JPS5629527A - Purification of unreacted isoprene and recovered solvent - Google Patents
Purification of unreacted isoprene and recovered solventInfo
- Publication number
- JPS5629527A JPS5629527A JP10362479A JP10362479A JPS5629527A JP S5629527 A JPS5629527 A JP S5629527A JP 10362479 A JP10362479 A JP 10362479A JP 10362479 A JP10362479 A JP 10362479A JP S5629527 A JPS5629527 A JP S5629527A
- Authority
- JP
- Japan
- Prior art keywords
- pipe
- solvent
- cyclopentadiene
- isoprene
- fraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 title abstract 12
- 239000002904 solvent Substances 0.000 title abstract 6
- 238000000746 purification Methods 0.000 title 1
- ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 abstract 10
- 238000004821 distillation Methods 0.000 abstract 5
- 238000011084 recovery Methods 0.000 abstract 4
- 239000000203 mixture Substances 0.000 abstract 2
- 238000006116 polymerization reaction Methods 0.000 abstract 2
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
PURPOSE: To remove cyclopentadiene, in high efficiency, from a mixture of unreacted isoprene and a solvent recovered from isoprene polymerization process, by extracting a part of recovered cyclopentadiene fraction obtained by the distillation and recovery of said mixture, from the bottom of the distillation column.
CONSTITUTION: Recovered fraction obtained from the isoprene polymerization process and containing unreacted isoprene and a solvent (e.g. ≤5C aliphatic hydrocarbon), is supplied to the distillation column 2 through the pipe 1 to perform distillation, and isoprene and the solvent are obtained through the pipe 3. The side stream is extracted through the pipe 5 as gaseous state, and distilled in a distillation column 6. Purified recovery fraction is obtained through the pipe 7. The bottom fraction is recycled through the pipe 8 after the heat recovery and cooling. The concentrated cyclopentadiene fraction obtained through the pipe 9 is introduced into the solvent recovery column 10 as side stream, and cyclopentadiene is extracted through the pipe 11. The recovered solvent is taken out from the bottom and recycled through the pipe 12 to the column 6.
EFFECT: The required amount of cyclopentadiene can be removed by treating a small amount of the fraction.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10362479A JPS5629527A (en) | 1979-08-16 | 1979-08-16 | Purification of unreacted isoprene and recovered solvent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10362479A JPS5629527A (en) | 1979-08-16 | 1979-08-16 | Purification of unreacted isoprene and recovered solvent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5629527A true JPS5629527A (en) | 1981-03-24 |
| JPS6225129B2 JPS6225129B2 (en) | 1987-06-01 |
Family
ID=14358915
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10362479A Granted JPS5629527A (en) | 1979-08-16 | 1979-08-16 | Purification of unreacted isoprene and recovered solvent |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5629527A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6110102U (en) * | 1984-06-25 | 1986-01-21 | 晃一 星野 | automatic hair curler |
-
1979
- 1979-08-16 JP JP10362479A patent/JPS5629527A/en active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6110102U (en) * | 1984-06-25 | 1986-01-21 | 晃一 星野 | automatic hair curler |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6225129B2 (en) | 1987-06-01 |
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