JPS5735529A - Preparation of aluminum alcoholate - Google Patents
Preparation of aluminum alcoholateInfo
- Publication number
- JPS5735529A JPS5735529A JP11080580A JP11080580A JPS5735529A JP S5735529 A JPS5735529 A JP S5735529A JP 11080580 A JP11080580 A JP 11080580A JP 11080580 A JP11080580 A JP 11080580A JP S5735529 A JPS5735529 A JP S5735529A
- Authority
- JP
- Japan
- Prior art keywords
- aluminum
- aluminum foil
- granules
- microns
- give
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title abstract 8
- 229910052782 aluminium Inorganic materials 0.000 title abstract 6
- 239000011888 foil Substances 0.000 abstract 4
- 239000008187 granular material Substances 0.000 abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 230000001788 irregular Effects 0.000 abstract 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000000428 dust Substances 0.000 abstract 1
- 238000004880 explosion Methods 0.000 abstract 1
- 230000005484 gravity Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 238000005096 rolling process Methods 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain the titled compound efficiently in a short time, by using an aluminum foil prepared by rolling the aluminum foil into granules with irregular gaps therebetween in reacting a metallic aluminum with an anhydrous alcohol.
CONSTITUTION: An aluminum foil having a thickness of 6W150 microns, particularly 7W25 microns, is rolled into granules with irregular gaps therebetween, having a grain diameter of 0.5W10mm, preferably 1W5mm, to give a granular aluminum foil having a bulk specific gravity of 0.1W1, particularly 0.2W0.6. An anhydrous alcohol is reacted with the resultant granules usually at 70W100°C to give an aluminum alcoholate. According to the method, the reaction proceeds rapidly and smoothly due to the large surface area of the metallic aluminum, and the unreacted aluminum fragments will not remain. The reaction is not violent and there is no danger of dust explosion. There is an advantage in that the raw material is not bulky in the transportation thereof.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11080580A JPS605576B2 (en) | 1980-08-12 | 1980-08-12 | Preparation method of aluminum alcoholate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11080580A JPS605576B2 (en) | 1980-08-12 | 1980-08-12 | Preparation method of aluminum alcoholate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5735529A true JPS5735529A (en) | 1982-02-26 |
| JPS605576B2 JPS605576B2 (en) | 1985-02-12 |
Family
ID=14545095
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11080580A Expired JPS605576B2 (en) | 1980-08-12 | 1980-08-12 | Preparation method of aluminum alcoholate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS605576B2 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60218344A (en) * | 1984-04-14 | 1985-11-01 | Res Dev Corp Of Japan | Synthesis of aluminum alkoxide and unit therefor |
| JP2013060389A (en) * | 2011-09-13 | 2013-04-04 | Sumitomo Chemical Co Ltd | Method for producing aluminum alkoxide |
-
1980
- 1980-08-12 JP JP11080580A patent/JPS605576B2/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60218344A (en) * | 1984-04-14 | 1985-11-01 | Res Dev Corp Of Japan | Synthesis of aluminum alkoxide and unit therefor |
| JP2013060389A (en) * | 2011-09-13 | 2013-04-04 | Sumitomo Chemical Co Ltd | Method for producing aluminum alkoxide |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS605576B2 (en) | 1985-02-12 |
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