JPS5547211A - Production of lithium nitride - Google Patents
Production of lithium nitrideInfo
- Publication number
- JPS5547211A JPS5547211A JP11920978A JP11920978A JPS5547211A JP S5547211 A JPS5547211 A JP S5547211A JP 11920978 A JP11920978 A JP 11920978A JP 11920978 A JP11920978 A JP 11920978A JP S5547211 A JPS5547211 A JP S5547211A
- Authority
- JP
- Japan
- Prior art keywords
- lithium
- gas
- lithium nitride
- nitrided
- temp
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- IDBFBDSKYCUNPW-UHFFFAOYSA-N lithium nitride Chemical compound [Li]N([Li])[Li] IDBFBDSKYCUNPW-UHFFFAOYSA-N 0.000 title abstract 3
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 abstract 3
- 229910052744 lithium Inorganic materials 0.000 abstract 3
- 238000010438 heat treatment Methods 0.000 abstract 2
- 239000012298 atmosphere Substances 0.000 abstract 1
- 238000005452 bending Methods 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000011109 contamination Methods 0.000 abstract 1
- 238000007796 conventional method Methods 0.000 abstract 1
- 238000005121 nitriding Methods 0.000 abstract 1
- 239000012299 nitrogen atmosphere Substances 0.000 abstract 1
- 238000005498 polishing Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/0607—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with alkali metals
- C01B21/061—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with alkali metals with lithium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)
Abstract
PURPOSE: To efficiently obtain lithium nitride without requiring heating by producing a working strain in metallic lithium followed by nitriding in N2 gas or mixed gas of N2 gas and rare gas.
CONSTITUTION: Metallic lithium of 99.9% purity is subjected to plastic deformation such as press. bending or polishing to produce a working strain, and it is nitrided in a reactor under an N2 atmosphere or an N2-rare gas type atmosphere. At this time, the lithium is thoroughly nitrided to the interior without requiring heating unlike a conventional method. Since no sudden temp. rise occurs, the reactor, etc. are not damaged, and contamination of the reaction product is prevented. No temp. control is also required, and lithium nitride is obtd. efficiently with a simple apparatus.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11920978A JPS5547211A (en) | 1978-09-29 | 1978-09-29 | Production of lithium nitride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11920978A JPS5547211A (en) | 1978-09-29 | 1978-09-29 | Production of lithium nitride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS5547211A true JPS5547211A (en) | 1980-04-03 |
Family
ID=14755627
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11920978A Pending JPS5547211A (en) | 1978-09-29 | 1978-09-29 | Production of lithium nitride |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5547211A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6096282A (en) * | 1996-09-10 | 2000-08-01 | The Regents Of The University Of California | Instantaneous synthesis of refractory nitrides from solid precursors |
| JP2014201511A (en) * | 2013-04-09 | 2014-10-27 | 古河機械金属株式会社 | Method of producing lithium nitride |
| JP2015074566A (en) * | 2013-10-07 | 2015-04-20 | 古河機械金属株式会社 | Method for producing lithium nitride |
-
1978
- 1978-09-29 JP JP11920978A patent/JPS5547211A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6096282A (en) * | 1996-09-10 | 2000-08-01 | The Regents Of The University Of California | Instantaneous synthesis of refractory nitrides from solid precursors |
| JP2014201511A (en) * | 2013-04-09 | 2014-10-27 | 古河機械金属株式会社 | Method of producing lithium nitride |
| JP2015074566A (en) * | 2013-10-07 | 2015-04-20 | 古河機械金属株式会社 | Method for producing lithium nitride |
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