction, the pH changed to neutral at pH 6.8, and the conductivity sharply decreased. The adsorption power is about 3-4 mmol.q / g (equivalent), which is a physically large amount.

[0081]

[Table 26]

[0082]

[Table 27]

[0083]

[Table 28]

[0084]

[Table 29]

[0085]

[Table 30]

[0086]

[Table 31]

As described above, the digitalis lanata plant suspension cells cultured for one week with a soft jade close to them exhibited about 30% or more growth in the absence of the soft jade. This is a rarer good growth result in many experiments performed for growth effects on conventional Digitalis lanata plant cells for high concentration cultures.

Further, in an experiment on how the softball changes the hard water, it was found that the softball softened the hard water even without coming into contact with water. In particular, in a component analysis experiment on water using distilled water, in the component analysis 48 hours after precipitation of the soft-ball flour, Ni, C
Unusual phenomena such as decrease of o component, removal of Cr and Pb, and phenomena such as increase of Mg with removal of heavy metal were observed.

As described above, the softballs and softball powders according to the present invention, which have not been apparently theoretically investigated so far, can change the hardness of water even without contact with water, and have the digitalislanata (Digitalis lanata). lanata) 3 plant suspension cells
It can be seen from the results of the infrared experiment of Experimental Example 5 that not only the growth of 0% or more, but also the removal of heavy metal components harmful to the human body, such as the reduction of Ni and Co components, the removal of Cr and Pb, etc. It can be clearly seen that the radiation effects of the electromagnetic wave wavelength of the flour powder and the ionic reaction caused by the mineral components contained in the flour. This also appears to be assured by the efficacy exhibited by the products according to the invention described above.

Such experimental results indicate that, in the case of the synthetic resin container containing the soft-ball flour of the present invention, the removal of heavy metals and the softening of hard water when storing food, drinking water, etc., and the synthetic resin product of the present invention This suggests the possibility of promoting the growth of organisms when used as a chalet or flower pot. <Experimental Example 10> In this experimental example, 50 male and female adults complaining or being diagnosed with symptoms such as headache, insomnia, numbness of limbs, indigestion, etc., were subjected to the accessory (neck) manufactured in Example 2 of the present invention. 20) at least one of the following:
After wearing for days, the effect was evaluated by questionnaire survey. The results are shown in [Table 32] below.

[0091]

[Table 32]

As can be seen from the above experimental results, when wearing a jewelry made of the synthetic resin of the present invention on the body, headache (80%), insomnia (81%), numbness of limbs (90%) were observed.
%) And indigestion (89%) were alleviated. <Experimental Example 11> In this experimental example, in order to know the bactericidal effect of Tamami and the Tamami used in the material of the present invention on the outside of the living body, an experiment was conducted on the effect of Tamami and Tamami on the germicidal effect. Performed by requesting a biology lab from the University of Natural Sciences.

The results of the research experiment will be described in detail below. Materials and Methods Specimen We used flour and tamsui collected at the soft jade mine located in Woljeong-ri, Dongmyeon, Chuncheon-si, Gangwon-do.

2. Experimental strains and culture The most symmetric strains that can come into contact with the skin in nature are the gram-positive bacteria Bacillus subtilis, the gram-negative bacteria Escherichia coli, and the yeast Saccharomyces cerevisiae (baker's yeast, Beer yeast and wine yeast). The strain used in the experiment is a strain that is stored and subcultured in the laboratory, and 3
The experiment was carried out after culturing the cells in a liquid medium at 7 ° C. for 24 hours to allow physiological activity. Bacillus subtilis, a gram-positive bacterium (Ba
cillus subtilis) and E. coli (Es
cherichia coli) is a nutrient liquid medium (Yeas
textract 3g, Bacto-peptone 5g, Sodium chloride 8g /
D. W11) was cultured with shaking in a 37 ° C incubator for 24 hours. The yeast, Saccharomyces cerevisiae, is
(Yeast extract 3g, Bacto-peptone 10g, Dextrose 30g
/ D. W 11) Shaking culture was performed in a liquid medium (Gerhardt et al., 1994) in a 30 ° C. incubator for 24 hours.

3. Ultraviolet irradiation method 1 ml was collected from the strain cultured for 24 hours and diluted in sterilized water.
tilis) and Escherichia c, a gram-negative bacterium
oli) is a nutrient (Nutrient) solid medium (Yeast extract 3)
g, Bacto-peptone 5g, Sodium chloride 8g, Agar 15g /
D. W11), the yeast Saccharomyces cerevisia
e is YPD (Yeast extract 3g, Bacto-peptone 10g, Dext
rose 30g, Agar 15g / D. W 11) A solid medium was inoculated in an amount of 0.1 ml each. Each of the strains inoculated on the solid medium was analyzed using an ultraviolet lamp (1
(15 V, 30 W, 2537 ° tube lamp) 50 cm below, and irradiated for each strain. Gram-positive and gram-negative bacteria were irradiated with ultraviolet light for 1 minute and 40 seconds, and yeast were irradiated for 1 minute and 30 seconds, and the ultraviolet light in the sterile table was measured with a Photometer (Licon LI-189). As a control group, the number of cells of the solid medium which was not irradiated with ultraviolet rays was used.

4. Distribution of hemolytic bacteria Among the microbial populations that are resident in ball meal and Tamami, a blood agar plate (BAP) is used to confirm the hemolytic bacteria population known as pathogenic bacteria. Counted (Be
nson, 1994). Blood agar medium (Trypticase soy aga
r (BBL) 40 g / D. W. 11) is 48-50 ℃ after sterilization
After cooling to 5%, 5% sterile defibrillated sheepblood was added and used. The ball powder and Tamsui were smeared on a blood agar medium and cultured in a 37 ° C. incubator for 24 hours. The cultured plate was taken out, and the morphology of the colonies and the characteristics of hemolysis were observed. When the periphery of the colonies became a green ring, α hemolysis was determined, and when a completely transparent hemolytic ring appeared around the colonies, β hemolysis was determined. When there was no hemolysis, it was judged as non-hemolytic (γ-type).

[0097] 5. Measurement of microbial communities a. Microbial community by concentration of ball meal and Tamsui To know the effect of ball meal and Tamsui on the growth of Gram-positive bacteria, Gram-negative bacteria and yeasts, constant concentration of the balls and Tamsui in Nutrient liquid medium and YPD liquid medium Cultured on a gradient. Tamami is 10%, 25%, 50%, 100% (v
/ V) with a concentration of 5%, 10%, 20%, 3
Mix at a concentration gradient of 0% (w / v), gram-positive and gram-negative bacteria at 37 ° C for 24 hours, and yeast at 30 ° C for 2 hours.
The cells were cultured for 4 hours and counted. As a control group, a liquid medium to which no ball powder and ball water were added was used.

B. Ultraviolet ray blocking effect The ultraviolet ray blocking effect was calculated by converting the number of surviving cells of gram-positive bacteria, gram-negative bacteria and yeast into percentages by irradiating ultraviolet rays according to time. Gram-positive bacteria and Gram-negative bacteria are smeared on three nutrient solid media and irradiated with ultraviolet light (115V, 30W, 2537 ° tube light).
The cells were cultured at 37 ° C. for 24 hours. Yeast is smeared on YPD 30
The cells were cultured at 24 ° C. for 24 hours and counted. The ultraviolet ray blocking effect by the concentrations of ball meal and ball water made Gram-positive bacteria, Gram-negative bacteria and yeast the same concentration gradient. Tamami is 10%, 25%,
With a concentration gradient of 50% and 100% (v / v),
%, 10%, 20%, and 30% (w / v). Cell counts were converted by dilution factor to CFU (colo
ny forming unit) / ml.

Results and Discussion Hemolytic bacteria Hemolytic bacteria are inoculated on a blood agar medium and classified into α-type and β-type according to the type of hemolytic ring formed around the colony. When there is no hemolysis, it is called non-hemolysis (γ-type). α-hemolysis is the conversion of oxyhemoglobin to methemoglobin,
A green ring is formed around the settlement, and β-hemolysis shows a haemolysis ring in which the settlement is completely transparent. Such hemolysis is caused by hemolytic toxins (Brock et al.). Such haemolytic settlements were also confirmed in Tamame and Tamami. In ball meal, beta hemolysis averages 930 CFU / ml, gamma hemolysis is 190 CFU / ml, and in Tamami, beta hemolysis is 30 CFU / ml and gamma hemolysis is 730 C
It was confirmed to be FU / ml. The reason that β-hemolytic bacteria were detected relatively more in the ball meal than in the ball water was because the ball water was collected from the steamed water of the ball meal at the time of sampling the ball water. However, due to the contamination of microorganisms during the storage and transfer of the sample, a larger number of cells was confirmed than the sterilized and stored Tamsui sample. Therefore, when applying flour and water in folk remedies, it should be sterilized to eliminate the danger of pathogenic strains that induce toxicity. Also, when the water quality of the soft mine is contaminated, if it is collected and consumed as natural water at the soft mine, there is a risk of exposure to pathogenic bacteria.

2. Measurement of microbial community In order to know the effects of ball meal and water on the microbial community, add 10 balls of water to a nutrient liquid medium and a YPD liquid medium.
%, 25%, 50% and 100%.
Bamboo flour was mixed at a concentration gradient of 5%, 10%, 20%, and 30% before cultivation. When compared with a control group in which ball flour and Tamsui were not added, Bacillus subtilis and Sacchar
omyces cerevisiae showed almost similar appearance,
Escherichia coli is 10%, 25%, 50%
When Tamsui was added, the number of individuals was larger than that of the control group. This is because the trace element contained in Tamsui is Escherichia col.
i) affects the growth of Bacillus subtili
s) and Saccharomyces cerevisiae were not affected. Therefore, an interpretation linked to the growth of microorganisms would be possible only by determining the components and contents of the trace elements contained in Tamsui. Bacillus subtilis (Baci
llus subtilis), Escherichia coli, and
All Saccharomyces cerevisiae showed a smaller population than the control group. In addition, as the concentration of the ball dust increases, the number of individuals tends to decrease, which is interpreted as that the ball dust is a powder that is not solubilized in a liquid medium and is not an inorganic or organic ion that can be sufficiently used by microorganisms. it can.

3. Ultraviolet ray blocking effect Microorganisms of normal skin bacteria can be distinguished into resident bacteria and bacterial bacteria. Even though the indigenous bacterium remains somewhat permanent, there are many factors that affect its persistence and its extent. In other words, climatic factors and personal hygiene habits that affect changes in temperature and humidity, and the persistence and range of resident bacteria due to external factors, such as children having more Gram-negative bacteria and latent pathogens than adults. (Brock et al., 1992).
Therefore, gastrointestinal microorganisms such as Bacillus subtilis, which is a representative strain of Gram-positive bacteria and Escherichia coli in Gram-negative bacteria, scattered in water, soil, etc. In order to test the effect of blocking the ultraviolet rays of the ball dust and the ball water, bacteria that had passed through the skin were selected from the bacteria that lived on the skin.

The ultraviolet blocking effect of the ball powder and the ball water was confirmed by the sensitivity of the microorganisms to ultraviolet light. Bacillus subtilis, which is a gram-positive bacterium, is a liquid medium containing 20% and 30% of ball meal when irradiated with ultraviolet light for 40 seconds, and 23% and 13% respectively do not contain ball powder. The number of surviving individuals was greater than 12% in the control group. In addition, the liquid medium to which Tamsui was added showed a similar tendency. In the case of Escherichia coli, it represents the highest surviving population,
Such an aspect was more remarkable in the culture medium containing the ball meal than in the liquid medium containing the ball water. That is, an average of 74 in the liquid medium added with Tamamizu.
%, And 82% in the medium supplemented with ball meal, and 90% in the liquid medium containing 10% ball meal, showing the highest surviving population. Irrespective of the type of microorganism, the effect of blocking ultraviolet light was higher in the ball powder than in the ball water.

It is known that the sensitivity of microorganisms to ultraviolet light is in the order of Gram-negative bacteria, yeast, spore-forming bacteria, and mold, and the physiological activity of bacteria for bactericidal action of ultraviolet light is also affected by enzymes, moisture, environmental substances, and the like. . After UV irradiation, photoreactivation varies depending on the bacterial species. Ultraviolet light has a maximum sterilizing ability at a wavelength of 260 nm, and when irradiated with a 15 W ultraviolet light at a distance of 50 cm, E. coli and S. typhi were reported to be killed within 10 minutes (Isao Shibasaki,
1983). Cryptococcus neofumans (Cryptococcus neof), a kind of bacteria that cause deep mycosis
Ormans) were reported to show significant changes depending on the duration of UV irradiation when irradiated with UV (Fang et al., 1972). At 5 minutes, the normal strain and no lice were reported to have appeared. In addition, when treated for more than 10 minutes, it was reported that the cells themselves caused morphological changes and changes in the contents of the cells began to appear, and the irradiated bacterial strain for 30 minutes found a mode in which the cells were destroyed (Fang et al. 197
2). As a result of examining the number of surviving cells by irradiating ultraviolet rays to Gram-positive bacteria, Gram-negative bacteria and yeast according to time,
UV sensitivity is based on Bacillus subtilis, Sacc
haromyces cerevisiae, Escherichia coli
The order was confirmed. That is, the effect of blocking ultraviolet rays is E. coli (Es
cherichia coli), Saccharomyces cerevisiae, and Bacillus subtilis. However, Escherichia coli, which has a relatively large population, is considered in connection with the results of the evaluation of the growth effects of ball meal and ball water.
Was confirmed to have the highest blocking effect. Research on the bactericidal effect of sunlight on Escherichia coli and Proteus vulgaris among intestinal bacteria showed that the bacteria were killed in proportion to the average amount of solar radiation, but this bactericidal effect was not short-lived by ultraviolet light. In connection with the results reported to be the action of visible light at wavelengths (Che et al., 1982), the study of the bactericidal effect of sunlight would have to be complemented.

Conclusions In order to know the effects of blocking the ball dust and Tamsui on the living body,
Microorganisms (Gram ⁺ , Gram ^- and Eu
caryotic yeast), the following results were obtained. 1. The microbial population changes depending on the storage conditions of the ball powder and the ball water, which may induce toxicity during drinking in folk remedies. Therefore, it must be sterilized before use.

2. In ball powder, β-hemolysis averaged 930C
FU / ml, γ-hemolysis is 190 CFU / ml, in Tamsui,
β-hemolysis was confirmed to be 30 CFU / ml, and γ-hemolysis was confirmed to be 730 CFU / ml. 3. The size of the microbial community grown in the culture medium containing Tamame and Tamami showed a change in the number of individuals in a negative correlation with the concentration of Tamami, rather than the Tamami concentration.

4. When analyzed using the results of measuring the number of microorganisms that survived after irradiation with ultraviolet light, the liquid culture medium added with ball water showed a higher ultraviolet blocking effect than the liquid medium added with ball water. 5. The effect of blocking UV light is Escherichia coli,
Saccharomyces cerevisiae, Bacillus subtil
It was confirmed that the culture was in the order of is). As described above, it has been found that the ball dust used in the material of the present invention has a very high ultraviolet ray blocking effect.

[0107]

According to the present invention, the material containing flourballs is
Manufacture a variety of articles into soft jade, especially soft jade flour specified by a negative value of δ ^{180 with} peridotite in mouldy Dali Iwao, or add soft jade flour to the raw materials of each article during the manufacturing process of said article After doing
When mixed and molded by the usual method, the manufactured synthetic resin product only has excellent medical and physical effects such as heavy metal removal function, odor removal function, plant growth promotion function, water quality improvement function, etc. In addition, it has an increasing effect of improving the physical properties of each article itself.

[Brief description of the drawings]

FIG. 1 is a scanning electron microscope (SEM) photograph of a crystal structure diagram of a material of the present invention, which is magnified 1500 times.

FIG. 2A is a 1500-times enlarged SEM photograph of non-treated water of silk of the present invention, and FIG.
It is an enlargement of 000 times.

FIG. 3A is a graph showing S of the water-treated silk of ball dust with the material of the invention
The EM photograph was enlarged 1500 times, and B shows the SEM photograph of the water-treated ball dust water by the material of the present invention by 500 times.
It is enlarged to 0 times.

FIG. 4 is a diagram showing the change in activity of a test device (mouse on day 20) after drinking water of ball dust with the material of the present invention.

Claims (3)

[Claims] 1. A material containing flour, characterized by containing 5 to 15% by weight of flour. 2. The material containing flour powder according to claim 1, wherein the flour powder has a particle size of 100 to 350 mesh. In tremolite nephrite of wherein nephrite powder in bitter soil Dali Iwao, a negative value [delta] ¹⁸ 0, characterized in that the following composition (wt%), according to claim 1 or 2 A material containing soft flour powder. Silicon 34 Magnesium 10 Calcium 4.9 Iron 0.23 Aluminum 0.16 Copper 0.17 Cobalt 0.046 Manganese 0.14 Tin 0.024 Beryllium 0.00072 Silver 0.0013 Titanium 0.0038 Nickel 0.0028 Chromium 0 .0030 Other 0