JPS5479217A - Preparation of pinacolone - Google Patents

Preparation of pinacolone

Info

Publication number
JPS5479217A
JPS5479217A JP14542077A JP14542077A JPS5479217A JP S5479217 A JPS5479217 A JP S5479217A JP 14542077 A JP14542077 A JP 14542077A JP 14542077 A JP14542077 A JP 14542077A JP S5479217 A JPS5479217 A JP S5479217A
Authority
JP
Japan
Prior art keywords
methyl
butene
reaction
pinacolone
formaldehyde
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP14542077A
Other languages
Japanese (ja)
Other versions
JPS6410505B2 (en
Inventor
Sunao Kyo
Hidetsugu Tanaka
Haruo Tsuchiya
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kuraray Co Ltd
Original Assignee
Kuraray Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kuraray Co Ltd filed Critical Kuraray Co Ltd
Priority to JP14542077A priority Critical patent/JPS5479217A/en
Publication of JPS5479217A publication Critical patent/JPS5479217A/en
Publication of JPS6410505B2 publication Critical patent/JPS6410505B2/ja
Granted legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To obtain pinacolone (tertiary butyl methyl ketone) easily and in high yield, by the reaction of 3-methyl-1-butene with formaldehyde at a specific temp. in the presence of an aqueous solution of an inorganic acid.
CONSTITUTION: Pinacolone is obtained by the reaction of 3-methyl-1-butene with formaldehyde at 80-200°C under the atmospheric pressure-30Kg/cm2 for 1-10 hr in the presence of an aqueous solution of an inorganic acid, e.g. hydrochloric acid, where 2-methyl-1-butene or 2-methyl-2-butene, possibly formed as a by-product in the preparation of 3-methyl-1-butene, may be present. The acid used is isolated from the organic layer after the reaction and recycled at need by concentration or other methods.
EFFECT: No use or formation of harmful substances and large amounts of industrial wastes. This process may not cause the environmental pollution.
USE: Solvent or synthetic intermediate for pesticides, rubber goods.
COPYRIGHT: (C)1979,JPO&Japio
JP14542077A 1977-12-02 1977-12-02 Preparation of pinacolone Granted JPS5479217A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP14542077A JPS5479217A (en) 1977-12-02 1977-12-02 Preparation of pinacolone

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP14542077A JPS5479217A (en) 1977-12-02 1977-12-02 Preparation of pinacolone

Publications (2)

Publication Number Publication Date
JPS5479217A true JPS5479217A (en) 1979-06-25
JPS6410505B2 JPS6410505B2 (en) 1989-02-22

Family

ID=15384828

Family Applications (1)

Application Number Title Priority Date Filing Date
JP14542077A Granted JPS5479217A (en) 1977-12-02 1977-12-02 Preparation of pinacolone

Country Status (1)

Country Link
JP (1) JPS5479217A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106397150A (en) * 2016-08-26 2017-02-15 张家港市振方化工有限公司 Preparation method of pinacolone
CN109809972A (en) * 2019-01-11 2019-05-28 栎安化学(上海)有限公司 A kind of method that green prepares pinacoline
CN114507125A (en) * 2022-02-24 2022-05-17 南通利奥化工科技有限公司 A kind of preparation method of pinacolone

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106397150A (en) * 2016-08-26 2017-02-15 张家港市振方化工有限公司 Preparation method of pinacolone
CN109809972A (en) * 2019-01-11 2019-05-28 栎安化学(上海)有限公司 A kind of method that green prepares pinacoline
CN114507125A (en) * 2022-02-24 2022-05-17 南通利奥化工科技有限公司 A kind of preparation method of pinacolone

Also Published As

Publication number Publication date
JPS6410505B2 (en) 1989-02-22

Similar Documents

Publication Publication Date Title
GB882524A (en) Manufacture of chlorinated polyethylene
ES463106A1 (en) Method for the production of 2,4,6-tri(3,5-ditertiary butyl-4-hydroxybenzyl) mesitylene
JPS5479217A (en) Preparation of pinacolone
ATE640T1 (en) PROCESS FOR OBTAINING A CONJUGATED DIOLEFIN FROM A C 4 OR C 5 HYDROCARBON MIXTURE.
AU8973691A (en) Process for the preparation of mixtures of cyclic acrolein glycerol acetals
JPS5277021A (en) Preparation of s-chlorobensaldenyde
ATE3848T1 (en) PROCESS FOR THE PRODUCTION OF COBALT(II) ACETYLACETONATE.
JPS5353632A (en) Preparation f aromatic ketones
JPS5359651A (en) Preparation of 2-chlorocyclododecanone
JPS5278831A (en) Recovery of urea adsorbed on ion-exchange resin
GB1162078A (en) Method of Process Acid Wastes from the Process of Chloromethyllating Copolymers of Styrene and Compounds of the Vinylaromatic Series
JPS5262201A (en) Bromination process
O'Gorman Attempted repetition of a reported total asymmetric synthesis
JPS57197279A (en) Novel hexaminum compound and its preparation
JPS53144543A (en) Improved method of producing cylcohexane derivative
JPS6490160A (en) Production of ethylene cyanohydrin
JPS5257111A (en) Process for organic carboxylic acid silver
JPS5359649A (en) Improved process for preparation of cyclohexane derivatives
JPS5432414A (en) Preparation of organic acid ester
JPS5346962A (en) Preparation of thiopheneacetic acids
FR2224443B3 (en)
JPS5630947A (en) Preparation of 3-bromobenzoic acid
JPS57142937A (en) Norbornyl-2-aldehyde having unsaturated hydrocarbon side chain and its preparation
JPS5645434A (en) Preparation of alpha-hydroxy-alpha- 2,7-octadienyl carbonyl compound
JPS5439019A (en) Preparation of 2-bromo-3-methylbutyryl urea