JPH11169843A - 水溶液からアンモニアまたはアンモニウムイオンを選択的に除去する方法 - Google Patents
水溶液からアンモニアまたはアンモニウムイオンを選択的に除去する方法Info
- Publication number
- JPH11169843A JPH11169843A JP10280186A JP28018698A JPH11169843A JP H11169843 A JPH11169843 A JP H11169843A JP 10280186 A JP10280186 A JP 10280186A JP 28018698 A JP28018698 A JP 28018698A JP H11169843 A JPH11169843 A JP H11169843A
- Authority
- JP
- Japan
- Prior art keywords
- solution
- ammonia
- mineral
- regeneration
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims abstract description 67
- 238000000034 method Methods 0.000 title claims abstract description 41
- 229910021529 ammonia Inorganic materials 0.000 title claims abstract description 34
- 239000007864 aqueous solution Substances 0.000 title claims description 20
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 title abstract description 7
- 238000001179 sorption measurement Methods 0.000 claims abstract description 38
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 22
- 239000011707 mineral Substances 0.000 claims abstract description 22
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical group O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002351 wastewater Substances 0.000 claims abstract description 15
- 229910001413 alkali metal ion Inorganic materials 0.000 claims abstract description 13
- 238000007872 degassing Methods 0.000 claims abstract description 11
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000003546 flue gas Substances 0.000 claims abstract description 5
- 229910052649 zeolite group Inorganic materials 0.000 claims abstract description 5
- 239000000243 solution Substances 0.000 claims description 35
- -1 ammonium ions Chemical class 0.000 claims description 33
- 238000011069 regeneration method Methods 0.000 claims description 27
- 230000008929 regeneration Effects 0.000 claims description 26
- 235000010755 mineral Nutrition 0.000 claims description 20
- 241000894006 Bacteria Species 0.000 claims description 15
- 230000001172 regenerating effect Effects 0.000 claims description 14
- 239000002699 waste material Substances 0.000 claims description 14
- 239000010457 zeolite Substances 0.000 claims description 14
- 229910021536 Zeolite Inorganic materials 0.000 claims description 12
- 230000001546 nitrifying effect Effects 0.000 claims description 10
- 239000000725 suspension Substances 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 6
- 230000003113 alkalizing effect Effects 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 239000010802 sludge Substances 0.000 claims description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 4
- 239000012876 carrier material Substances 0.000 claims description 4
- 238000006477 desulfuration reaction Methods 0.000 claims description 4
- 230000023556 desulfurization Effects 0.000 claims description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 3
- JYIBXUUINYLWLR-UHFFFAOYSA-N aluminum;calcium;potassium;silicon;sodium;trihydrate Chemical compound O.O.O.[Na].[Al].[Si].[K].[Ca] JYIBXUUINYLWLR-UHFFFAOYSA-N 0.000 claims description 3
- 229910001603 clinoptilolite Inorganic materials 0.000 claims description 3
- 229920002635 polyurethane Polymers 0.000 claims description 3
- 239000004814 polyurethane Substances 0.000 claims description 3
- 238000000746 purification Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000005995 Aluminium silicate Substances 0.000 claims description 2
- 235000012211 aluminium silicate Nutrition 0.000 claims description 2
- 230000002209 hydrophobic effect Effects 0.000 claims description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 2
- 239000001103 potassium chloride Substances 0.000 claims description 2
- 235000011164 potassium chloride Nutrition 0.000 claims description 2
- 229910052611 pyroxene Inorganic materials 0.000 claims description 2
- 239000012266 salt solution Substances 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 229920003002 synthetic resin Polymers 0.000 claims description 2
- 239000000057 synthetic resin Substances 0.000 claims description 2
- 159000000011 group IA salts Chemical class 0.000 claims 1
- 150000002500 ions Chemical class 0.000 abstract description 4
- JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 abstract description 3
- 229910001424 calcium ion Inorganic materials 0.000 abstract description 3
- 229910001425 magnesium ion Inorganic materials 0.000 abstract description 3
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 abstract description 2
- 230000003009 desulfurizing effect Effects 0.000 abstract 1
- 239000003463 adsorbent Substances 0.000 description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
- 229910002651 NO3 Inorganic materials 0.000 description 5
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 5
- 239000011734 sodium Substances 0.000 description 5
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 150000003863 ammonium salts Chemical class 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000010881 fly ash Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000002054 transplantation Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/42—Treatment of water, waste water, or sewage by ion-exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/16—Alumino-silicates
- B01J20/165—Natural alumino-silicates, e.g. zeolites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/3408—Regenerating or reactivating of aluminosilicate molecular sieves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
- B01J20/3475—Regenerating or reactivating using a particular desorbing compound or mixture in the liquid phase
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
- B01J2220/56—Use in the form of a bed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
- B01J2220/60—Use in several different columns
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
- B01J2220/60—Use in several different columns
- B01J2220/606—Use in several different columns parallel disposed columns
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Hydrology & Water Resources (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Water Treatment By Sorption (AREA)
- Treating Waste Gases (AREA)
- Removal Of Specific Substances (AREA)
- Purification Treatments By Anaerobic Or Anaerobic And Aerobic Bacteria Or Animals (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19747444.6 | 1997-10-28 | ||
| DE19747444A DE19747444A1 (de) | 1997-10-28 | 1997-10-28 | Verfahren zur selektiven Eliminierung von Ammoniak bzw. Ammonium-Ionen aus einer wässrigen Lösung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH11169843A true JPH11169843A (ja) | 1999-06-29 |
Family
ID=7846785
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10280186A Pending JPH11169843A (ja) | 1997-10-28 | 1998-10-01 | 水溶液からアンモニアまたはアンモニウムイオンを選択的に除去する方法 |
Country Status (3)
| Country | Link |
|---|---|
| EP (1) | EP0915057A3 (de) |
| JP (1) | JPH11169843A (de) |
| DE (1) | DE19747444A1 (de) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100869059B1 (ko) | 2008-03-28 | 2008-11-17 | (주)대성그린테크 | 제올라이트 재생부산물을 이용한 고농도 질소함유 산업폐수 처리방법 |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2154973B1 (es) * | 1998-04-29 | 2001-11-16 | Consejo Superior Investigacion | Procedimiento para la filtracion de efluentes de tratamientos biologicos de aguas residuales urbanas. |
| FI109898B (fi) * | 2001-03-29 | 2002-10-31 | Kemira Chemicals Oy | Ammoniumtypen talteenotto jätevedestä |
| DE10337550B4 (de) * | 2003-08-14 | 2007-10-04 | Dr. Ecker Gmbh | Verfahren zur kontinuierlichen Regenerierung von Sorptionsmittel bei der Wasserreinigung |
| ITVR20090152A1 (it) * | 2009-09-30 | 2011-04-01 | Giovanni Bonometti | Impianto e procedimento per l'estrazione di azoto ammoniacale da reflui liquidi |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3723308A (en) * | 1970-11-16 | 1973-03-27 | D Breck | Process for removal of ammonia from waste water streams |
| DE2111794A1 (de) * | 1971-03-11 | 1972-09-28 | Hamburger Wasserwerke Gmbh | Verfahren zur biogenen Oxydation von in hoeheren Konzentrationen vorliegendem Ammonium in Wasser |
| US3985859A (en) * | 1974-07-03 | 1976-10-12 | Ecodyne Corporation | Vacuum stripping of ammonia |
| CA1048175A (en) * | 1974-07-15 | 1979-02-06 | John D. Sherman | Phillipsite-gismondite for ammonia |
| US4098690A (en) * | 1976-03-29 | 1978-07-04 | The University Of Illinois Foundation | Water purification process |
| JPS5370551A (en) * | 1976-12-03 | 1978-06-23 | Sumitomo Chem Co Ltd | Method of nitrifying ammonia contained in sewage |
| HU195457B (en) * | 1984-04-02 | 1988-05-30 | Vizepitoeipari Troeszt | Process for removing suspended materials, biogene nutrients and soluted metal-compounds from waters containing organic and inorganic impurities |
| US4695387A (en) * | 1985-05-07 | 1987-09-22 | Advanced Separation Technologies Incorporated | Removal of ammonia from wastewater |
| DD243486A1 (de) * | 1985-12-17 | 1987-03-04 | Projekt Wasserwirtschaft Veb | Verfahren und vorrichtung zur mikrobiellen wasserbehandlung |
| US5082813B1 (en) * | 1989-01-06 | 1998-06-02 | Petr Taborsky | Aluminiosilicates with modified cation affinity |
| FR2658807B1 (fr) * | 1990-02-27 | 1993-09-03 | Augarde Jacques | Traitement des eaux, des boues, et des dechets par reactifs mineraux recycles. |
| DE4138670A1 (de) * | 1991-11-25 | 1993-05-27 | Sued Chemie Ag | Verfahren zur gewinnung von landwirtschaftlich verwertbarem klaerschlamm |
| US5364439A (en) * | 1992-04-29 | 1994-11-15 | Union Oil Company Of California | Method to treat geothermal fluid streams |
| ATE159698T1 (de) * | 1993-02-04 | 1997-11-15 | Ct Umwelttechnik Ag | Anlage und verfahren zum weitergehenden reinigen von ablaufwasser aus einer biologischen kläranlage |
| US5484533A (en) * | 1994-01-04 | 1996-01-16 | A.C.T. Partnership, Ltd. | Method for the stabilization and detoxification of waste material |
-
1997
- 1997-10-28 DE DE19747444A patent/DE19747444A1/de not_active Withdrawn
-
1998
- 1998-09-10 EP EP98117092A patent/EP0915057A3/de not_active Withdrawn
- 1998-10-01 JP JP10280186A patent/JPH11169843A/ja active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100869059B1 (ko) | 2008-03-28 | 2008-11-17 | (주)대성그린테크 | 제올라이트 재생부산물을 이용한 고농도 질소함유 산업폐수 처리방법 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE19747444A1 (de) | 1999-04-29 |
| EP0915057A3 (de) | 1999-07-28 |
| EP0915057A2 (de) | 1999-05-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |