JPS5441900A - Purification of stevioside - Google Patents
Purification of steviosideInfo
- Publication number
- JPS5441900A JPS5441900A JP10689877A JP10689877A JPS5441900A JP S5441900 A JPS5441900 A JP S5441900A JP 10689877 A JP10689877 A JP 10689877A JP 10689877 A JP10689877 A JP 10689877A JP S5441900 A JPS5441900 A JP S5441900A
- Authority
- JP
- Japan
- Prior art keywords
- stevioside
- solution
- synthetic resin
- precipitate
- purification
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 title abstract 6
- 229940013618 stevioside Drugs 0.000 title abstract 6
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 title abstract 6
- 235000019202 steviosides Nutrition 0.000 title abstract 6
- 238000000746 purification Methods 0.000 title 1
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 abstract 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- 229920003002 synthetic resin Polymers 0.000 abstract 2
- 239000000057 synthetic resin Substances 0.000 abstract 2
- 239000002250 absorbent Substances 0.000 abstract 1
- 230000002745 absorbent Effects 0.000 abstract 1
- 239000003463 adsorbent Substances 0.000 abstract 1
- 229910000019 calcium carbonate Inorganic materials 0.000 abstract 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 abstract 1
- 239000000920 calcium hydroxide Substances 0.000 abstract 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 235000021096 natural sweeteners Nutrition 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
Landscapes
- Seasonings (AREA)
- Saccharide Compounds (AREA)
Abstract
PURPOSE:A solution containing stevioside is specifically pretreated and then treated with an adsorbent of synthetic resin to produce high-purity and colorless stevioside, a natural sweetener. CONSTITUTION:After calcium hydroxide is added to a crude stevioside solution, carbon dioxide is passed through the solution at room temperature to precipitate calcium carbonate and impurities. After the precipitate is removed, the stevioside solution is contacted with an absorbent of synthetic resin with macro network structure and then eluted, thus giving purified stevioside of the formula.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10689877A JPS5441900A (en) | 1977-09-06 | 1977-09-06 | Purification of stevioside |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10689877A JPS5441900A (en) | 1977-09-06 | 1977-09-06 | Purification of stevioside |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS5441900A true JPS5441900A (en) | 1979-04-03 |
Family
ID=14445276
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10689877A Pending JPS5441900A (en) | 1977-09-06 | 1977-09-06 | Purification of stevioside |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5441900A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5643632U (en) * | 1979-09-14 | 1981-04-20 | ||
| JPS5681027U (en) * | 1979-11-22 | 1981-07-01 | ||
| CN101946887A (en) * | 2010-09-01 | 2011-01-19 | 桂林莱茵生物科技股份有限公司 | Preparation method of stevioside |
| US9005444B2 (en) | 2008-05-13 | 2015-04-14 | Cargill, Incorporated | Separation of rebaudioside A from stevia glycosides using chromatography |
| US9131718B2 (en) | 2009-06-16 | 2015-09-15 | Epc (Beijing) Natural Products Co., Ltd. | Process for rebaudioside D |
| US9578895B2 (en) | 2010-08-23 | 2017-02-28 | Epc (Beijing) Natural Products Co., Ltd. | Rebaudioside A and stevioside compositions |
| US9795156B2 (en) | 2011-03-17 | 2017-10-24 | E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd | Rebaudioside B and derivatives |
| US10264811B2 (en) | 2014-05-19 | 2019-04-23 | Epc Natural Products Co., Ltd. | Stevia sweetener with improved solubility |
| US10357052B2 (en) | 2014-06-16 | 2019-07-23 | Sweet Green Fields USA LLC | Rebaudioside A and stevioside with improved solubilities |
| US10485256B2 (en) | 2014-06-20 | 2019-11-26 | Sweet Green Fields International Co., Limited | Stevia sweetener with improved solubility with a cyclodextrin |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5024300A (en) * | 1973-06-29 | 1975-03-15 | ||
| JPS5391173A (en) * | 1977-01-20 | 1978-08-10 | Chugai Pharmaceutical Co Ltd | Isolating method of steviaside |
-
1977
- 1977-09-06 JP JP10689877A patent/JPS5441900A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5024300A (en) * | 1973-06-29 | 1975-03-15 | ||
| JPS5391173A (en) * | 1977-01-20 | 1978-08-10 | Chugai Pharmaceutical Co Ltd | Isolating method of steviaside |
Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5643632U (en) * | 1979-09-14 | 1981-04-20 | ||
| JPS5681027U (en) * | 1979-11-22 | 1981-07-01 | ||
| US9005444B2 (en) | 2008-05-13 | 2015-04-14 | Cargill, Incorporated | Separation of rebaudioside A from stevia glycosides using chromatography |
| US9131718B2 (en) | 2009-06-16 | 2015-09-15 | Epc (Beijing) Natural Products Co., Ltd. | Process for rebaudioside D |
| US9635878B2 (en) | 2009-06-16 | 2017-05-02 | Epc (Beijing) Natural Products Co., Ltd. | Process for rebaudioside D |
| US10285425B2 (en) | 2010-08-23 | 2019-05-14 | Epc Natural Products Co. Ltd | Rebaudioside A and stevioside compositions |
| US9578895B2 (en) | 2010-08-23 | 2017-02-28 | Epc (Beijing) Natural Products Co., Ltd. | Rebaudioside A and stevioside compositions |
| US11202462B2 (en) | 2010-08-23 | 2021-12-21 | Sweet Green Fields International Co., Limited | Rebaudioside A and stevioside compositions |
| CN101946887A (en) * | 2010-09-01 | 2011-01-19 | 桂林莱茵生物科技股份有限公司 | Preparation method of stevioside |
| CN101946887B (en) | 2010-09-01 | 2012-10-03 | 桂林莱茵生物科技股份有限公司 | Preparation method of stevioside |
| US9795156B2 (en) | 2011-03-17 | 2017-10-24 | E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd | Rebaudioside B and derivatives |
| US11510428B2 (en) | 2011-03-17 | 2022-11-29 | Sweet Green Fields International Co., Limited | Rebaudioside B and derivatives |
| US10561165B2 (en) | 2014-05-19 | 2020-02-18 | Sweet Green Fields International Co., Limited | Stevia sweetener with improved solubility |
| US10264811B2 (en) | 2014-05-19 | 2019-04-23 | Epc Natural Products Co., Ltd. | Stevia sweetener with improved solubility |
| US11206857B2 (en) | 2014-05-19 | 2021-12-28 | Sweet Green Fields International Co., Limited | Stevia sweetener with improved solubility |
| US10357052B2 (en) | 2014-06-16 | 2019-07-23 | Sweet Green Fields USA LLC | Rebaudioside A and stevioside with improved solubilities |
| US10568351B2 (en) | 2014-06-16 | 2020-02-25 | Sweet Green Fields USA LLC | Rebaudioside A and stevioside with improved solubilities |
| US11241031B2 (en) | 2014-06-16 | 2022-02-08 | Sweet Green Fields Usa, Llc | Rebaudioside A and stevioside with improved solubilities |
| US10485256B2 (en) | 2014-06-20 | 2019-11-26 | Sweet Green Fields International Co., Limited | Stevia sweetener with improved solubility with a cyclodextrin |
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