JPS5538331A - Separation of aromatic aldehyde - Google Patents
Separation of aromatic aldehydeInfo
- Publication number
- JPS5538331A JPS5538331A JP11179878A JP11179878A JPS5538331A JP S5538331 A JPS5538331 A JP S5538331A JP 11179878 A JP11179878 A JP 11179878A JP 11179878 A JP11179878 A JP 11179878A JP S5538331 A JPS5538331 A JP S5538331A
- Authority
- JP
- Japan
- Prior art keywords
- aldehyde
- bisulfite
- adduct
- aqueous solution
- solution containing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE:To separate and recover an aromatic aldehyde from a mixture containing the same, in high yield, at a low temperature, without loss of a bisulfite, etc., by using a sulfite together with a bisulfite, thereby accelerating the decomposition of an aldehyde adduct and the extraction of isolated aldehyde. CONSTITUTION:A mixture containing an aromatic aldehyde is mixed with an aqueous solution containing a bisulfite (pref. alkali metal bisulfite, esp. Na and/or K bisulfite), to form an aldehyde adduct. The aqueous solution containing said adduct is brought into contact with an oil-soluble and water-insoluble solvent having higher bioling point than the separated aldehyde, in the presence of an aqueous solution containing a bisulfite and a sulfite (alkali metal salt, esp. Na and/or K salts), and the aldehyde adduct is decomposed into aldehyde and the bisulfite. The isolated aldehyde is extracted with an oil-soluble solvent at >=30 deg.C. The aqueous layer is pref. recycled and reused.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11179878A JPS5538331A (en) | 1978-09-13 | 1978-09-13 | Separation of aromatic aldehyde |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11179878A JPS5538331A (en) | 1978-09-13 | 1978-09-13 | Separation of aromatic aldehyde |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS5538331A true JPS5538331A (en) | 1980-03-17 |
Family
ID=14570413
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11179878A Pending JPS5538331A (en) | 1978-09-13 | 1978-09-13 | Separation of aromatic aldehyde |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5538331A (en) |
-
1978
- 1978-09-13 JP JP11179878A patent/JPS5538331A/en active Pending
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