JPS5544312A - Production of granular cellulose gel - Google Patents
Production of granular cellulose gelInfo
- Publication number
- JPS5544312A JPS5544312A JP11666178A JP11666178A JPS5544312A JP S5544312 A JPS5544312 A JP S5544312A JP 11666178 A JP11666178 A JP 11666178A JP 11666178 A JP11666178 A JP 11666178A JP S5544312 A JPS5544312 A JP S5544312A
- Authority
- JP
- Japan
- Prior art keywords
- cellulose
- calcium
- same
- solution
- granular
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- PTHCMJGKKRQCBF-UHFFFAOYSA-N Cellulose, microcrystalline Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC)C(CO)O1 PTHCMJGKKRQCBF-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- 229910052791 calcium Inorganic materials 0.000 abstract 3
- 239000011575 calcium Substances 0.000 abstract 3
- 159000000007 calcium salts Chemical class 0.000 abstract 2
- 229920002678 cellulose Polymers 0.000 abstract 2
- 239000001913 cellulose Substances 0.000 abstract 2
- 239000000499 gel Substances 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 abstract 2
- 229920000875 Dissolving pulp Polymers 0.000 abstract 1
- 229920000297 Rayon Polymers 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000008064 anhydrides Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000011324 bead Substances 0.000 abstract 1
- 238000004587 chromatography analysis Methods 0.000 abstract 1
- 238000011033 desalting Methods 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- 238000002523 gelfiltration Methods 0.000 abstract 1
- 238000005342 ion exchange Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000011148 porous material Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 239000002964 rayon Substances 0.000 abstract 1
- 239000012266 salt solution Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
- Glanulating (AREA)
Abstract
PURPOSE: To produce the granular cellulose gel material having fine pore distribution characteristics and mechanical stability by dissolving cellulose in an aqueous solution of calcium thicyanate, etc. and letting the same disperse in an organic solvent then desalting the same.
CONSTITUTION: Cellulose raw materials such as of hulp or the like for rayon production are dissolved about 1W15% in the aqueous calcium salt solution composed primarily of calcium thiocynate (containing calcium acid at about 50W60% as anhydride) and the solution is cooled to gel. This is ground and is dispersed in an organic solvent such as of carbon tetrachloride added with a small amount of surfactants. Next, this is mixed with a dispersion solution and a solvent such as methanol or other which dissolves calcium salt is added to desalte the same, after which it is washed with water. This method yields the cellulose gels of granular or beads form useful for gel filtration, ion exchange, chromatography, etc.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11666178A JPS5544312A (en) | 1978-09-25 | 1978-09-25 | Production of granular cellulose gel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11666178A JPS5544312A (en) | 1978-09-25 | 1978-09-25 | Production of granular cellulose gel |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5544312A true JPS5544312A (en) | 1980-03-28 |
| JPS6362252B2 JPS6362252B2 (en) | 1988-12-01 |
Family
ID=14692756
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11666178A Granted JPS5544312A (en) | 1978-09-25 | 1978-09-25 | Production of granular cellulose gel |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5544312A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5328603A (en) * | 1990-03-20 | 1994-07-12 | The Center For Innovative Technology | Lignocellulosic and cellulosic beads for use in affinity and immunoaffinity chromatography of high molecular weight proteins |
| JPWO2005083056A1 (en) * | 2004-03-02 | 2008-01-17 | 独立行政法人海洋研究開発機構 | Cellulose solid medium and method for producing the same |
| WO2015029790A1 (en) | 2013-09-02 | 2015-03-05 | Jnc株式会社 | Method for producing porous cellulose particles, and porous cellulose particles |
| WO2025216143A1 (en) * | 2024-04-12 | 2025-10-16 | Jnc株式会社 | Fine magnetic particles and production method for same |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014061411A1 (en) | 2012-10-18 | 2014-04-24 | Jnc株式会社 | Cation exchange chromatography carrier for refining of antibodies, and method for separation of antibody monomers from polymers thereof produced in antibody drug manufacturing process |
-
1978
- 1978-09-25 JP JP11666178A patent/JPS5544312A/en active Granted
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5328603A (en) * | 1990-03-20 | 1994-07-12 | The Center For Innovative Technology | Lignocellulosic and cellulosic beads for use in affinity and immunoaffinity chromatography of high molecular weight proteins |
| JPWO2005083056A1 (en) * | 2004-03-02 | 2008-01-17 | 独立行政法人海洋研究開発機構 | Cellulose solid medium and method for producing the same |
| US7790457B2 (en) | 2004-03-02 | 2010-09-07 | Japan Agency For Marine-Earth Science And Technology | Solid cellulosic culture medium and process for producing the same |
| JP4665184B2 (en) * | 2004-03-02 | 2011-04-06 | 独立行政法人海洋研究開発機構 | Cellulose solid medium and production method thereof |
| WO2015029790A1 (en) | 2013-09-02 | 2015-03-05 | Jnc株式会社 | Method for producing porous cellulose particles, and porous cellulose particles |
| US11685793B2 (en) | 2013-09-02 | 2023-06-27 | Jnc Corporation | Method for producing porous cellulose particles, and porous cellulose particles |
| WO2025216143A1 (en) * | 2024-04-12 | 2025-10-16 | Jnc株式会社 | Fine magnetic particles and production method for same |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6362252B2 (en) | 1988-12-01 |
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